The reactions of M[BF4] (M = LI, K) and (C2H5)2O·BF3 with (CH3)3SiCN. Formation of m[BFx(CN)4-x] (M = Li, K; x = 1, 2) and (CH3)3SiNCBFx(CN)3-x, (x = 0, 1);Die reaktionen von M[BF4] (M = LI, K) und (C2H5)2O·BF3 mit (CH3)3SiCN. Bildung von M[BFx(CN)4-x] (M = Li, K; x = 1, 2) und (CH3)3SiNCBFx(CN)3-x, (x = 0, 1)

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 629, Issue 4, 2003, Pages 677-685

  Bernhardt, Eduard ^a,c   Berkei, Michael ^a   Willner, Helge ^a,c   Schürmann, Markus ^a,b  

^a Fachgebiet Anorganische Chemie der Universitt   (Germany)

^b TU DORTMUND UNIVERSITY   (Germany)

^c UNIVERSITY OF DUISBURG ESSEN   (Germany)

Author keywords

Cyanoborates; Structure elucidation; Vibrational spectroscopy

Indexed keywords

LITHIUM DERIVATIVE; POTASSIUM DERIVATIVE; SILICON DERIVATIVE;

ARTICLE; CHEMICAL REACTION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION TIME; SYNTHESIS; TEMPERATURE; X RAY DIFFRACTION;

EID: 0037740994     PISSN: 00442313     EISSN: None     Source Type: Journal    
DOI: 10.1002/zaac.200390115     Document Type: Article

References (17)

1. E. Bernhardt, G. Henkel, H. Willner, Z. Anorg. Allg. Chem. 2000, 626, 560.
2. D. Williams, B. Pleune, J. Kouvetakis, M. D. Williams, R. A. Andersen, J. Am. Chem. Soc. 2000, 122, 7735.
3. J. K. Rasmussen, S. M. Heilmann, L. R. Krepski, Adv. Silicon Chem. 1991, 1, 65.
4. E. C. Evers, W. O. Freitag, W. A. Kriner, A. G. MacDiarmid, S. Sujshi, J. Inorg. Nucl. Chem. 1960, 13, 239.
5. E. C. Evers, W. O. Freitag, J. N. Keith, W. A. Kriner, A. G. MacDiarmid, S. Sujshi, J. Am. Chem. Soc. 1959, 81, 4493.
6. E. C. Evers, W. O. Freitag, W. A. Kriner, A. G. MacDiarmid, J. Am. Chem. Soc. 1959, 81, 5106.
7. E. Bessler, J. Goubeau, Z. Anorg. Allg. Chem. 1967, 362, 67.
8. E. Bernhardt, G. Henkel, H. Willner, G. Pawelke, H. Bürger, Chem. Eur. J. 2001, 7, 4696.
9. J. A. Seckar, J. S. Thayer, Inorg. Chem. 1976, 15, 501.
10. P. D. Blair, A. J. Blake, R. W. Cockman, S. Cradock, E. A. V. Ebsworth, D. W. H. Rankin, J. Mol. Struct. 1989, 193, 279.
11. S. Brownstein, G. Latremouille, Can. J. Chem. 1978, 56, 2764.
12. E. Bernhardt, M. Berkei, G. Henkel, H. Willner, in Vorbereitung.
13. Z. Otwinowsky, W Minor, Methods in Enzymology 1997, 276, 307.
14. G. M. Sheldrick, Acta Crystallogr. 1990, A46, 467.
15. G. M. Sheldrick, Univ. Göttingen, 1997.
16. M. R. Booth, S. G. Frankiss, Spectrochim. Acta 1970, 26A, 859.
17. M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, V. G. Zakrzewski, J. A. Montgomery, R. E. Stratmann, J. C. Burant, S. Dapprich, J. M. Millam, A. D. Daniels, K. N. Kudin, M. C. Strain, O. Farkas, J. Tomasi, V. Barone, M. Cossi, R. Cammi, B. Mennucci, C. Pomelli, C. Adamo, S. Clifford, J. Ochterski, G. A. Petersson, P. Y. Ayala, Q. Cui, K. Morokuma, D. K. Malick, A. D. Rabuck, K. Raghavachari, J. B. Foresman, J. Cioslowski, J. V. Ortiz, B. B. Stefanov, G. Liu, A. Liashenko, P. Piskorz, I. Komaromi, R. Gomperts, R. L. Martin, D. J. Fox, T. Keith, M. A. Al-Laham, C. Y. Peng, A. Nanayakkara, C. Gonzales, M. Challacombe, P. M. W. Gill, B. Johnson, W. Chen, M. W. Wong, J. L. Andres, C. Gonzales, M. Head-Gordon, E. S. Replogle, J. A. Pople, in GAUSSIAN98 (Revision A.6), Gaussian, Inc. Pittsburgh PA, Gaussian, Inc. Pittsburgh PA, 1998.