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0346602981
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note
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2| data. All non-hydrogen atoms were refined anisotropically. Hydrogen atoms were treated as idealized contributions. Scattering factors and anomalous dispersion coefficients are contained in the SHELXTL 5.03 program library (G. M. Sheldrick, Madison, WI). CCDC-182287 (3), CCDC-182288 (4), and CCDC-190997 (5) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit @ccdc.cam.ac.uk).
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0032476842
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23
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0346602980
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Utrecht University, Utrecht, The Netherlands, A. L. Spek
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The accessible void volumes were calculated with the program PLATON by using a probe with a radius of 1.2 Å. A. M. C. T. PLATON, Utrecht University, Utrecht, The Netherlands, A. L. Spek, 1998.
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PLATON
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24
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0345971608
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note
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II complexes, generated in exactly the same manner, indicate that the materials are isomorphous with 5.
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25
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0347232727
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note
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x, which forms a tightly packed herringbone pattern and contains no channels or cavities; details will be reported in due course.
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26
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0347232724
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note
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-1.
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27
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0347232726
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note
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Ball-and-stick and space-filling diagrams were prepared using DIAMOND-Visual Crystal Structure Information System CRYSTAL IMPACT, Postfach 1251, 53002 Bonn.
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