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85039655972
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note
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The alkoxide showed an exclusive syn-selectivity in dialkylation of 1 in THF, giving 3a-c in 90, 67 and 52% yields, respectively.
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15
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85039656004
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note
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3) δ 31.2, 31.3, 32.4, 33.6, 33.9, 35.9, 39.5, 72.1, 124.4, 125.1, 125.3, 125.6, 126.2, 126.6, 127.3, 127.8, 128.5, 132.1, 133.7, 136.3, 142.7, 147.1, 149.1, 151.5.
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16
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33751498991
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C. Jaime, J. De Mendoza, P. Parados, P. M. Nieto, and C. Sanchez, J. Org. Chem., 56, 3372 (1991).
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Jaime, C.1
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17
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0032857803
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Kuwahara, S.1
Fujita, K.2
Watanabe, M.3
Harada, N.4
Ishida, T.5
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