Synthesis and solid-state NMR studies of P-vinylbenzylphosphonic acid

Chemistry - A European Journal

Volumn 9, Issue 3, 2003, Pages 770-775

  Frantz, Richard ^a   Durand, Jean Olivier ^a   Carré, Francis ^a   Lanneau, Gérard F ^a   Le Bideau, Jean ^a   Alonso, Bruno ^b   Massiot, Dominique ^b  

^a UNIVERSITÉ DE MONTPELLIER   (France)

^b Centre National de la Recherche Scientifique   (France)

Author keywords

NMR spectroscopy; Phosphonic acid; Structure elucidation; Styrene

Indexed keywords

CRYSTALLIZATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHASE TRANSITIONS; SYNTHESIS (CHEMICAL); X RAY CRYSTALLOGRAPHY;

HETERONUCLEAR CORRELATION;

ORGANIC ACIDS;

4 VINYLBENZYLPHOSPHONIC ACID; PHOSPHONIC ACID DERIVATIVE; STYRENE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; CORRELATION ANALYSIS; CRYSTALLIZATION; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; SOLID STATE; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 0037416023     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/chem.200390086     Document Type: Article

References (31)

1. a) A. M. El-Naggar, A. S. Emara, S. G. Abdalla, J. Appl. Polym. Sci. 1997, 65, 1091;
2. b) S. D. Alexandratos, M. E. Bates, Macromolecules 1988, 21, 2905;
3. c) B. Boutevin, H. Bachar, J. P. Parisi, B. Améduri, Eur. Polym. J. 1996, 32, 159;
4. d) G. Alberti, in Comprehensive Supramolecular Chemistry, Vol. 7 (Ed.: J.-M. Lehn, J. L. Atwood, J. E. D. Davies, D. D. MacNinol, F. Vögtle, Pergamon, Oxford, 1996, pp. 151-187;
5. e) F. Fredoueil, V. Penicaud, M. Bujoli-Doeuff, B. Bujoli, Inorg. Chem. 1997, 36, 4702;
6. f) F. Fredoueil, M. Evain, M. Bujoli-Doeuff, B. Bujoli, Eur. J. Inorg. Chem. 1999, 1077;
7. g) P. Bonhôte, J. E. Moser, R. Humphry-Backer, N. Vlachopoulos, S. M. Zakeeruddin, L. Walder, M. Grätzel, J. Am. Chem. Soc. 1999, 121, 1324;
8. h) A. G. Neff, N. M. Helfrich, M. C. Clifton, C. J. Page, Chem. Mater. 2000, 12, 2363;
9. i) C. Maillet, P. Janvier, M. Pipelier, T. Praveen, Y. Andres, B. Bujoli, Chem. Mater. 2001, 13, 2879;
10. j) R. Frantz. J. O. Durand, G. F. Lanneau, J. C. Jumas, O.-J. Fourcade, M. Cretin, M. Persin, Eur. J. Inorg. Chem. 2002, 1088.
11. a) L. H. Merwin, W. A. Dollase, G. Hägele, H. Blum, Phosphorus, Sulfur, Silicon 1991, 56, 117;
12. b) R. K. Harris, L. H. Merwin. G. Hägele, J. Chem. Soc. Faraday Trans. 1 1989, 85, 1409;
13. c) R. K. Harris, P. Jackson, L. H. Merwin, B. J. Say, G. Hägele, J. Chem. Soc. Faraday Trans. 1 1988, 84, 3649;
14. d) R. K. Harris, L. H. Merwin. G. Hägele, Magn. Res. Chem. 1989, 27, 470;
15. e) G. Ohms, K. Krüger, A. Rabis, V. Kaiser, Phosphorus Sulfur Silicon Relat. Elem. 1996, 114, 75.
16. a) E. Vinogradov, P. K. Madhu, S. Vega, Chem. Phys. Lett. 1999, 314, 443;
17. b) D. Sakellariou, A. Lesage, P. Hodgkinson. L. Emsley, Chem. Phys. Lett, 2000, 319, 253;
18. c) A. Lesage, L. Duma, D. Sakellariou, L. Emsley, J. Am. Chem. Soc. 2001, 123, 5747;
19. d) P. K. Madhu, X. Zhao, M. H. Levitt, Chem. Phys. Lett. 2001, 346, 142.
20. a) B. J. van Rossum, H. Forster, J. H. de Groot, J. Magn. Reson. 1997, 124, 516;
21. b) A. Lesage, D. Sakalleriou, S. Steuernagel, L. Emsley, J. Am. Chem. Soc. 1998, 120, 13194.
22. a) V. Ladizhansky, G. Hodes, S. Vega, J. Phys. Chem. B 2000, 104, 1939;
23. b) D. Massiot, B. Alonso, F. Fayon, F. Fredoueil, B. Bujoli Solid State Sci. 2001, 3, 11.
24. M. Anbar, G. A. St. John, A. C. Scott, J. Dent. Res. 1974, 867.
25. R. R. Holmes, R. O. Day, Y. Yoshida, J. M. Holmes, J. Am. Chem. Soc. 1992, 114, 1771.
26. D. Massiot, F. Fayon, M. Capron, I. King, S. Le Calvé, B. Alonso, J. O. Durand, B. Bujoli, Z. Gan, G. Hoatson. Magn. Reson. Chem. 2002, 40, 70.
27. 31P signals along the F1 (vertical) and F2 (horizontal) dimensions, respectively.
28. M. Lee, W. I. Golburg, Phys Rev. A 1965, 140, 1261.
29. A. Bielecki, A. C. Kolbert, M. H. Levitt, Chem. Phys. Lett. 1989, 155, 341.
30. E. Brunner, U. Sternberg, Prog. Nucl. Magn. Reson. Spectrosc. 1998, 32, 21.
31. G. Metz, X. Wu, S. O. Smith, J. Magn. Reson. A 1994, 11, 219.