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0012984885
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note
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2 indicate the conformation of calix[4]arene: a pair of doublets between 3.0 and 4.5 ppm in proton NMR with Δδ around 0.9 ppm and one carbon NMR signal at 31 ppm is consistent with all the cone conformation calix[4]arenes.
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20
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0013018853
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note
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+ reference electrode. Ferrocene is used as an external standard.
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22
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0001505211
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