An efficient separation method for enol phosphate and corresponding β-ketophosphonate from their mixtures under aqueous conditions

Synthetic Communications

Volumn 33, Issue 12, 2003, Pages 2069-2086

  Moorhoff, Cornelis M ^a  

^a UNIVERSITY OF TASMANIA   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

1 [(DIETHOXYPHOSPHINYL)OXO]STYRENE; 2 (DIETHOXYPHOSPHINYL)ACETOPHENONE; ACETOPHENONE DERIVATIVE; DICHLOROMETHANE; STYRENE DERIVATIVE; UNCLASSIFIED DRUG;

ACIDIFICATION; ANALYTIC METHOD; AQUEOUS SOLUTION; ARBUZOV REACTION; ARTICLE; DERIVATIZATION; DRUG MIXTURE; PHASE SEPARATION; REACTION ANALYSIS;

EID: 0038053024     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1081/SCC-120021033     Document Type: Article

References (20)

1. Battacharya, A.K.; Thyagaran, G. Chem. Rev. 1981, 81, 415.
2. Moorhoff, C.M.; Grosse, A.C. Heteroatom Chemistry 1997, 8, 361. And references cited.
3. Yuan, C.; Xie, R. Phosphorus, Sulfur, Silicon, Relat. Elem. 1994, 90, 47.
4. Kim, D.Y.; Kong, M.S.; Rhie, D.Y. Synth. Commun. 1995, 25, 2865. And references cited.
5. Kim, D.Y.; Kong, M.S.; Kim, T.H. Synth. Commun. 1996, 26, 2487. And references cited.
6. Corbel, B.; L'Hostis-Kervella, I.; Haelters, J.-P. Synth. Commun. 1996, 26, 2561.
7. Fouqué, D.; About-Jaudet, E.; Collignon, N. Synth. Commun. 1992, 22, 219.
8. Borowitz, I.J.; Anschel, M.; Firstenberg, S. J. Org. Chem. 1967, 32, 1723.
9. Bianchini, J.P.; Gaydou, E.M. Hebd. Seances Acad. Sci. Ser. C 1975, 280 (25), 1521.
10. Belcuig, M.P.; Modro, A.M.; Modro, T.A.; Wessels, P.L. J. Phys. Org. Chem. 1992, 5, 787.
11. Jagodic, V. Croat. Chem. Acta 1977, 49, 487.
12. Moorhoff, C.M.; Schneider, D.F. Tetrahedron Lett. 1987, 28, 559.
13. DuPisani, C.; Schneider, D.F.; Venter, P.C.R. Synth. Commun. 2002, 32, 305.
14. Moorhoff, C.M. Ph.D. thesis, Stellenbosch 1986. Unpublished results.
15. Pudovik, A.N.; Avery'anova, V.P. Zhur Obschei Khim. 1956, 26, 1426.
16. Lichtenthaler, F.W. Chem. Ber. 1961, 61, 607.
17. Öhler, E.; Kang, H.-S.; Zbiral, E. Synthesis 1988, 9, 623.
18. Tavares, D.F.; O'Sullivan, W.I.; Hauser, C.R. J. Org. Chem. 1962, 27, 1251.
19. Duthaler, R.O. Helv. Chim. Acta 1983, 66, 1475.
20. Sakamoto, M.; Fukuda, Y.; Kamiyama, T.; Kawasaki, T. Chem. Pharm. Bull. 1994, 42, 1919.