Templated assembly of sulfide nanoclusters into cubic-C3N4 type framework

Journal of the American Chemical Society

Volumn 125, Issue 20, 2003, Pages 6024-6025

  Bu, Xianhui ^a,b   Zheng, Nanfeng ^a   Li, Yuqi ^a   Feng, Pingyun ^a  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b Department of Chemistry ^*  (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CADMIUM; CARBON; COBALT; DIVALENT CATION; IRON; NANOPARTICLE; NITROGEN; SOLVENT; SULFIDE; ZINC ION;

ARTICLE; CHEMICAL STRUCTURE; MATERIALS; POROSITY; REACTION ANALYSIS; SEMICONDUCTOR; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0038288929     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja030103s     Document Type: Article

References (16)

1. Wehmschulte, R. J.; Power, P. P. J. Am. Chem. Soc. 1997, 119, 9566-9567.
2. Li, H.; Laine, A.; O'Keeffe, M.; Yaghi, O. M. Science 1999, 283, 1145-1147.
3. Li, H.; Kim, J.; Groy, T. L.; O'Keeffe, M.; Yaghi, O. M. J. Am. Chem. Soc. 2001, 123, 4867-6868.
4. Bedard, R. L.; Wilson, S. T.; Vail, L. D.; Bennett, J. M.; Flanigen, E. M. In Zeolites: Facts, Figures, Future. Proceedings of the 8th International Zeolite Conference; Jacobs. P. A., van Santen, R. A., Eds.: Elsevier: Amsterdam, 1989; p 375.
5. Scott, R. W. J.; MacLachlan, M. J.; Ozin, G. A. Curr. Opin. Solid State Mater. Sci. 1999, 4, 113-121.
6. Cahill, C. L.; Ko, Y.; Parise, J. B. Chem. Mater. 1998, 10, 19-21.
7. Cahill, C. L.; Parise, J. B. J. Chem. Soc., Dalton Trans. 2000, 1475-1482.
8. Bu, X.; Zheng, N.; Li, Y.; Feng, P. J. Am. Chem. Soc. 2002, 124, 12646-12647.
9. Zheng, N.; Bu, X.; Feng, P. J. Am. Chem. Soc. 2003, 125, 1138-1139.
10. Wang, C.; Li, Y.; Bu, X.; Zheng, N.; Zivkovic, O.; Yang, C.; Feng, P. J. Am. Chem. Soc. 2001, 123, 11506-11507.
11. Zheng, N.; Bu, X.; Wang, B.; Feng, P. Science 2002, 298, 2366-2369.
12. 2O (125.5 mg), di-n-butylamine (2.1036 g), and ethyleneglycol (4.2520 g) were mixed in a 23 mL Teflon-lined stainless steel autoclave and stirred for about 20 min. The vessel was then sealed and heated at 150 °C for 6 d. The autoclave was subsequently allowed to cool to room temperature. Clear tetrahedral crystals were obtained with an approximate yield of 36%.
13. Teter, D.; Hemley, R. J. Science 1996, 271, 53-55.
14. O'Keeffe, M.; Hyde, B. G. Crystal Structures 1. Patterns and Symmetry; Mineralogical Society of America: Washington D.C., 1996.
15. Chen, B.; Eddaoudi, M.; Hyde, S. T.; O'Keeffe, M.; Yaghi, O. M. Science 2001, 291, 1021-1023.
16. Spek, A. L. Acta Crystallogr. 1990, A46, C34.