Multiple-spin effects in fast magic angle spinning Lee-Goldburg cross-polarization experiments in uniformly labeled compounds

Journal of Chemical Physics

Volumn 118, Issue 12, 2003, Pages 5547-5557

  Ladizhansky, V ^a,c   Vinogradov, E ^a   Van Rossum, B J ^b,d   De Groot, H J M ^b   Vega, S ^a  

^a WEIZMANN INSTITUTE OF SCIENCE   (Israel)

^b LEIDEN UNIVERSITY   (Netherlands)

^c MASSACHUSETTS INSTITUTE OF TECHNOLOGY   (United States)

^d FMP   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

COMPUTER SIMULATION; HAMILTONIANS; HYDROCARBONS; NUMERICAL METHODS; OSCILLATIONS; PROTONS; QUANTUM THEORY;

HIGH SPINNING FREQUENCY; MULTIPLE SPIN EFFECTS; PROTON POLARIZATION; ZERO QUANTUM DIPOLAR INTERACTION TERMS;

NUCLEAR MAGNETIC RESONANCE;

EID: 0037461028     PISSN: 00219606     EISSN: None     Source Type: Journal    
DOI: 10.1063/1.1517299     Document Type: Article

References (33)

1. A. Pines, M. G. Gibby, and J. S. Waugh, J. Chem. Phys. 59, 569 (1973).
2. E. R. Andrew, A. Bradbury, and R. G. Eads, Nature (London) 183, 1802 (1959).
3. I. J. Lowe, Phys. Rev. Lett. 2, 285 (1959).
4. M. Mehring, A. Pines, W.-K. Rhim, and J.S. Waugh J. Chem. Phys. 54, 3239 (1971).
5. A. E. Bennett, C. M. Rienstra, M. Auger, K. V. Lakshmi, and R. G. Griffin, J. Chem. Phys. 103, 6951 (1995).
6. D. E. Demco, J. Tegenfeldt, and J. S. Waugh, Phys. Rev. B 11, 4133 (1975).
7. M. H. Levitt, D. Suter, and R. R. Ernst, J. Chem. Phys. 84, 4243 (1986).
8. B. H. Meier, Chem. Phys. Lett. 188, 201 (1992).
9. D. Marks and S. Vega, J. Magn. Reson. Ser. A 118, 157 (1996).
10. S. Ray, V. Ladizhansky, and S. Vega, J. Magn. Reson. 135, 237 (1998).
11. B.-J. van Rossum, C. P. de Groot, V. Ladizhansky, S. Vega, and H. J. M. de Groot, J. Am. Chem. Soc. 122, 3465 (2000).
12. V. Ladizhansky and S. Vega, J. Chem. Phys. 112, 7158 (2000).
13. M. Lee and W. I. Goldburg, Phys. Rev. A 140, 1261 (1965).
14. S. R. Hartmann and E. L. Hahn, Phys. Rev. 128, 2042 (1962).
15. P. R. Costa, Ph.D. thesis, Massachusetts Institute of Technology, 1997.
16. M. Hohwy, C. M. Rienstra, C. P. Jaroniec, and R. G. Griffin, J. Chem. Phys. 110, 7983 (1999).
17. A. Brinkmann, M. Eden, and M. H. Levitt, J. Chem. Phys. 112, 8539 (2000).
18. B. Luy and S. J. Glaser, J. Magn. Reson. 142, 280 (2000).
19. P. Hodgkinson and L. Emsley, J. Magn. Reson. 139, 46 (1999).
20. E. Vinogradov, P. K. Madhu, and S. Vega, Chem. Phys. Lett. 314, 443 (1999).
21. E. Vinogradov, P. K. Madhu, and S. Vega, Chem. Phys. Lett. 329, 207 (2000).
22. E. Vinogradov, P. K. Madhu, and S. Vega, J. Chem. Phys. 115, 8983 (2001).
23. M. Mehring and J. S. Waugh, Phys. Rev. B 5, 3459 (1972).
24. A. Bielecki, A. C. Kolbert, and M. H. Levitt, Chem. Phys. Lett. 155, 341 (1989).
25. A. G. Redfield and S. D. Kunz, J. Magn. Reson. 19, 250 (1975).
26. M. Bak, J. T. Rasmussen, and N. C. Nielsen, J. Magn. Reson. 147, 296 (2000).
27. M. Veshtort and R. G. Griffin (unpublished).
28. A. E. Bennett, R. G. Griffin, and S. Vega, in NMR Basic Principles and Progress Springer-Verlag, Berlin, (1994), Vol. 33.
29. A. Wokaun and R. R. Ernst, J. Chem. Phys. 67, 1752 (1977).
30. S. Vega, J. Chem. Phys. 68, 5518 (1978).
31. L. D. Landau and E. M. Lifshitz, Quantum Mechanics, 3rd ed., Course of Theoretical Physics, edited by L. D. Landau and E. M. Lifshtitz (Pergamon, Oxford, 1981), Vol. 3.
32. M. N. Frey, T. F. Koetzle, M. S. Lehmann, and W. C. Hamilton, J. Chem. Phys. 58, 2547 (1973).
33. See EPAPS Document No. E-JCPSA6-117-014245 for the LG-CP build-up curves of the carbon signals. A direct link to this document may be found in the online article's HTML reference section. The document may also be reached via the EPAPS homepage (http://www.aip.org/pubservs/epaps.html) or from tfp.aip.org. in the directory /epaps/. See the EPAPS homepage for more information.