Synthesis of novel mixed metal cluster complexes of osmium and mercury: Formation of the wheel-shaped cluster complexes Os6(μ-6-Hg)(μ-PR2)2(CO)20 (R = Ph, i-Bu)

Organometallics

Volumn 21, Issue 9, 2002, Pages 1925-1932

  Egold, Hans ^a   Schraa, Markus ^a   Flörke, Ulrich ^a   Partyka, Janusch ^a  

^a UNIVERSITY OF PADERBORN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

SINGLE-CRYSTAL X-RAY ANALYSIS;

CHEMICAL BONDS; HEATING; ISOMERS; MERCURY COMPOUNDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OSMIUM COMPOUNDS; PHOTOSENSITIVITY; RATE CONSTANTS; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); THERMODYNAMIC PROPERTIES; TOLUENE; ULTRAVIOLET SPECTROSCOPY; X RAY ANALYSIS;

ORGANOMETALLICS;

EID: 0037667402     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om0110585     Document Type: Article

References (42)

1. Ermer, S.; King, K.; Hardcastle, K. I.; Rosenberg, E.; Lanfredi, A. M. M.; Tiripicchio, A.; Tiripicchio-Camellini, M. Inorg. Chem. 1983, 22, 1339.
2. Gomez-Sal, M. P.; Johnson, B. F. G.; Lewis, J.; Raithby, P. R.; Syed-Mustaffa, S. N.; Azman B. J. Organomet. Chem. 1984, 272, C21.
3. Hajela, S.; Novak, B. M.; Rosenberg, E. Organometallics 1989, 8, 468.
4. Rosenberg, E.; Hardcastle, K. I.; Day, M. W.; Gobetto, R.; Hajela, S.; Muftikian, R. Organometallics 1991, 10, 203.
5. Andreu, P. L.; Cabeza, J. A.; Llamazares, A.; Riera, V.; Bois, C.; Jeannin, Y. J. Organomet. Chem. 1991, 420, 431.
6. Osella, D.; Milone, L.; Kukharenko, S. V.; Strelets, V. V.; Rosenberg, E.; Hajela, S. J. Organomet. Chem. 1993, 451, 153.
7. Au, Y.-K.; Wong, W.-T. J. Chem. Soc., Dalton Trans. 1995, 1389.
8. Au, Y.-K.; Wong, W.-T. J. Chem. Soc., Dalton Trans. 1996, 899.
9. Au, Y.-K.; Wong, W.-T. Inorg. Chem. 1997, 36, 2092.
10. Kong, F.-S.; Wong, W.-T. J. Chem. Soc., Dalton Trans. 1999, 2497.
11. Gade, L. H. Angew. Chem. 1998, 105, 25.
12. King, R. B. Polyhedron 1988, 7, 1813.
13. King, R. B. J. Chem. Inf. Comput. Sci. 1994, 34, 410.
14. Bianchini, A.; Farrugia, L. J. Organometallics 1992, 11, 540.
15. Farrugia, L. J. Chem. Commun. 1987, 147.
16. Yamamoto, Y.; Yamazaki, H.; Sakurai, T. J. Am. Chem. Soc. 1982, 104, 2329.
17. Albinati, A.; Moor, A.; Pregosin, P. S.; Venanzi, L. M. J. Am. Chem. Soc. 1982, 104, 7672.
18. Mednikov, E. G.; Eremenko, N. K.; Bashilov, V. V.; Sokolov, V. I. Inorg. Chim. Acta 1983, 76, L31.
19. Yamamoto, Y.; Takahashi, K.; Yamazaki, H. Chem. Lett. 1985, 201.
20. Yamamoto, Y.; Yamazaki, H. J. Chem. Soc., Dalton Trans. 1989, 2161.
21. Tanase, T.; Horiuohi, T.; Yamamoto, Y.; Kobayashi, K. J. Organomet. Chem. 1992, 440, 1.
22. Yamamoto, Y.; Yamazaki, H. Organometallics 1993, 12, 933.
23. Yamamoto, Y.; Yamazaki, H Inorg. Chim. Acta 1994, 217,121.
24. Hao, L.; Vittal, J. J.; Puddephatt, R. J. Inorg. Chem. 1996, 35, 269.
25. Hao, L.; Vittal, J. J.; Puddephatt, R. J. Organometallics 1996, 15, 3115.
26. Jones, R. A.; Mayor R..F.; Wilkinson, G.; Galas, A. M. R.; Hursthouse, M. B. J. Chem. Soc., Dalton Trans. 1981, 126.
27. Braunstein, P.; Rose, J.; Tiripicchio, A.; Tiripicchio-Camellini, M. Angew. Chem. 1985, 97, 761.
28. Braunstein, P.; Rose, J.; Tiripicchio, A.; Tiripicchio-Camellini, M. J. Chem. Soc., Dalton Trans. 1992, 911.
29. Gade, L. H.; Johnson, B. F. G.; Lewis, J.; McPartlin, M.; Scowen, I. J. J. Chem. Soc., Dalton Trans. 1996, 597.
30. Charadonna, G.; Ingrosso, G.; Marchetti, F. Angew. Chem., Int. Ed. 2000, 39, 3872.
31. Housecroft, C. E.; Johnson, B. F. G.; Lewis, J.; Lunniss, J. A.; Owen, S. M.; Raithby, P. R. J. Organomet. Chem. 1991, 409, 271.
32. Mauser, H. Experimentelle Methoden der Physik und Chemie (Band 1): Formale Kinetik; Bertelsmann Universitätsverlag, 1974.
33. Autorenkollektiv. Photochemie, VEB Deutscher Verlag der Wissenschaften: Berlin, 1975.
34. Colbran, S. B.; Irele, P. T.; Johnson, B. F. G.; Lahoz, F. J.; Lewis, J.; Raithby, P. R. J. Chem. Soc., Dalton Trans. 1989, 2023.
35. Colbran, S. B.; Irele, P. T.; Johnson, B. F. G.; Lahoz, F. J.; Lewis, J.; Raithby, P. R. J. Chem. Soc., Dalton Trans. 1989, 2033.
36. Fajardo, M.; Holden, H. D.; Johnson, B. F. G.; Lewis, J.; Raithby, P. R. J. Chem. Soc., Chem. Commun. 1984, 24.
37. Johnson, B. F. G.; Lewis, J.; Pippard, D. A.. J. Chem. Soc., Dalton Trans. 1981, 407.
38. Drake, S. R.; Khattar, R. Organomet. Synth. 1988, 4, 234.
39. Sheldrick, G. M. SHELX-97, A Program for Crystal Structure Solution and Refinement; University of Göttingen, 1998.
40. Swinbourne, E. S. Auswertung und Analyse kinetische Messungen; Verlag Chemie: Weinheim, 1975.
41. Wedler, G. Lehrbuch der physikalischen Chemie, 4.Auflage; VCH-Wiley: Weinheim, 1997.
42. Egold, H.; Schraa, M.; Flörke, U., unpublished results.