Structural Chemistry of Lithium Tetrahydroborate Ether Solvates

European Journal of Inorganic Chemistry

Volumn , Issue 7, 1998, Pages 941-949

  Giese, Hans Hermann ^a   Nöth, Heinrich ^a   Schwenk, Holger ^a   Thomas, Steffen ^a  

^a UNIVERSITY OF MUNICH   (Germany)

Author keywords

Lithium tetrahydridoborate diethyl ether (1:1); Lithium tetrahydridoborate dimethoxyethane (1:2); Lithium tetrahydridoborate diveron (1:1); Lithium tetrahydridoborate tetrahydrofuran (1:3); Lithium tetrahydridoborate triglyme (1:1)

Indexed keywords

ATOMS; CHAINS; HYDROGEN BONDS; LITHIUM COMPOUNDS; MOLECULES; NEGATIVE IONS; ORGANIC SOLVENTS;

DIETHYL ETHERS; DIOXOLANE; LI ATOMS; LITHIUM TETRAHYDRIDOBORATE DIETHYL ETHER (1:1); LITHIUM TETRAHYDRIDOBORATE DIMETHOXYETHANE (1:2); LITHIUM TETRAHYDRIDOBORATE DIVERON (1:1); LITHIUM TETRAHYDRIDOBORATE TETRAHYDROFURAN (1:3); LITHIUM TETRAHYDRIDOBORATE TRIGLYME (1:1); TETRA-HYDROFURAN; TETRAHYDROFURANS;

ETHERS;

EID: 0038398521     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1099-0682(199807)1998:7<941::AID-EJIC941>3.0.CO;2-Y     Document Type: Article

References (32)

1. H. Nöth, S. Thomas, M. Schmidt, Chem. Ber. 1996, 129, 451-458.
2. H. Hajos, Komplexe Hydride, VEB, Deutscher Verlag der Wissenschaften, Berlin, 1966.
3. K. M. Mackay, Hydrogen Compounds of the Metallic Elements, E. & F. N. Spon Ltd., London, 1996.
4. E. Wiberg, E. Amberger, Hydrides of the Elements of Main Groups I-IV, Elsevier Publ. Comp., Amsterdam, London, New York, 1971.
5. Y. M. Choi, S. Narasimha, Inorg Chem. 1981, 20, 4456-4457; 1982, 21, 3657-3661.
6. Y. M. Choi, S. Narasimha, Inorg Chem. 1981, 20, 4456-4457; 1982, 21, 3657-3661.
7. R. E. Mesmer, W. L. Jolly, Inorg. Chem. 1962, 1, 608-612 and literature cited therein; J. A. Gardiner, J. W. Collat, ibid. 1965, 4, 1208-1212.
8. R. E. Mesmer, W. L. Jolly, Inorg. Chem. 1962, 1, 608-612 and literature cited therein; J. A. Gardiner, J. W. Collat, ibid. 1965, 4, 1208-1212.
9. A. S. Antsyshikina, G. G. Sadikov, M. A. Porai-Koshits, V. N. Konoplev, T. A. Silina, A. S. Sizareva, Koord. Khim. 1994, 20, 277-284.
10. Gmelin Handbuch der Anorganischen Chemie, Supplement to 8th ed., vol. 33, Boron Compounds, part B, 1976.
11. T. L. Volski, H. B. Moore, L. E. Rott, K. J. Martin, G. W. Schaeffer, J. Am. Chem. Soc. 1958, 80, 522-549.
12. G. W. Schaeffer, T. L. Kolski, D. L. Ekstedt, J. Am. Chem. Soc. 1957, 79, 5912-5915.
13. E. Wiberg, H. Nöth, R. Usön, Z. Naturforsch., Part B 1956, 11, 490-491; T. L. Kolski, H. B. Moore, L. E. Roth, K. J. Martin, G. W. Schaeffer, J. Am. Chem. Soc. 1958, 80, 549-592.
14. E. Wiberg, H. Nöth, R. Usön, Z. Naturforsch., Part B 1956, 11, 490-491; T. L. Kolski, H. B. Moore, L. E. Roth, K. J. Martin, G. W. Schaeffer, J. Am. Chem. Soc. 1958, 80, 549-592.
15. N. M. Joseph, R. E. Paul, French Patent, 1077048 (1954); Chem. Abstr. 1959, 53, 10681.
16. D. S. Marynick, W. N. Lipscomb, Inorg. Chem. 1972, 11, 820.
17. C. S. Mayo, M. Brown, V. K. Loyd, Acta Crystallogr., Sect. C 1994, 50, 367-369; J. E. Gozum, S. R. Wilson, G. S. Girolani, J. Am. Chem. Soc. 1992, 114, 4483-9492.
18. C. S. Mayo, M. Brown, V. K. Loyd, Acta Crystallogr., Sect. C 1994, 50, 367-369; J. E. Gozum, S. R. Wilson, G. S. Girolani, J. Am. Chem. Soc. 1992, 114, 4483-9492.
19. M. Dionne, S. Hao, S. Gambarotta, Can. J. Chem. 1995, 73, 1126.
20. D. R. Armstrong, W. Clegg, H. M. Colquhoun, J. A. Danils, R. E. Mulvey, I. R. Stephenson, K. Wade, J. Chem. Soc., Chem. Comm. 1987, 630-631.
21. H. Nöth, M. Thomann, M. Bremer, G. Wagner, Current Topics in the Chemistry of Boron, Royal Soc. Chem. Special Publ. No. 143, 1994, p. 387-391.
22. K. B. Harvey, N. R. M. Quaker, Can. J. Chem. 1971, 49, 3272-3281; V. V. Volkov, E. V. Sobolev, Z. A. Grankina, I. S. Kalina, Zh. Neorg. Khim, 1968, 13, 659-664.
23. K. B. Harvey, N. R. M. Quaker, Can. J. Chem. 1971, 49, 3272-3281; V. V. Volkov, E. V. Sobolev, Z. A. Grankina, I. S. Kalina, Zh. Neorg. Khim, 1968, 13, 659-664.
24. D. E. Young, G. E. McAchran, S. G. Shore, J. Am. Chem. Soc. 1966, 88, 4390.
25. A. Heine, D. Stalke, J. Organomet. Chem. 1997, 542, 25-28, have independently determined the structure of 1 in the solid state. Therefore, we restrict the discussion of the structure to some essentials necessary to compare 1 with the structure of 2.
26. H. Edelstein, Inorg. Chem. 1981, 20, 299-303.
27. 3], and others will be published soon.
28. H. Nöth, A. Schlegel, J. Knizek, H. Schwenk, Angew. Chem. 1997, 109, 2754-2758; Angew. Chem. Int. Ed. Engl. 1997, 36, 2640-2643.
29. H. Nöth, A. Schlegel, J. Knizek, H. Schwenk, Angew. Chem. 1997, 109, 2754-2758; Angew. Chem. Int. Ed. Engl. 1997, 36, 2640-2643.
30. Siemens Analytical Instrum. Div., SAINT, Version 4.
31. SHELX-93 programs; G. W. Sheldrick, University of Göttingen, 1993, and SHELXTL, Siemens Analytical Instruments, version 5, 1994.
32. SHELX-93 programs; G. W. Sheldrick, University of Göttingen, 1993, and SHELXTL, Siemens Analytical Instruments, version 5, 1994.