Synthesis of new oxy and thiolate [hydro-tris(pyrazol-1-yl)borato] titanium and zirconium(IV) complexes. Molecular structure of [Ti(HB(3,5-Me2pz)3)Cl3]

Journal of Organometallic Chemistry

Volumn 577, Issue 2, 1999, Pages 174-180

  Antinolo A ^a   Carrillo Hermosilla, F ^a   Corrochano, A E ^a   Fernandez Baeza J ^a   Lanfranchi, M ^b   Otero, A ^a   Pellinghelli, M A ^b  

^a UNIVERSITY OF CASTILLA LA MANCHA   (Spain)

^b UNIVERSITY OF PARMA   (Italy)

Author keywords

Dynamic behavior; Pyrazolylborates; Pyridine; Pyrimidine; Titanium; Zirconium

Indexed keywords

OXY;

EID: 0037808750     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(98)01015-8     Document Type: Article

References (23)

1. (a) S. Trofimenko, Acc. Chem. Res. 4 (1971) 17.
2. (b) S. Trofimenko, Chem. Rev. 72 (1972) 497.
3. (c) S. Trofimenko, Chem. Rev. 93 (1993) 943.
4. (a) J.K. Kouba, S.S. Wreford, Inorg. Chem. 15 (1976) 2313.
5. (b) D.L. Reger, M.E. Tarquini, Inorg. Chem. 21 (1982) 840.
6. (a) D.L. Reger, M.E. Tarquini, Inorg. Chem. 22 (1983) 1064.
7. (b) D.L. Reger, M.E. Tarquini, L. Lebloda, Organometallics 2 (1983) 1763.
8. (c) R.A. Kresinski, T.A. Hamor, L. Isam, C.J. Jones, J.A. McCleverty, Polyhedron 8 (1989) 845.
9. (d) R.A. Kresinski, C.J. Jones, J.A. McCleverty, Polyhedron 9 (1990) 2185.
10. (e) R.A. Kresinski, T.A. Hamor, C.J. Jones, J.A. McCleverty, J. Chem. Soc. Dalton Trans. (1991) 603.
11. (f) R.A. Kresinski, T.A. Hamor, C.J. Jones, J.A. McCleverty, J. Chem. Soc. Dalton Trans. (1991) 1835.
12. (g) J. Ipaktschi, W. Sulzbach, J. Organomet. Chem. 426 (1992) 59.
13. Dunn S.C., Mountford P., Shishkin O.V. Inorg. Chem. 35:1996;1006.
14. Fandos R., Lanfranchi M., Otero A., Pellinghelli M.A., Ruiz M.J., Terreros P. Organometallics. 15:1996;4725.
15. LeCloux D.D., Keyes M.C., Osawa M., Reynolds V., Tolman W.B. Inorg. Chem. 33:1994;6361.
16. D.L. Hughes, G.J. Leigh, D.G. Walker, J. Chem. Soc. Dalton Trans. (1988) 1153.
17. Sandström J. Dynamic NMR Spectroscopy. 1982;Academic Press, New York.
18. Lehmann M.S., Larsen F.K. Acta Crystallogr. Sect. A. 30:1974;580.
19. Altomare A., Cascarano G., Giacovazzo C., Gualiardi A., Burla M.C., Polidori G., Camalli M. J. Appl. Crystallogr. 27:1994;435.
20. G.M. Sheldrick, SHELX-76 program for crystal structure determination, University of Cambridge, England, 1976.
21. International Tables for X-ray Crystallography, vol. IV, Kynoch Press, Birmingham, England, 1974.
22. Nardelli M. Comput. Chem. 7:1983;95.
23. C.K. Johnson ORTEP. Report ORNL-3794, revised, Oak Ridge National Laboratory, Oak Ridge, TN, 1965.