Large scale synthesis of 4′-(4-bromophenyl)-2,2′:6′,2″-terpyridine and nature of the mysterious green by-product

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Volumn 58, Issue 5, 2003, Pages 443-446

  Siemeling, Ulrich ^a   Der Brüggen, Jens Vor ^a   Vorfeld, Udo ^a   Stammler, Anja ^b   Stammler, Hans Georg ^b  

^a UNIVERSITY OF KASSEL   (Germany)

^b BIELEFELD UNIVERSITY   (Germany)

Author keywords

Indolizinium Compounds; Rigid Rod Molecules; X Ray Data

Indexed keywords

CHEMISTRY;

4-METHYLPHENYL; HEXAFLUOROPHOSPHATES; INDOLIZINIUM COMPOUNDS; LARGE SCALE SYNTHESIS; PYRIDINIUM IODIDE; RIGID RODS; TERPYRIDINES; X RAY DATA;

CRYSTAL STRUCTURE;

1 [3 (4 BROMOPHENYL)INDOLIZIN 1 YL 1 IMINO] 3 (4 BROMOPHENYL) 1H INDOLIZINIUM IODIDE; 1 [3 (4 METHYLPHENYL)INDOLIZIN 1 YL 1 IMINO] 3 (4 METHYLPHENYL) 1H INDOLIZINIUM HEXAFLUOROPHOSPHATE; 2 [3 (4 BROMOPHENYL) 1 OXOPROP 2 ENYL]PYRIDINE; 4' (4 BROMOPHENYL) 2,2':6',2'' TERPYRIDINE; INDOLIZINE DERIVATIVE; IODINE DERIVATIVE; N [2 OXO 2 (2 PYRIDYL)ETHYL]PYRIDINIUM IODIDE; PYRIDINE DERIVATIVE; PYRIDINIUM DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CRYSTAL STRUCTURE; STOICHIOMETRY; SYNTHESIS;

EID: 0038204356     PISSN: 09320776     EISSN: None     Source Type: Journal    
DOI: 10.1515/znb-2003-0514     Document Type: Article

References (8)

1. W. Spahni, G. Calzaferri, Helv. Chim. Acta 67, 450 (1984).
2. F. Kröhnke, Synthesis 1 (1976).
3. P. Korall, A. Börje, P.-O. Norrby, B. Åkermark, Acta Chem. Scand. 51, 760 (1997).
4. F.W. Kröck, F. Kröhnke, Chem. Ber. 104, 1645 (1971).
5. D. A. Maiboroda, E. V. Babaev, K. Jug, J. Org. Chem. 62, 7100 (1997).
6. T. L. Gilchrist, Heterocyclenchemie, p. 16, VCH, Weinheim (1995).
7. C. Mikel, P. G. Potvin, Inorg. Chim. Acta 325, 1 (2001).
8. G. U. Priimov, P. Moore, P. K. Maritim, P. K. Butalanyi, N. W. Alcock, J. Chem. Soc., Dalton Trans. 445 (2000).