Determination of formaldehyde in cosmetics by HPLC method and acetylacetone method

Journal of Food and Drug Analysis

Volumn 11, Issue 1, 2003, Pages 8-15

  Wu, Pai Wen ^a   Chang, Chieu Chen ^a   Chou, Shin Shou ^a  

^a DEPARTMENT OF HEALTH   (Taiwan)

Author keywords

Acetylacetone; Cosmetics; Formaldehyde; Formaldehyde donor; HPLC

Indexed keywords

2,4 DINITROPHENYLHYDRAZINE; ACETONITRILE; ACETYLACETONE; COSMETIC; FORMALDEHYDE;

ANALYTIC METHOD; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL PROCEDURES; CHEMICAL REACTION; COLORIMETRY; CONTROLLED STUDY; COSMETIC INDUSTRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SAMPLING;

EID: 0038134866     PISSN: 10219498     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (25)

1. Cosmetic Ingredient Review. 1984. Final report on the safety assessment of formaldehyde. Journal of the American college of the Toxicology. 157-184.
2. Department of Health, Executive Yuan. 1985. Ordinance No. 539747. July. 23, 1985. Taipei. (in Chinese)
3. Goldemberg, R. L. 1994. International cosmetics: How regulatory practices create formulating problems (Part II). DCI. (March): 48-55.
4. Steinberg, D. C. 1992. Cosmetic Preservations: Current International Trends. Cosmetics & Toiletries. 107:77-82.
5. Mufti, J., Cernasov, D., and Macchio, R. 2001. Preserving personal care and household products. Happi. May: 69-80.
6. Ministry of Health, Labour and Welfare. 1995. Ordinance No. 1747. Oct. 9. 1995. Tokyo. Japan. (in Japanese)
7. Department of Health, Executive Yuan. 1998. Ordinance No. 87041266. July. 7, 1998. Taipei. (in Chinese)
8. Commission of European Communities (CEC). 1975. Determination of free formaldehyde. Panel on the analysis of cosmetic products. Doc. XI/650/75-E.
9. Lien, D. H. 1977. Analysis of antimicrobial compounds in cosmetics. Cosmetics and Toiletries. 92 (3): 59-72.
10. Hseigh, P. S. 1984. Analysis of formaldehyde. Methods of Analysis for Hygienic Chemistry with Commentary. Kung-Shuei-Shur Publishing Co., Ltd. Tainan (in Chinese). 134-138.
11. Fransway, A. 1991. The problem of preservation in 1990s: I. Statement of the problem, solution(s) of industry, and the current use of formaldehyde and formaldehyde-releasing biocides. American Journal of Contact Dermatitis. 2(1): 6-23.
12. Gryllaki-Berger, M., Mugny, C., Perrenoud, D., Pannatier, A. and Frenk, E. 1992. A comparative study of formaldehyde detection using chromotropic acid, acetylacetone and HPLC in cosmetics and household cleaning products. Contact Dermatitis. 26:149-154.
13. Benassi, C. A., Semenzato, A. and Bettero, A. 1989. High performance liquid chromatographic determination of free formaldehyde in cosmetics. Journal of Chromatography. (464): 387-393.
14. European Economic community (EEC). 1990. IV. Identification and determination of free formaldehyde. Official Journal of the European Communities. No L 108/93.
15. Pharmaceutical Society of Japan. 1996. Formaldehyde analysis of cosmetics. Standard Methods of Analysis for Hygienic Chemistry with Commentary. Kanehara Publishing Co., Ltd. Tokyo. Japan. Ya-Lung Publishing Co., Ltd. Taipei. (in Chinese)
16. Bureau of Standards, Metrology and Inspection, Ministry of Economics Affairs. 1999. Methods of test for free formaldehyde analysis in cosmetics. CNS 9538, S 2084. Taipei. (in Chinese)
17. Michels, J. J. 2001. Improved measurement of formaldehyde in water-soluble polymers by high-performance liquid chromatography coupled with post-column reaction detection. Journal of chromatography A, 914:123-129.
18. Vanhees, I., Van den Bergh, V., Schilderman, R., De Boer, R., Compernolle, F. and Vinckier, C. 2001. Determination of the oxidation product of the reaction between a-pinene and hydroxyl radicals by high-performance liquid chromatography. Journal of chromatography A, 915:75-83.
19. Engelhardt, H. and Klinkner, R. 1985. Determination of free formaldehyde in the presence of donators in cosmetics by HPLC and post-column derivation. Chromatographia. 20:559-565.
20. Hurley, F. 1994. Information of formaldehyde releasers. Working Report of Food and Drug Administration, September 26.
21. Benassi, C. A., Semenzato, A., Zaccaria, F. and Bettero, A. 1990. High performance liquid chromatographic determination of free formaldehyde in cosmetics preserved with Dowicil 200. Journal of Chromatography. 502: 193-200.
22. Berke, P. A., and Rosen, W. E. 1982. Germall II- A new broad spectrum cosmetic preservative. Cosmetics & Toiletries. 97(6), 49-53.
23. Rosen, M., and Mcfarland, A. D. 1984. Free formaldehyde in anionic shampoos. Journal of Society Cosmetic Chemistry. 35:157-69.
24. Rastogi, S. C. 1992. A survey of formaldehyde in shampoos and skin creams on the Danish market. Contact Dermatitis. 27: 235-240.
25. Summers, W. R. 1990. Characterization of formaldehyde and formaldehyde-releasing preservatives by combined reversed-phase cation-exchange high-performance liquid chromatography with postcolumn derivation using nash's reagent. Anal. Chem. 62:1397-1402.