GC behavior of disaccharide trimethylsilyl oximes

Journal of Chromatographic Science

Volumn 41, Issue 4, 2003, Pages 205-208

  Sanz, M L ^a   Diez Barrio, M T ^a   Sanz, J ^a   Martinez Castro I ^a  

^a INSTITUTO DE QUÍMICA ORGÁNICA GENERAL   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

DISACCHARIDE; OXIME DERIVATIVE; SILICONE DERIVATIVE; TRIMETHYLSILYL DERIVATIVE;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; DATA ANALYSIS; GAS CHROMATOGRAPHY; MULTIVARIATE ANALYSIS;

EID: 0037676225     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/41.4.205     Document Type: Article

References (14)

1. 7 carbohydrates as the trimethylsilyloxime derivatives on packed and capillary columns. J. Chromatogr. Sci. 21: 132-38 (1983).
2. J.T. Scanlon and D.E. Willis. Calculation of flame ionization detector relative response factors using the effective carbon number concept. J. Chromatogr. Sci. 23: 333-40 (1985).
3. I. Molnar-Perl and K. Horvath. Simultaneous quantitation of mono-, di- and trisaccharides as their TMS ether oxime derivatives by GC-MS: I. In model solutions. Chromatographia 45: 321-27 (1997).
4. J.A. Gómez-Barez, R.J. García-Vilanova, S. Elvira-García, and A.M. González-Paramás. Optimization of the capillary gas chromatographic analysis of mono- and oligosaccharides in honeys. Chromatographia 50: 461-69 (1999).
5. G.W. Chapman and R.J. Horvath. Determination of nonvolatile acids and sugars from fruits and sweet potato extracts by capillary GLC and GLC/MS. J. Agric. Food Chem. 37: 947-50 (1989).
6. R. Mateo and F. Bosch-Reig. Sugar profiles of Spanish unifloral honeys. Food Chem. 60: 33-41 (1997).
7. K.M. Brobst and C.E. Lott. Determination of some components in corn syrup by gas-liquid chromatography of trimethylsilyl derivatives. Cereal Chem. 43: 35-43 (1966).
8. B.W. Li and P.J. Schumann. Gas chromatographic analysis of sugars in granola cereals. J. Food Sci. 46: 425-27 (1981).
9. W.J. Dixon, Ed. BMDP Statistical Software release 7. University Press of California, Los Angeles, CA, 1992.
10. W. Funcke and C. von Sonntag. Syn and anti forms of some monosaccharide o-methyl oximes: a 13C-n.m.r. and g.l.c. study. Carbohyd. Res. 69: 247-51 (1979).
11. A. Garcia-Raso, M.I. Páez, I. Martinez-Castro, J. Sanz, and M.M. Calvo. Gas chromatographic retention of carbohydrate trimethylsilyl ethers; IV Disaccharides. J. Chromatogr. 607: 221-25 (1992).
12. L.M. Blumberg and M.S. Klee. Metrics of separation in chromatography. J. Chromatogr. A 933: 1-11 (2001).
13. J. Haverkamp, J.P. Kamerling, and J.F.G. Vliegentart. Gas-liquid chromatography of trimethylsilyl disaccharides. J. Chromatogr. 59: 281-87 (1971).
14. C.C. Sweeley, R. Bentley, M. Makita, and W.W. Wells. Gas-liquid chromatography of trimethylsilyl derivatives of sugars and related substances. J. Am. Chem. Soc. 85: 2497-2507 (1963).