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Volumn 4, Issue 4, 2002, Pages 663-666

Unprecedented microwave effects on the cycloaddition of fulvenes. A new approach to the construction of polycyclic ring systems

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ARTICLE;

EID: 0038166544     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol017304q     Document Type: Article
Times cited : (62)

References (31)
  • 15
    • 0043255510 scopus 로고    scopus 로고
    • note
    • Focused microwave irradiation was carried out at atmospheric pressure with a Synthewave S402 Prolabo microwave reactor (300 W, monomode system, 10 mL reactors). The apparatus has a quartz reactor, visual control, PC-controlled 300 W irradiation, and infrared temperature measurement with continuous feedback control.
  • 16
    • 0043255491 scopus 로고    scopus 로고
    • note
    • f = 0.32 in 15% EtOAc-hexane) to give the adducts 1 and 2 as colorless liquids (1: 328 mg. 32% yield; 2: 341 mg, 33% yield).
  • 17
    • 0042754338 scopus 로고
    • 2,6]undecane structure, fulvene dimer, was proposed as the first step ([6+4]-dimerization) in the trimerization of 6,6-dimethyl fulvene; see: Uebersax, M.; Neuenschwander, M.; Engel, P. Helv. Chim. Acta 1982, 65, 89-104.
    • (1982) Helv. Chim. Acta , vol.65 , pp. 89-104
    • Uebersax, M.1    Neuenschwander, M.2    Engel, P.3
  • 28
    • 0034700812 scopus 로고    scopus 로고
    • This indene skeleton is widespread among natural products; for example see: (a) for amaminol A and B: Sata, N.; Noriko, U.; Fusetani, N. Tetrahedron Lett. 2000, 41, 489-492.
    • (2000) Tetrahedron Lett. , vol.41 , pp. 489-492
    • Sata, N.1    Noriko, U.2    Fusetani, N.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.