Synthesis, characterization and crystal structure of a phenol-functionalized diazamesocyclic derivative with unexpected configuration

Journal of Molecular Structure

Volumn 646, Issue 1-3, 2003, Pages 191-196

  Guo, Ya Mei ^a   Du, Miao ^b   Bu, Xian He ^b  

^a TIANJIN UNIVERSITY   (China)

^b NANKAI UNIVERSITY   (China)

Author keywords

1,4 Diazacycloheptane; Configuration; Crystal structure; Synthesis

Indexed keywords

1,4 BIS(3 TERT BUTYL 5 METHYL 2 HYDROXYBENZYL) 1,4 DIAZACYCLOHEPTANE; 2 TERT BUTYL PARA CRESOL; COORDINATION COMPOUND; CYCLOHEPTANE DERIVATIVE; HEXAHYDRO 1,4 DIAZEPINE; PHENOL DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CIS TRANS ISOMERISM; CRYSTAL STRUCTURE; CRYSTALLOGRAPHY; HYDROGEN BOND; INFRARED SPECTROSCOPY; MANNICH REACTION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLID STATE; SYNTHESIS; X RAY DIFFRACTION;

EID: 0037453990     PISSN: 00222860     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-2860(02)00711-1     Document Type: Article

References (20)

1. D.O. Nielson, M.L. Larsen, R.D. Wallett, J.I. Legg, J. Am. Chem. Soc. 93 (1971) 5079.
2. D.K. Mills, J.H. Reibenspies, M.Y. Darensbourg, Inorg. Chem. 29 (1990) 4364.
3. W.K. Musker, Coord. Chem. Rev. 117 (1992) 133.
4. C.A. Grapperhaus, M.Y. Darensbourg, Acc. Chem. Res. 31 (1998) 451.
5. J.A. Halfen, J.M. Uhan, D.C. Fox, M.P. Mehn, L. Que Jr, Inorg. Chem. 39 (2000) 4913.
6. X.H. Bu, M. Du, Z.L. Shang, R.H. Zhang, D.Z. Liao, M. Shionoya, T. Clifford, Inorg. Chem. 39 (2000) 4190.
7. X.H. Bu, M. Du, L. Zhang, Z.L. Shang, R.H. Zhang, M. Shionoya, J. Chem. Soc. Dalton Trans. (2001) 729.
8. X.H. Bu, M. Du, Z.L. Shang, L. Zhang, Q.H. Zhao, R.H. Zhang, M. Shionoya, Eur. J. Inorg. Chem. (2001) 1551.
9. M. Du, X.H. Bu, G.C. Wang, Y.M. Guo, R.H. Zhang, Inorg. Chim Acta 320 (2001) 192.
10. M. Du, X.H. Bu, Q. Xu, Z.L. Shang, R.H. Zhang, J. Chem. Crystallogr. 30 (2000) 531.
11. M. Du, Y.M. Guo, X.H. Bu, J. Ribas, M. Monfort, New J. Chem. 26 (2002) 939.
12. Y.M. Guo, M. Du, X.H. Bu, J. Mol. Struct. 610 (2002) 27.
13. X.H. Bu, M. Du, L. Zhang, D.Z. Liao, J.K. Tang, R.H. Zhang, M. Shionoya, J. Chem. Soc. Dalton Trans. (2001) 593.
14. M. Du, Z.L. Shang, X.B. Leng, X.H. Bu, Polyhedron 20 (2001) 3065.
15. M. Du, Y.M. Guo, X.H. Bu, J. Ribas, M. Monfort, New J. Chem. 26 (2002) 645.
16. M. Du, X.H. Bu, Y.M. Guo, L. Zhang, D.Z. Liao, J. Ribas, Chem. Commun. (2002) 1478.
17. Bruker AXS, SAINT Software Reference Manual, Madison, WI, 1998.
18. G.M. Sheldrick, SHELXTL NT Version 5.1. Program for Solution and Refinement of Crystal Structures, University of Göttingen, Germany, 1997.
19. Y.M. Guo, M. Du, G.C. Wang, X.H. Bu, J. Mol. Struct. (2002) 643-677.
20. Y. Sasada, Molecular and Crystal Structures, Chemistry Handbook, third ed., The Chemical Society of Japan, Maruzen, Tokyo, 1984.