Boron trifluoride-methanol complex - Mild and powerful reagent for deprotection of labile acetylated amines

Tetrahedron Letters

Volumn 44, Issue 11, 2003, Pages 2301-2303

  Miltsov, Serguei ^a   Rivera, Laia ^a   Encinas, Cristina ^a   Alonso, Julián ^a  

^a UNIVERSITAT AUTÒNOMA DE BARCELONA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

ACETIC ACID DERIVATIVE; AMINE; BORON DERIVATIVE; CYANINE DYE; FLUORIDE; METHANOL;

ACETYLATION; ARTICLE; COLUMN CHROMATOGRAPHY; DEPROTECTION REACTION;

EID: 0037430648     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(03)00271-5     Document Type: Article

References (10)

1. Greene T.W., Wuts P.G.M. Protective Groups in Organic Synthesis. 1991;309-406 Wiley.
2. Lipowska M., Patonay G., Strekowski L. Synth. Commun. 23:(21):1993;3087-3094.
3. Mujumdar R.B., Ernst L.A., Mujumdar S.R., Waggoner A.S. Cytometry. 10:1989;11-19.
4. Ernst L.A., Ravinder K.G., Ratnakar B.M., Waggoner A.S. Cytometry. 10:1989;3-10.
5. Puyol M., Miltsov S., Salinas I., Alonso J. Anal. Chem. 74:2002;570-576.
6. Sihlbom L. Acta Chem. Scand. 8:1954;529-530.
7. The synthesis of acetylated aminodye 1 was performed according to Ref. 2; acetylated dye 2: Miltsov, S.; Encinas, C.; Alonso, J. Tetrahedron Lett. 1999, 40, 4067-4068; dye 3: Strekowski, L.; Lipowska, M.; Patonay, G. J. Org. Chem. 1992, 57, 4578; dyes 4-6: Miltsov, S.; Encinas, C.; Alonso, J. Tetrahedron Lett. 2001, 42, 6129-6131.
8. The synthesis of acetylated aminodye 1 was performed according to Ref. 2; acetylated dye 2: Miltsov, S.; Encinas, C.; Alonso, J. Tetrahedron Lett. 1999, 40, 4067-4068; dye 3: Strekowski, L.; Lipowska, M.; Patonay, G. J. Org. Chem. 1992, 57, 4578; dyes 4-6: Miltsov, S.; Encinas, C.; Alonso, J. Tetrahedron Lett. 2001, 42, 6129-6131.
9. The synthesis of acetylated aminodye 1 was performed according to Ref. 2; acetylated dye 2: Miltsov, S.; Encinas, C.; Alonso, J. Tetrahedron Lett. 1999, 40, 4067-4068; dye 3: Strekowski, L.; Lipowska, M.; Patonay, G. J. Org. Chem. 1992, 57, 4578; dyes 4-6: Miltsov, S.; Encinas, C.; Alonso, J. Tetrahedron Lett. 2001, 42, 6129-6131.
10. max=835 nm.