Native fluorescence determination of pyridoxine hydrochloride (vitamin B6) in pharmaceutical preparations after sorption on Sephadex SP C-25

Spectroscopy Letters

Volumn 36, Issue 1-2, 2003, Pages 133-149

  Ortega Algar, S ^a   Ramos Martos, N ^a   Molina Diaz A ^a  

^a UNIVERSITY OF JAÉN   (Spain)

Author keywords

Drug formulations; Pyridoxine hydrochloride; Solid phase spectrofluorimetry

Indexed keywords

PYRIDOXINE; SEPHADEX;

ARTICLE; CATION EXCHANGE; DRUG DETERMINATION; DRUG FORMULATION; DRUG MANUFACTURE; FLUORESCENCE; GEL; MEASUREMENT; SOLID; SPECTROFLUOROMETRY; VALIDATION PROCESS;

EID: 0037639764     PISSN: 00387010     EISSN: None     Source Type: Journal    
DOI: 10.1081/SL-120021783     Document Type: Article

References (39)

1. Rocha, F.R.P.; Fatibello Filho, O.; Reis, B.F. A multicommuted flow system for sequential spectrophotometric determination of hydrosoluble vitamins in pharmaceutical preparations. Talanta 2003, 59, 191-200.
2. Ortega-Barrales, P.; Domínguez-Vidal, A.; Fernández-Córdova, M.L.; Molina-Díaz, A. Simultaneous determination of thiamine and pyridoxine in pharmaceuticals by using a single flow-through biparameter sensor. J. Pharm. Biomed. Anal. 2000, 24, 619-630.
3. Abdine, H.H.; Gazy, A.A.; Abdel-Hay, M.H. Simultaneous determination of melatonin-pyridoxine combination in tablets by zero-crossing derivative spectrophotometry and spectrofluorimetry. J. Pharm. Biomed. Anal. 1998, 17, 379-386.
4. Dinq, E.; Kokdil, G.; Onur, F. A comparison of matrix resolution method, ratio spectra derivative spectrophotometry and HPLC method for the determination of thiamine HCI and pyridoxine HCI in pharmaceutical preparation.
5. Ayora Cañada, M.J.; Pascual Reguera, M.I.; Molina Díaz, A. Selective determination of pyridoxine in the presence of hydrosoluble vitamins using a continuous-flow solid phase sensing device. Int. J. Pharm. 2000, 202, 113-120.
6. Escandar, G.M.; Bystol, A.J.; Campiglia, A.D. Spectrofluorimetric method for determination of piroxicam and pyridoxine. Anal. Chim. Acta 2002, 466, 275-283.
7. García, L.; Blázquez, S.; San Andrés, M.P.; Vera, S. Determination of thiamine, riboflavin and pyridoxine in pharmaceuticals by synchronous fluorescence spectrometry in organized media. Anal. Chim. Acta 2001, 434, 193-199.
8. Ramos Martos, N.; Molina Díaz, A.; Navalón, A.; De Orbe Payá, I.; Capitán Vallvey, L.F. Simultaneous spectrofluorimetric determination of (acetyl) salicylic acid, codeine and pyridoxine in pharmaceutical preparations using partial least-squares multivariate calibration. J. Pharm. Biomed. Anal. 2000, 23, 837-844.
9. Alwarthan, A.A.; Aly, F.A. Chemiluminescent determination of pyridoxine hydrochloride in pharmaceutical samples using flow injection. Talanta 1998, 45, 1131-1138.
10. Höller, U.; Brodhag, C.; Knöbel, A.; Hofmann, P.; Spitzer, V. Automated determination of selected water-soluble vitamins in tablets using a bench-top robotic system coupled to reversed-phase (RP-18) HPLC with UV detection. J. Pharm. Biomed. Anal. 2003, 31, 151-158.
11. Monferrer-Pons, L.; Capella-Peiró, M.E.; Gil-Agustf, M.; Esteve-Romero, J. Micellar liquid chromatography determination of B vitamins with direct injection and ultraviolet absorbance detection. J. Chromatogr. 2003, 984, 223-231.
12. 12, in multivitamin tablets by high performance liquid chromatography. J. Pharm. Biomed. Anal. 2002, 30, 1403-1410.
13. Moreno, P.; Salvadó, V. Determination of eight water-and fat-soluble vitamins in multi-vitamin pharmaceutical formulations by high-performance liquid chromatography. J. Chromatogr. 2002, 870, 207-215.
14. Chen, G.; Ding, X.; Cao, Z.; Ye, J. Determination of melatonin and pyridoxine in pharmaceutical preparations for health-caring purposes by capillary electrophoresis with electrochemical detection. Anal. Chim. Acta 2000, 408, 249-256.
15. Nuñez-Vergara, L.J.; Squella, J.A.; Sturm, J.C.; Baez, H.; Camargo, C. Simultaneous determination of melatonin and pyridoxine in tablets by gas chromatography-mass spectrometry. J. Pharm. Biomed. Anal. 2001, 26, 929-938.
16. Molina Díaz, A.; Ramos Martos, N.; Navalón, A.; Capitán Vallvey, L.F. Simultaneous determination of codeine and pyridoxine in pharmaceutical preparations by first-derivative spectrofluorimetry. J. AOAC. Int. 2002, 85, in press.
17. Ortega-Barrales, P.; Molina-Díaz, A.; Pascual-Reguera, M.I.; Capitán-Vallvey, L.F. Solid-phase spectrophotometric determination of trace amounts of hydrazine at sub-ng/mL level. Anal. Chim. Acta 1997, 353, 115-122.
18. Yoshimura, K.; Waki, H. Ion-exchanger phase absorptiometry for trace analysis. Talanta 1985, 32, 345-352.
19. Ortega-Barrales, P.; Fernández-Córdova, M.L.; Molina-Díaz, A. Indirect determination of ascorbic acid by solid-phase spectrophotometry. Anal. Chim. Acta 1998, 360, 143-152.
20. Ortega-Barrales, P.; Ayora-Cañada, M.J.; Molina-Díaz, A.; Garrigues, S.; de la Guardia, M. Solid phase Fourier transform near infrared spectroscopy. Analyst 1999, 124, 579-582.
21. Vilchez, J.L.; Rohand, J.; Navalón, A.; Avidad, R.; Capitán-Vallvey, L.F. Determination of warfarin at trace-levels in water by solid-phase spectrofluorimetry. Fresenius' J. Anal. Chem. 1996, 354, 470-473.
22. Pascual-Reguera, M.I.; Molina-Díaz, A.; Ramos-Martos, N. Determination of traces of vanadium with 5-bromosalicylhydroxamic acid by solid-phase spectrophotometry. Anal. Lett. 1991, 12 (24), 2245-2261.
23. 12 by solid-phase UV spectrophotometry. Anal. Chem. 1998, 2 (70), 271-275.
24. Capitán, F.; Sánchez-Palencia, G.; Navalón, A.; Capitán-Vallvey, L.F. Simultaneous determination of molybdenum and tungsten by first-derivative synchronous solid-phase spectrofluorimetry. Anal. Chim. Acta 1992, 259, 345-353.
25. Yoshimura, K. Implementation of ion-exchanger absorptiometric detection in flow analysis systems. Anal. Chem. 1987, 59, 2922-2924.
26. Lázaro, F.; Luque, M.D.; Valcárcel, M. Integrated reaction/spectrophotometric detection in unsegmented flow systems. Anal. Chim. Acta 1988, 214, 217-227.
27. Torre, M.; Fernández-Gámez, F.; Lázaro, F.; Luque, M.D.; Valcárcel, M. Spectrofluorimetric flow-trough sensor for the determination of beryllium in alloys. Analyst 1991, 116, 81-83.
28. Ayora-Cañada, M.J.; Pascual-Reguera, M.I.; Molina-Díaz, A. An integrated reaction-retention and spectrophotometric detection flow system for the determination of nickel. Fresenius' J. Anal. Chem. 1999, 363, 59-63.
29. Matsuoka, S.; Yoshimura, K.; Tateda, A. Application of ion-exchanger phase visible light absorption to flow analysis. Determination of vanadium in natural water and rock. Anal. Chim. Acta 1995, 317, 207-213.
30. Ruíz-Medina, A.; Fernández-Córdova, M.L.; Molina-Díaz, A. Flow-trough solid-phase UV Spectrophotometric determination of amoxycillin. Anal. Lett. 1999, 4 (32), 729-742.
31. Molina-Díaz, A.; Ruíz-Medina, A.; Fernández-Córdova, M.L. The potential of flow-trhough optosensors in pharmaceuticals analysis. J. Pharm, Biomed. Anal. in press.
32. Navalón, A.; Ballesteros, O.; Sánchez-Palencia, G.; Vilchez, J.L. Determination of ciprofloxacin in human urine and serum samples by solid-phase spectrofluorimetry. Talanta 2000, 52, 845-852.
33. Navalón, A.; Ballesteros, O.; Taoffki, J.; Vilchez, J.L. Determination of the antibacterial drug norfloxacin in human urine and serum samples by solid-phase spectrofluorimetry. Anal. Chim. Acta 2001, 52, 279-286.
34. Vilchez, J.L.; Taoffki, J.; Navalón, A. Determination of the antibacterial drug trovafloxacin by solid phase spectrofluorimetry. Anal. Lett. 2002, 35, 257-268.
35. Ballesteros, O.; Vilchez, J.L.; Navalón, A. Determination of antibacterial ofloxacin in human urine and serum samples by solid-phase spectrofluorimetry. J. Pharm. Biomed. Anal. 2002, 30, 1103-1110.
36. Rendell, D. Fluorescence and Phosphorescence Spectroscopy; Wiley Interscience: New York, 1987; 91-93.
37. I.U.P.A.C. Analytical Chemistry Division Nomenclature, symbols, units and their usage in spectrochemical analysis-II. Data interpretation. Spectrochim. Acta, Part B 1978, 33, 242-245.
38. A.C.S. Guidelines for data acquisition and data quality evaluation in environmental chemistry. Anal. Chem. 1980, 52, 2242-2249.
39. Ruíz-Medina, A.; Fernández-Córdova, M.L.; Molina-Díaz, A. Flow injection-solid phase spectrofluorimetric determination of pyridoxine in presence of group B-vitamins. Fresenius' J. Anal. Chem 1999, 363, 265-269.