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Inoue, A.1
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7
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0037009038
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Kondo, Y.1
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Muraka, N.4
Sakamoto, T.5
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10
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0035073818
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Abarbri, M.1
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0037127088
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Quéguiner, G.6
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14
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0141437707
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note
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2,3,5-Triiodobenzoic acid is commercially available from Aldrich.
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15
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0033949367
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Millot, N.; Piazza, C.; Avolio, S.; Knochel, P. Synthesis 2000, 7, 941.
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(2000)
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Millot, N.1
Piazza, C.2
Avolio, S.3
Knochel, P.4
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16
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0027180369
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Lennick, K.2
Tucker, C.E.3
Knochel, P.4
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18
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0141549272
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note
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4, and concentrated in vacuo. Purification by flash chromatography (n-pentane/diethyl ether = 10:1) yielded 310 mg (70% yield) of 4e as a white solid, mp 76°C.
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20
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0012397313
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This effect has been extensively used to perform ortho-directed metalations: Snieckus, V. Chem. Rev. 1990, 90, 879.
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(1990)
Chem. Rev.
, vol.90
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Snieckus, V.1
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21
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0001494245
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Haddadin, M. J.; Agha, B. J.; Tabri, R. F. J. Org. Chem. 1979, 44, 494.
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Haddadin, M.J.1
Agha, B.J.2
Tabri, R.F.3
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22
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0141437706
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note
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4, and concentrated in vacuo. Purification by flash chromatography (n-pentane/diethyl ether = 2:1) yielded 295 mg (70%) of 6g as a colorless oil.
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