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Volumn 42, Issue 2, 2003, Pages 255-257

NMR evaluation of the configurational stability of Cu(I) complexes

Author keywords

[No Author keywords available]

Indexed keywords

1,10 PHENANTHROLINE; 2 IMINOPYRIDINE; 2,2' BIPYRIDINE; COPPER COMPLEX; PYRIDINE DERIVATIVE; UNCLASSIFIED DRUG;

EID: 0037467785     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic0259890     Document Type: Article
Times cited : (55)

References (28)
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    • note
    • R and S correspond to and configurations in the oriented-skew-lines reference system, respectively.
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    • note
    • c , the frequency separation of the peaks, Δν (Hz), and the coupling constant between the nuclei, J (Hz).
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    • note
    • Chiral ligands (L*) can also be used to induce an NMR differentiation. However, a high diastereoselectivity is often observed upon complex formation, meaning that only the signals of the major diastereomer appear: see ref 2d.
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    • Dietrich-Buchecker, C. O.; Nierengarten, J. F.; Sauvage, J. P.; Armaroli, N.; Balzani, V.; De Cola, L. J. Am. Chem. Soc. 1993, 115, 11237-11244. Dietrich-Buchecker, C.; Jimdnez, M. C.; Sauvage, J. P. Tetrahedron Lett. 1999, 40, 3395-3396.
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    • 0012879497 scopus 로고    scopus 로고
    • note
    • [Cinchonidinium] [Δ-4] (dr > 39:1) was used for the ion exchange.
  • 26
    • 0012825055 scopus 로고    scopus 로고
    • note
    • The lower barrier for exchange of bpy-derived complexes as compared to those derived from phen might be due to the probable stepwise mechanism for the exchange process, which could be better accommodated by the flexible 2,2′-bond of the bpy. We thank the reviews for this suggestion.
  • 27
    • 0012835186 scopus 로고    scopus 로고
    • note
    • c ≥ 328 K and Δν = 11.4 Hz (Δδ 0.030 ppm for H(t-Bu)). See Supporting Information.
  • 28
    • 0012774392 scopus 로고    scopus 로고
    • note
    • 2][Δ-4].


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.