A novel dinuclear species in the aqueous distribution of aluminum in the presence of citrate

Inorganic Chemistry

Volumn 42, Issue 2, 2003, Pages 252-254

  Dakanali, Maria ^a   Raptopoulou, Catherine P ^b   Terzis, Aristidis ^b   Lakatos, Andrea ^d   Banyai, Istvan ^c   Kiss, Tamas ^d   Salifoglou, Athanasios ^a  

^a UNIVERSITY OF CRETE   (Greece)

^b INSTITUTE OF NANOSCIENCE AND NANOTECHNOLOGY   (Greece)

^c UNIVERSITY OF DEBRECEN   (Hungary)

^d UNIVERSITY OF SZEGED   (Hungary)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINUM; CITRIC ACID;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; COMPLEX FORMATION; INFRARED SPECTROSCOPY; MOLECULAR INTERACTION; NUCLEAR MAGNETIC RESONANCE; PROTON TRANSPORT; REACTION ANALYSIS; THERMODYNAMICS;

EID: 0037467717     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic0258025     Document Type: Article

References (36)

1. (a) Nayak, P. Environ. Res. 2002, 89, 101-115.
2. (b) Campbell, A.; Yang, E. Y.; Tsai-Turton. M.; Bondy, S. C. Brain Res. 2002, 933, 60-65.
3. (c) Rondeau, V. Rev. Environ. Health 2002, 17, 107-121.
4. (d) Meiri, H.; Banin, E.; Roll, M.; Rouesseau, A. Prog. Neurobiol. 1993, 40, 89-121.
5. (e) Van der Voet, G. B.; Van Ginkel, M. F.; de Wolff, F. A. Toxicol. Appl. Pharmacol. 1989, 99, 90.
6. (f) Kerr, D. N. S.; Ward. M. K. In Metal Ions in Biological Systems; Sigel, H., Sigel, A., Eds.; Marcel Dekker: New York, 1988; Vol. 24, Chapter 6, pp 217-258.
7. (a) Malluche, H. H. Nephrol. Dial. Transplant. 2002, 17 (Suppl. 2), 21-24.
8. (b) Cannata-Andia, J. B.; Fernandez-Martin, J. L. Nephrol. Dial. Transplant. 2002, 17 (Suppl. 2), 9-12.
9. (c) Pratico, D.; Uryu, K.; Sung, S.; Tang, S.; Trojanowski, J. Q.; Lee, V. M. FASEB J. 2002, 16, 1138-1140.
10. (d) Hull, M. J.; Abraham, J. L. Hum. Pathol. 2002, 33, 819-825.
11. (e) Exley, C. J. Alzheimer's Dis. 2001, 3, 551-552.
12. (f) Rondeau, V.; Commenges, D. In Aluminium and Alzheimer's Disease: The Science that Describes the Link; Exley, C., Ed.; Elsevier Science: New York, 2001.
13. (g) Rondeau, V.; Commenges, D.; Jacqmin-Gadda, H.; Dartigues, J.-F. Am. J. Epidemiol. 2000, 152, 59-66.
14. (h) Fasman, G. D.; Moore, C. D. Proc. Natl. Acad. Sci. U.S.A. 1994, 91, 11232-11235.
15. (a) Martin, R. B. J. Inorg. Biochem. 1986, 28, 181-187.
16. (b) Etcheverry, S. B.; Apella, M. C.; Baran, E. J. J. Inorg. Biochem. 1984, 20, 269-274.
17. (c) Glusker, J. P. Acc. Chem. Res. 1980, 13, 345-352.
18. 3 and citric acid were placed in aqueous solution with a molar ratio of 1:2. The resulting reaction mixture was stirred overnight with mild heating. On the following day, the reaction mixture was taken to dryness by means of a rotary evaporator. The residue was redissolved in the minimum amount of water, and the pH of the resulting solution was adjusted to ∼3.5 with a solution of aqueous ammonia (1:1). Stirring continued at room temperature for an additional 2 h. Subsequently, ethanol was added and the reaction flask was placed in the refrigerator. Two weeks later, a colorless crystalline material was deposited at the bottom of the flask. The crystals were isolated by filtration and dried in vacuo (yield ∼50%). Satisfactory elemental analysis was obtained for 1 (See Supporting Information).
19. 1 four-circle diffractometer, upgraded by Crystal Logic. Unit cell dimensions for 1 were determined and refined by using the angular settings of 25 automatically centered reflections in the range 22° < 2θ < 54°. Intensity data were measured by using θ-2θ scans. Detailed crystallographic information has been deposited as Supporting Information.
20. Sheldrick, G. M. SHELXS-86: Structure Solving Program; University of Göttingen: Göttingen, Germany, 1986.
21. Sheldrick, G. M. SHELXL-93: Structure Refinement Program; University of Göttingen: Göttingen, Germany, 1993.
22. Matzapetakis, M.; Raptopoulou, C. P.; Terzis, A.; Lakatos, A.; Kiss, T.; Salifoglou, A. Inorg. Chem. 1999, 38, 618-619.
23. Matzapetakis, M.; Kourgiantakis, M.; Danakali. M.; Raptopoulou, C. P.; Terzis, A.; Lakatos, A.; Kiss, T.; Banyai, I.; Iordanidis, L.; Mavromoustakos, T.; Salifoglou, A. Inorg. Chem. 2001, 40, 1734-1744.
24. Feng, T. L.; Gurian, P. L.; Healy, M. D.; Barron, A. R. Inorg. Chem. 1990, 29, 408-411.
25. Deacon, G. B.; Philips, R. J. Coord. Chem. Rev. 1980, 33, 227-250.
26. (a) Lakatos, A.; Banyai, I.; Decock. P.; Kiss, T. Eur. J. Inorg. Chem. 2001, 461-469.
27. (b) Jackson, G. E. Polyhedron 1990, 163-170.
28. (c) Taylor, M. J. Polyhedron 1990, 9, 207-214.
29. (d) Venturini, M.; Berthon, G. J. Inorg. Biochem. 1989, 37, 69-90.
30. (e) Öhman, L.-O. Inorg. Chem. 1988, 27, 2565-2570.
31. (f) Gregor, J. E.; Powell, H. K. J. Aust. J. Chem. 1986, 39, 1854-1864.
32. (g) Motekaitis, R. J.; Martell, A. E. Inorg. Chem. 1984, 23, 18-23.
33. (h) Öhman, L.-O.; Sjöberg, S. J. J. Chem. Soc., Dalton Trans. 1983, 2513-2517.
34. Harris, W. R.; Martell, A. E. Inorg. Chem. 1976, 15, 713-720.
35. Hodgkins, P. S.; Prasher, V.; Farrar, G.; Armstrong, R.; Sturman, S.; Corbett, J.; Blair, J. A. Neuro Report 1993, 5, 23-24.
36. Roskams, A. J.; Connor, J. R. Proc. Natl. Acad. Sci. U.S.A. 1990, 87, 9024-2027.