Direct determination of estriol 3- and 16-glucuronides in pregnancy urine by column-switching liquid chromatography with electrospray tandem mass spectrometry

Biomedical Chromatography

Volumn 17, Issue 4, 2003, Pages 219-225

  Yang, Yoon Jung ^a   Lee, Jeongae ^a   Choi, Man Ho ^a   Chung, Bong Chul ^a  

^a Korea Institute of Science and Technology   (South Korea)

Author keywords

Estriol glucuronides; Negative ion ESI; Pre column concentration; Selected reaction monitoring

Indexed keywords

BODY FLUIDS; COLUMN CHROMATOGRAPHY; ELECTROSPRAY IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; OBSTETRICS; SCREENING; SIGNAL TO NOISE RATIO;

COLUMN SWITCHING; DIRECT DETERMINATION; ELECTROSPRAY TANDEM MASS SPECTROMETRY; ESTRIOL GLUCURONIDE; GLUCURONIDES; ION ELECTROSPRAY IONIZATION; NEGATIVE ION ELECTROSPRAY IONIZATION; PRE-COLUMN CONCENTRATION; SELECTED REACTION MONITORING; URINE SAMPLE;

NEGATIVE IONS;

ESTRIOL 16 GLUCURONIDE; ESTRIOL 3 GLUCURONIDE; ESTROGEN DERIVATIVE; UNCLASSIFIED DRUG;

ACCURACY; ANALYTIC METHOD; ARTICLE; ASSAY; CALIBRATION; CLINICAL ARTICLE; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; FEMALE; FETUS; FETUS MONITORING; FILTRATION; HUMAN; INJECTION; LINEAR SYSTEM; LIQUID CHROMATOGRAPHY; MEMBRANE FILTER; PATIENT MONITORING; PREGNANCY; SCREENING TEST; SENSITIVITY ANALYSIS; SIGNAL NOISE RATIO; TANDEM MASS SPECTROMETRY; TIME; URINALYSIS; URINE LEVEL;

EID: 0037710731     PISSN: 02693879     EISSN: None     Source Type: Journal    
DOI: 10.1002/bmc.215     Document Type: Article

References (16)

1. de Alda MJL and Barceló D. Determination of steroid sex hormones and related synthetic compounds considered as endocrine disrupters in water by liquid chromatography-diode array detection-mass spectrometry. Journal of Chromatography A 2000; 892: 391.
2. Andreolini F, Borra C, Di Corcia A, Samperi R and Raponi G. Improved determination of estriol-16α-glucuronide in pregnancy urine by direct liquid chromatography with fluorescence detection. Clinical Chemistry 1985; 31: 124.
3. Barnard G, Collins WP, Kohen F and Lindner HR. The measurement of urinary estriol-16 alpha-glucuronide by a solid-phase chemiluminescence immunoassay. Journal of Steroid Biochemistry 1981; 14: 941.
4. Caccamo F. Carfagnini G, Di Corcia A and Samperi R. Measurement of urinary estriol glucuronides during the menstrual cycle by high-performance liquid chromatography. Journal of Chromatography 1988; 434: 61.
5. Dipietro DL. Assay of estriol-16α-(β-D-glucuronide) in pregnancy urine with a specific antiserum. American Journal of Obstetric Gynecology 1976; 125: 841.
6. Iwata T, Hirose T and Yamaguchi M. Direct determination of estriol 3-and 16-glucuronides in pregnancy urine by column-switching high-performance liquid chromatography with fluorescence detection. Journal of Chromatography B 1997; 695: 201.
7. Kohen F, Kim JB, Barnard G and Lindner HR. An assay for urinary estriol-16 alpha-glucuronide based on antibody-enhanced chemiluminescence. Steroids 1980; 36: 405.
8. Lehtinen T and Adlercreutz H. Solid-phase radioimmunoassays of estriol-16alpha-glucuronide in urine and pregnancy plasma. Journal of Steroid Biochemistry 1977; 8: 99.
9. Levitz M, Kadner S and Young BK. Intermediary metabolism of estriol in pregnancy. Journal of Steroid Biochemistry 1984; 20: 971.
10. Mendizabal AF, Quiroga S. Farinati Z, Lahoz M and Nagle C. Hormonal monitoring of early pregnancy by a direct radioimmunoassay of steroid glucuronides in first morning urine. Fertility and Sterility 1984; 42: 737.
11. Peter M, Dorr HG and Sippell WG. Changes in the concentrations of dehydroepiandrosterone sulfate and estriol in maternal plasma during pregnancy: a longitudinal study in healthy women throughout gestation and at term. Hormone Research 1994; 42: 278.
12. Schimada K, Xie F and Nambara T. Studies on steroids. CLXXIX. Determination of estriol 16- and 17-glucuronide in biological fluids by high-performance liquid chromatography with electrochemical detection. Journal of Chromatography 1982; 232: 13.
13. Schöneshöfer M, Dhar TK and Ioanides D. Total urinary estriol determined by "on-line" liquid chromatography with ultraviolet detection. Clinical Chemistry 1986; 32: 1948.
14. Sugar J, Alexander S, Dessy C and Schwers J. Radioimmunoassay of estriol-16-glucuronide. Journal of Clinical Endocrinology and Metabolism 1977; 45: 945.
15. Tiel U, Heilmann P, Rejaibi R and Schöneshöfer M. Urinary oesriol-16-glucuronide determined by "on-line" liquid chromatography. Journal of Clinical Chemistry and Clinical Biochemistry 1989; 27: 205.
16. Zhang H and Henion J. Quantitative and qualitative determination of estrogen sulfates in human urine by liquid chromatography/tandem mass spectrometry using 96-well technology. Analytical Chemistry 1999; 71: 3955.