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1
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0000331770
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-
as reviewed in: Efraty, A.
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(a) Work by Criegee, R. et al., as reviewed in: Efraty, A. Chem. Rev. 1977, 77, 691.
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(1977)
Chem. Rev.
, vol.77
, pp. 691
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Criegee, R.1
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2
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0013537489
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(b) Maitlis, P. M.; Efraty, A.; Games, M. L. J. Am. Chem. Soc. 1965, 87, 719.
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(1965)
J. Am. Chem. Soc.
, vol.87
, pp. 719
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-
Maitlis, P.M.1
Efraty, A.2
Games, M.L.3
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3
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51149209880
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(a) Crocker, M.; Green, M.; Orpen, A. G.; Neumann, H.-P.; Schaverien, C. J. J. Chem. Soc., Chem. Commun. 1984, 1351.
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(1984)
J. Chem. Soc., Chem. Commun.
, pp. 1351
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-
Crocker, M.1
Green, M.2
Orpen, A.G.3
Neumann, H.-P.4
Schaverien, C.J.5
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4
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-
0000883171
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(b) Crocker, M.; Green, M.; Nagle, K. R.; Orpen, A. G.; Neumann, H.-P.; Morton, C. E.; Schaverien, C. J. Organometallics 1990, 9, 1422.
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(1990)
Organometallics
, vol.9
, pp. 1422
-
-
Crocker, M.1
Green, M.2
Nagle, K.R.3
Orpen, A.G.4
Neumann, H.-P.5
Morton, C.E.6
Schaverien, C.J.7
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5
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-
0038158125
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-
(a) Rüba, E.; Mereiter, K.; Schmid, R.; Kirchner, K.; Bustelo, E.; Puerta, M. C.; Valerga, P. Organometallics 2002, 21, 2912.
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(2002)
Organometallics
, vol.21
, pp. 2912
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-
Rüba, E.1
Mereiter, K.2
Schmid, R.3
Kirchner, K.4
Bustelo, E.5
Puerta, M.C.6
Valerga, P.7
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6
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-
37049089839
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(b) Brammer, L.; Crocker, M.; Dunne, B. J.; Green, M.; Morton, C. E.; Nagle, K. R.; Orpen, A. G. J. Chem. Soc., Chem. Commun. 1986, 1226.
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(1986)
J. Chem. Soc., Chem. Commun.
, pp. 1226
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-
Brammer, L.1
Crocker, M.2
Dunne, B.J.3
Green, M.4
Morton, C.E.5
Nagle, K.R.6
Orpen, A.G.7
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7
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0002504356
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note
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2 and TlCp in THF: Koelle, U. Inorg. Chim. Acta 1981, 47, 13. For an alternative that avoids the use of TlCp see ref 5.
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(1981)
Inorg. Chim. Acta
, vol.47
, pp. 13
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Koelle, U.1
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8
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0038620034
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note
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2O) with hexane as eluent, and crystallization from methanol at -80 °C afforded 1 (2.22 g, 95%) as a spectroscopically pure, brownish yellow, crystalline solid.
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-
-
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9
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37049084186
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(a) Cook, M. R.; Härter, P.; Pauson, P. L.; Šraga, J. J. Chem. Soc., Dalton Trans. 1987, 2757.
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(1987)
J. Chem. Soc., Dalton Trans.
, pp. 2757
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Cook, M.R.1
Härter, P.2
Pauson, P.L.3
Šraga, J.4
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11
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0036787482
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(c) Butovskii, M. V.; Englert, U.; Fil'chikov, A. A.; Herberich, G. E.; Koelle, U.; Kudinov, A. R. Eur. J. Inorg. Chem. 2002, 2656.
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(2002)
Eur. J. Inorg. Chem.
, pp. 2656
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Butovskii, M.V.1
Englert, U.2
Fil'chikov, A.A.3
Herberich, G.E.4
Koelle, U.5
Kudinov, A.R.6
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12
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0037943806
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note
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2): δ 11.70 (2-Me, HMBC, HETCOR), 23.54 (3-Me, HMBC, HETCOR), 28.64 (C-5, HETCOR), 30.96 (1-Me, HMBC, HETCOR), 85.40 (C-4, HETCOR), 88.24 (Cp, HETCOR), 100.86 (C-2, HMBC), 119.45 (C-3, HMBC), 292.11 (C-1). The atom numbering is in accordance with the name (2Z,3Z)-1,2,3-trimethylpenta-1,3-dienyl of the open-chain ligand.
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-
-
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13
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0037943805
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note
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2O mixture.
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-
-
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14
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0038620035
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note
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2)/3; non-hydrogen atoms were refined anisotropically, all hydrogen atoms were included as riding in idealized geometry. Further details of the crystal structure determinations are available on request from the Cambridge Crystallographic Data Centre, on quoting the depository number CCDC-204444.
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15
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0000049879
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(b) Coppens, P.; Leiserowitz, L.; Rabinovich, D. Acta Crystallogr. 1965, 18, 1035.
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(1965)
Acta Crystallogr.
, vol.18
, pp. 1035
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Coppens, P.1
Leiserowitz, L.2
Rabinovich, D.3
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16
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0004150157
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-
Program for Crystal Structure Solution; University of Göttingen
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(c) Sheldrick, G. M. SHELXS97, Program for Crystal Structure Solution; University of Göttingen, 1997.
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(1997)
SHELXS97
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Sheldrick, G.M.1
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17
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0004150157
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Program for Crystal Structure Refinement; University of Göttingen
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(d) Sheldrick, G. M. SHELXL97, Program for Crystal Structure Refinement; University of Göttingen, 1997.
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(1997)
SHELXL97
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Sheldrick, G.M.1
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19
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0038620036
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note
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2): δ 17.31 (4-Me, HMBC, HETCOR), 19.60 [Me(C-6), HETCOR], 22.38 (3-Me, HMBC, HETCOR), 58.53 (C-1, HETCOR), 81.47 (C-5, HETCOR), 88.63 (Cp, HETCOR), 93.40 (C-2, HETCOR), 109.53 (C-4, HMBC), 113.75 (C-3, HMBC). The atom numbering is in accordance with the name (2Z,3Z,4E)-3,4-dimethylhexa-2,4-dienyl for the open-chain ligand.
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-
-
-
20
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33845378924
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For carbene to olefin conversions see: (a) Casey, C. P.; Miles, W. H.; Tukada, H. J. Am. Chem. Soc. 1985, 107, 2924.
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(1985)
J. Am. Chem. Soc.
, vol.107
, pp. 2924
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-
Casey, C.P.1
Miles, W.H.2
Tukada, H.3
-
23
-
-
0037605727
-
-
note
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2): δ 14.80 (3-/-4-Me, HETCOR), 19.10 (C-1,6, HETCOR), 45.75 (C-2,5, HETCOR), 81.83 (Cp, HETCOR), 88.98 (C-3,4, HETCOR).
-
-
-
-
24
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0037943808
-
-
note
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4 as hydride source produces a mixture of isomers and is also accompanied by reductive decomposition.
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