Structural study of Maya Blue: Textural, thermal and solid-state multinuclear magnetic resonance characterization of the palygorskite-indigo and sepiolite-indigo adducts

Clays and Clay Minerals

Volumn 51, Issue 3, 2003, Pages 318-326

  Hubbard, Basil ^a   Kuang, Wenxing ^a   Moser, Arvin ^a   Facey, Glenn A ^a   Detellier, Christian ^a  

^a UNIVERSITY OF OTTAWA   (Canada)

Author keywords

Indigo; Maya Blue; Palygorskite; Sepiolite; Solid state multinuclear magnetic resonance; Textural analysis; Thermal analysis

Indexed keywords

DYES; HEAT TREATMENT; MICROPOROSITY; MIXTURES; NUCLEAR MAGNETIC RESONANCE; SPECTRUM ANALYSIS; TEXTURES;

ADDUCTS;

CLAY MINERALS;

ARCHAEOLOGY; NUCLEAR MAGNETIC RESONANCE; PALYGORSKITE; PIGMENT; SEPIOLITE;

INDIGOFERA;

EID: 0038419655     PISSN: 00098604     EISSN: None     Source Type: Journal    
DOI: 10.1346/CCMN.2003.0510308     Document Type: Article

References (26)

1. Ahlrichs, J.L., Serna, C. and Serratosa, J.M. (1975) Structural hydroxyls in sepiolite. Clays and Clay Minerals, 23, 119-124.
2. Brindley, G.W. (1959) X-ray and electron diffraction data for sepiolite. American Mineralogist, 44, 495-500.
3. Cooksey, C.J. and Dronsfield, A.T. (2002) Adolf von Baeyer and the indigo molecule. Dyes in History and Archaeology. 18, 13-19.
4. Gettens, R.J. (1962) Maya blue: an unsolved problem in ancient pigments. American Antiquity, 27, 557-564.
5. Gettens, R.J. and Stout, G.L. (1946) Painting Materials: A Short Encyclopedia. D. Van Nostrand, New York, pp. 130-131.
6. Gordon, P.F. and Gregory, P. (1983) Indigoid Dyes. Pp. 208-211 in: Organic Chemistry in Colour. Springer-Verlag, Berlin.
7. Gribova, E.A. (1955) X-ray study of indigo and thioindigo. L. Ya. Karpov Physical Chemistry Institute: Doklady Akademii Nauk SSSR, 102, 279-81.
8. Horvath, G. and Kawazoe, K. (1983) Method for the calculation of effective pore size distribution in molecular sieve carbon. Journal of Chemical Engineering of Japan, 16, 470-475.
9. Jones, B.F. and Galán, E. (1998) Sepiolite and palygorskite. Pp. 631-674 in: Hydrous Phyllosilicates (S.W. Bailey, editor). Reviews in Mineralogy, 19. Mineralogical Society of America, Washington, D.C.
10. Jose-Yacaman, M., Rendon, L., Arenas, J. and Puche, M.C.S. (1996) Maya blue paint: an ancient nanostructured material. Science, 273, 223-225.
11. Kleber, R., Masschelein-Kleiner, L. and Thissen, J. (1967) Study and identification of Maya blue. Studies in Conservation, 12, 41-56.
12. th International Conference on Solid State Chemistry, Bratislava, Slovak Republic.
13. Le Van Mao, R., Rutinduka, E., Detellier, C., Gougay, P., Hascoet, V., Tavakoliyan, S., Hoa, S.V. and Matsuura, T. (1999) Mechanical and pore characteristics of zeolite composite membranes. Journal of Materials Chemistry, 9, 783-788.
14. Merwin, H.E. (1931) In: The Temple of the Warriors at Chichen Itza (E.H. Morris, J. Charlot and A.A. Morris, editors). Carnegic Institution of Washington. Washington, D.C., publ. 406.
15. Myriam, M., Suarez, M. and Martin-Pozas, J.M. (1998) Structural and textural modifications of palygorskite and sepiolite under acid treatment. Clays and Clay Minerals, 46, 225-231.
16. Pedro, G. (1972) Report of the AIPEA Nomenclature Committee. AIPEA Newsletter, 4, 3-4.
17. Polette, L.A., Meitzner, G., Jose-Yacaman, M. and Chianelli, R.R. (2002) Maya blue: application of XAS and HRTEM to materials science in art and archaeology. Microchemical Journal, 71, 167-174.
18. Ruiz-Hitzky, E. (2001) Molecular access to intracrystalline tunnels of sepiolite. Journal of Materials Chemistry, 11, 86-91.
19. Serna, C. and van Scoyoc, G.E. (1979) Infrared study of sepiolite and palygorskite surfaces. Pp. 197-206 in: Proceedings of the International Clay Conference, Oxford, 1978 (M.M. Mortland and V.C. Farmer, editors). Elsevier, Amsterdam.
20. Shepard, A. (1962) Maya blue: alternative hypotheses. American Antiquity, 27, 565-566.
21. Tagle, A., Paschinger, H., Richard, H. and Infante, G. (1990) Maya blue: its presence in Cuban colonial wall paintings. Studies in Conservation, 35, 156-159.
22. Van Olphen, H. (1966) Maya Blue: a clay mineral-organic pigment? Science, 154, 645-646.
23. Wang, Q.K., Matsuura, T., Feng, C.Y., Weir, M.R., Detellier, C., Rutinduka, E. and Le Van Mao, R. (2001) The sepiolite membrane for ultrafiltration. Journal of Membrane Science, 184, 153-163.
24. 29Si solid state NMR study of guest acetone molecules occupying the zeolitic channels of partially dehydrated sepiolite clay. Studies in Surface Science and Catalysis, 129, 551-558.
25. Weir, M.R., Rutinduka, E., Detellier, C., Feng, C.Y., Wang, Q., Matsuura, T. and Le Van Mao, R. (2001) Fabrication, characterization and preliminary testing of all-inorganic ultrafiltration membranes composed entirely of a naturally occurring sepiolite clay mineral. Journal of Membrane Science, 182, 41-50.
26. Weir, M.R., Kuang, W., Facey, G.A. and Detellier, C. (2002) Solid state nuclear magnetic resonance study of sepiolite and partially dehydrated sepiolite. Clays and Clay Minerals, 50, 240-247.