Optimized separation of isoquinoline alkaloids in Thalictrum herbal medicine by microemulsion electrokinetic chromatography

Journal of Liquid Chromatography and Related Technologies

Volumn 26, Issue 11, 2003, Pages 1719-1730

  Luo, Yiqi ^a   Bo, Tao ^a   Li, Meng ^a   Gong, Suxuan ^a   An Li, Ke ^a   Liu, Huwei ^a  

^a PEKING UNIVERSITY   (China)

Author keywords

Isoquinoline alkaloid; Microemulsion electrokinetic chromatography; Thalictrum

Indexed keywords

COMPOSITION; ELECTRIC POTENTIAL; MICROEMULSIONS; OPTIMIZATION; PLANTS (BOTANY); SEPARATION;

ELECTROKINETIC CHROMATOGRAPHY;

LIQUID CHROMATOGRAPHY;

ANALGESIC AGENT; BERBAMINE; BERBERINE; BUTANOL; CHOLIC ACID; DODECYL SULFATE SODIUM; HEPTANE; ISOQUINOLINE ALKALOID; JATRORRHIZINE; METHANOL; NORTHALFINE; PHOSPHATE; STEROID; STYLOPINE; THALIFARETINE; THALIFARICINE; UNCLASSIFIED DRUG; VITAMIN;

ARTICLE; HERB; HERBAL MEDICINE; MICELLAR ELECTROKINETIC CHROMATOGRAPHY; MICROEMULSION; PH; SEPARATION TECHNIQUE; TEMPERATURE DEPENDENCE; THALICTRUM;

THALICTRUM;

EID: 0037715299     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-120021279     Document Type: Article

References (23)

1. Gao, G.Y. Study of the Chemical Components of T. Atriplex Finet et Gagep; Institute of Medicinal Plant Development, Peking Union Medical College and Chinese Academy of Medical Sciences: Beijing, China, 1995; Ph.D. Dissertation, 12-18.
2. Zhou, Y.; Guo, Y.Z.; Meng, X.S. Chinese Herbal Medicine (Chinese) 1990, 21 (9), 13-14.
3. Wang, X.X.; Guo, Y.Z. Shenyang Yaoxue Xuebao (Chinese) 1992, 9 (1), 22-25.
4. Zhou, Y.; Guo, Y.Z.; Meng, X.S. Shenyang Yaoxue Xuebao (Chinese) 1991, 8 (4), 291-292.
5. Wang, Z.T.; Xiao, P.G. Chinese Herbal Medicine 1988, 19 (4), 17-18.
6. Zhu, M., Xiao, P.G. Yaowu Fenxi Zazhi (Chinese) 1990, 10 (2), 72-77.
7. Li, Y.; Liu, H.; Ji, X.; Li, J. Optmimized separation of pharmacologically active anthraquinones in rhubarb by capillary electrochromatography. Electrophoresis 2000, 21, 3109-3115.
8. Hsieh, F.Y.L.; Cai, J.; Henion, J. Determination of trace impurities of peptides and alkaloids by capillary electrophoresis-ion spray mass spectrometry. J. Chromatogr. A 1994, 679, 206-211.
9. Henion, J.D.; Mordehai, A.V.; Cai, J. Quantitative capillary electrophoresis-ion spray mass spectroscopy on a benchtop ion trap for the determination of isoquinoline alkaloids. Anal. Chem. 1994, 66, 2103-2109.
10. Eeva, M.; Sala, J.P., Oksman-Caldentey, K.M. Determination of the main tropane alkaloids from transformed Hyoscyamus muticus plants by capillary zone electrophoresis. J. Pharm. Biomed. Anal. 1998, 16, 717-722.
11. Terabe, S.; Otsuka, K.; Ichikawa, K.; Tsuchiya, A.; Ando, T. Electrokinetic separations with micellar solutions and open-tubular capillaries. Anal. Chem. 1984, 56, 111-113.
12. Szucs, R.; Van Hove, E.; Sandra, P. Micellar and microemulsion electrokinetic chromatography of hop bitter acids. J. High Resol. Chromatogr. 1996, 19, 189-192.
13. Liu, Y.M.; Sheu, S.J. Determination of coptisine, berberine and palmatine in traditional Chinese medicinal perparations by capillary electrophoresis. J. Chromatogr. A 1993, 639, 323-328.
14. Lee, M.CH.; Sheu, S.J. Determination of coptis-evodia herb couple by capillary electrophoresis. J. Liq. Chromatogr. & Rel. Technol. 1997, 20, 63-78.
15. Su, X.D.; Bo, T; Li, R.K.; Li, K.A.; Liu, H.W. Determination of isoquinoline alkaloids in Thalictrum herbal drugs by non-aqueous capillary electrophoresis. Chromatographia 2002, 55 (1/2), 63-68.
16. Altria, K.D. Background theory and applications of microemulsion electrokinetic chromatography. J. Chromatogr. A 2000, 892, 171-186.
17. Watarai, H.; Ogawa, K.; Abe, M.; Monta, T.; Takahashi, I. Capillary electrophoresis with O/W microemulsions of water/SDS/1-butanol/ heptane. Anal. Sci. 1991, 7, 245-248.
18. ow) by microemulsion electrokinetic chromatography. J. Chromatogr. B 2000, 745, 117-126.
19. Gluck, S.J.; Benko, M.H.; Hallberg, R.K.; Steele, K.P. Indirect determination of octanol-water partition coefficients by microemulsion electrokinetic chromatography. J. Chromatogr. A 1996, 744, 141-146.
20. Ishihama, Y.; Oda, Y.; Asakawa, N. Hydrophobicity of cationic solutes measured by electrokinetic chromatography with cationic microemulsions. Anal. Chem. 1996, 68, 4281-4284.
21. Watarai, H. Microemulsions in separation sciences. J. Chromatogr. A 1997, 780, 93-102.
22. Watarai, H. Microemulsion capillary electrophoresis. Chem. Lett. 1991, 3, 391-394.
23. Gong, S.X.; Su, X.D.; Bo, T.; Li, K.A.; Liu, H.W. Determination of dissociation constants of ten alkaloids by capillary zone electrophoresis. J. Sep. Sci. in press.