Ligand exchange reactions of ReCl4(PPh3)2, ReOCl3(PPh3)2 and NiCl2(PPh3)2 with acetylacetone thiobenzoylhydrazone. An unexpected template reaction at the ReO3+ core. Molecular structures of the resulting oxorhenium(V) and nickel complexes

Inorganica Chimica Acta

Volumn 277, Issue 2, 1998, Pages 219-224

  Sawusch, Stefan ^a   Schilde, Uwe ^a   Lehmann, Andreas ^b   Uhlemann, Erhard ^a  

^a UNIVERSITY OF POTSDAM   (Germany)

^b BAM FEDERAL INSTITUTE FOR MATERIALS RESEARCH AND TESTING   (Germany)

Author keywords

Crystal structures; Hydrazone complexes; Nickel complexes; Oxo complexes; Rhenium complexes

Indexed keywords

ACETONE; CRYSTAL STRUCTURE; CRYSTALS; LIGANDS; MASS SPECTROMETRY; RHENIUM COMPOUNDS; ULTRAVIOLET VISIBLE SPECTROSCOPY;

HYDRAZONE COMPLEXES; LIGAND EXCHANGE REACTIONS; NICKEL COMPLEX; OXO COMPLEXES; RHENIUM COMPLEXES; TEMPLATE REACTIONS; UV-VIS SPECTROSCOPY; X RAY STRUCTURAL ANALYSIS;

NICKEL COMPOUNDS;

EID: 0037841010     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(97)06154-9     Document Type: Article

References (28)

1. A. Müller, R. Jostes, E. Krickmeyer and H. Böge, Naturwissenschaften, 74 (1987) 388.
2. G. Battistuzzi, M. Borsari and R. Battisluzzi, Polyhedron, 16 (1997) 2093.
3. B.K. Dirghangi, M. Menon, A. Pramanik and A. Chakravorty, Inorg. Chem., 36 (1997) 1095.
4. E. Deutsch, K. Libson, J.-L. Vanderheyden, A.R. Ketring and H. Maxon, Nucl. Med. Biol., 13 (1986) 465.
5. W.A. Volkert, W.F. Goeckler, G.J. Ehrhard and A.R. Ketring, J. Nucl. Med., 32 (1991) 174.
6. E. Deutsch, K. Libson and J.-L. Vanderheyden, The inorganic chemistry of rhenium and technetium as related to nuclear medicine, in M. Nicolini, G. Bandoli and U. Mazzi (eds.), Proc. Int. Symp. Technetium in Chemistry and Nuclear Medicine, in Verona Cortina Int., 3 (1990) 13.
7. S. Sawusch, U. Schilde and E. Uhlemann, Z. Naturforsch., Teil B, 52 (1997) 61.
8. W. Banße, E. Ludwig, E. Uhlemann, F. Weller, K. Dehnicke and W. Herrmann, Z. Anorg. Allg. Chem., 613 (1992) 36.
9. W. Bansse, E. Ludwig, E. Uhlemann, H. Mehner, F. Weller and K. Dehnicke, Z. Anorg. Allg. Chem., 607 (1992) 177.
10. H. Hefele, H. Janke, S. Sawusch, U. Schilde and E. Uhlemann, Struct. Chem., 8 (3) (1997) 211.
11. S. Sawusch, U. Schilde, I. Slarke, A. Lehmann and E. Uhlemann, Inorg. Chim. Am, 268 (1998) 109.
12. G. Rouschias, Chem. Rev., 74 (1974) 542.
13. N.P. Johnson, C.J.L. Lock and G. Eilkinson, Inorg. Synth., 9 (1967) 145.
14. D.K. Johnson, T.B. Murphy, N.J. Rose, W.H. Goodwin and L. Pickart, Inorg. Chim. Acta, 67 (1982) 159.
15. X-RED Rev. 1.05 Data Reduction Program, Stoe+CIE, Darmstadt, 1995.
16. S. Parkin, B. Meozzi and H. Hope, XABS2: An empirical absorption correction program, J. Appl. Crystallogr., 28 (1995) 53.
17. G.M. Sheldrick, SHELXS-86, program for the solution of crystal structures, Göttingen, Germany, 1985.
18. G.M. Sheldrick, SHELXL-93, program for the crystal structure refinement, Göttingen, Germany, 1993.
19. International Tables for X-Ray Crystallography, Vol. 4, Kynoch, Birmingham, UK, 1974.
20. H.D. Flack, Acta Crystallogr., Sect. A, 39 (1983) 876.
21. G. Bandoli, M. Nicolini, U. Mazzi, F. Refosco and F. Tisato, J. Chem. Soc., Dalton Trans., (1986) 1623.
22. M. Lipowska, B.L. Hayes, L. Hansen, A. Taylor and L.G. Marzilli, Inorg. Chem., 35 (1996) 4227.
23. S. Jurisson, E.O. Schlemper, D.E. Troutner, L.R. Canning, D.P. Nowotnik and R.D. Neirinchx, Inorg. Chem., 25 (1986) 543.
24. D.Y. Chi, S.R. Wilson and J.A. Katzenellenbogen, Inorg. Chem., 34 (1995) 1624.
25. F. Tisato, U. Mazzi, G. Bandoli, G. Cros, M.H. Darbieu, Y. Coulais and R. Guiraud, J. Chem. Soc., Dalton Trans., (1991) 1301.
26. H. Alarabi, R.A. Bell, H.E. Howardlock, J. Kowanetz and C.J.L. Lock, Can. J. Chem., 74 (1996) 554.
27. T.W. Jackson, M. Kojima, R.M. Lambrecht, D.C. Craig and A.D. Rae, Aust. J. Chem., 74 (1996) 239.
28. M.T. Toshev, V.G. Yusupov, S.O. Saidov, Z.T. Karimov, Kh.B. Dustov, M.M. Karimov, K.N. Zelenin and N.A. Parpiev, Koord. Khim., 18 (1992) 974, Engl. edn. (842).