Structural investigations of three triazines: Solution-state NMR studies of internal rotation and structural information from solid-state NMR, plus a full structure determination from powder x-ray diffraction in one case

Magnetic Resonance in Chemistry

Volumn 41, Issue 5, 2003, Pages 324-336

  Birkett, Helen E ^a   Cherryman, Julian C ^b   Chippendale, A Margaret ^b   Evans, John S O ^a   Harris, Robin K ^a   James, Mark ^b   King, Ian J ^a   McPherson, Graham J ^b  

^a DURHAM UNIVERSITY   (United Kingdom)

^b Avecia Biologics Limited   (United Kingdom)

Author keywords

13C NMR; 15N NMR; 1H NMR; Conformation; Magic angle spinning; NMR; Powder XRD; Rotamers; Structure solution; Triazines

Indexed keywords

CHEMICAL SHIFT; CRYSTAL STRUCTURE; HYDROGEN BONDS; LIGHT POLARIZATION; MOLECULES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SIMULATED ANNEALING; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION;

13C NMR; 15N NMR; 1H NMR; INTERNAL ROTATIONS; MAGIC-ANGLE SPINNING; POWDER XRD; POWDERS X-RAY DIFFRACTIONS; ROTAMERS; STRUCTURE SOLUTIONS; TRIAZINE;

MAGIC ANGLE SPINNING;

TRIAZINE DERIVATIVE;

AB INITIO CALCULATION; ANALYTIC METHOD; ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COMPARATIVE STUDY; CONFORMATION; CRYSTAL STRUCTURE; HYDROGEN BOND; MOLECULAR MODEL; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROTON NUCLEAR MAGNETIC RESONANCE; SOLID STATE; STRUCTURE ANALYSIS; SYNTHESIS; TEMPERATURE DEPENDENCE; X RAY POWDER DIFFRACTION;

EID: 0038375092     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1185     Document Type: Article

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