Reaction of benzoquinones and naphthoquinones with 1,8-diamino-3,6-dioxanonane and with 1,11-diamino-3,6,9-trioxaundecane

Tetrahedron Letters

Volumn 44, Issue 29, 2003, Pages 5531-5534

  Machocho, Alex K ^a   Win, Thida ^b   Grinberg, Sarina ^c   Bittner, Shmuel ^c  

^a KENYATTA UNIVERSITY   (Kenya)

^b University of Mandalay   (Myanmar)

^c BEN GURION UNIVERSITY OF THE NEGEV   (Israel)

Author keywords

Bis quinonylamines; Crown ethers; Polyoxyethylenediamines; Quinones

Indexed keywords

1,11 DIAMINO 3,6,9 TRIOXAUNDECANE; 1,4 BENZOQUINONE; 1,4 NAPHTHOQUINONE DERIVATIVE; 1,8 DIAMINO 3,6 DIOXANONANE; 2,3 DICHLORO 1,4 NAPHTHOQUINONE; AMINE; BENZOQUINONE DERIVATIVE; BROMANIL; CHEMICAL COMPOUND; CHLORANIL; CROWN ETHER DERIVATIVE; DIAMINE DERIVATIVE; DICHLORODICYANOBENZOQUINONE; S PHENYLBENZOQUINONE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; SYNTHESIS;

EID: 0038200793     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(03)01263-2     Document Type: Article

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15. -1. Crystal dimensions 0.32×0.35×0.78 mm. Data were measured at 295 K on a standard Bruker SMART 6K CCD diffractometer [l(Mo Kα)]=0.711069 Å, graphite monochromator. The structure was solved by direct methods and refined by least-squares in full-matrix approximation. Hydrogen atoms were placed to the calculated positions and were refined using the 'riding model' SHELXTL [Bruker AXS, 1998] software package for calculations and drawing. Atomic coordinates, bond lengths and angles, and thermal parameters have been deposited at the Cambridge Crystallographic Data Centre.
16. -1. Crystal dimensions 0.64×0.44×0.32 mm. Data were measured at 295 K on a standard Bruker SMART 6K CCD diffractometer with graphite monochromated Mo Kα radiation. The structure was solved by direct methods and refined by least-squares in full-matrix approximation. Hydrogen atoms were placed to the calculated positions and were refined using the 'riding model' SHELXTL [Bruker AXS, 1998] software package for calculations and drawing. Atomic coordinates, bond lengths and angles, and thermal parameters have been deposited at the Cambridge Crystallographic Data Centre.
17. Crystallographic data (excluding structure factors) for the structures in this paper, have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication numbers CCDC 203258 and 203259. Copies of the data can be obtained, free of charge, on application to CCDC, 12 Union Road, Cambridge CB2 1EZ UK (Fax: +44(0)-1223-336033 or e-mail: deposit@ccdc.cam.ac.uk).