Crystalline transition behaviors of nylons 12 20 and 10 20

European Polymer Journal

Volumn 39, Issue 6, 2003, Pages 1133-1140

  Huang, Yue ^a   Li, Weihua ^a   Yan, Deyue ^a  

^a SHANGHAI JIAO TONG UNIVERSITY   (China)

Author keywords

Brill transition; Nylons 12 20 and 10 20; Real time FT IR; Variable temperature WAXD

Indexed keywords

ANNEALING; CRYSTAL STRUCTURE; CRYSTALLIZATION; FOURIER TRANSFORM INFRARED SPECTROSCOPY; HYDROGEN BONDS; PHASE TRANSITIONS; SYNTHESIS (CHEMICAL); THERMAL EXPANSION; X RAY DIFFRACTION ANALYSIS;

CRYSTALLINE TRANSITION;

NYLON POLYMERS;

EID: 0037410016     PISSN: 00143057     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0014-3057(02)00376-2     Document Type: Article

References (30)

1. Bunn C.W., Garner E.V. The crystal structures of the polyamide (nylons). Proc. R. Soc. (London). 189A:1947;3279.
2. Brill R. Über Beziehungen zwischen der Struktur der Polyamide und der des Seidenfibroins. Z. Phys. Chem. B. 53:1943;61.
3. Jones N.A., Atkins E.D.T., Hill M.J., Cooper S.J., Franco L. Chain-folded lamellar crystals of aliphatic polyamides, comparisons between nylons 4 4, 6 4, 8 4, 10 4, and 12 4. Macromolecules. 29:1996;6011.
4. Jones N.A., Atkins E.D.T., Hill M.J. Investigation of solution-crown, chain-folded lamellar crystals of the even-even nylons: 6 6, 8 6, 8 8, 10 6, 10 8, 10 10, 12 6, 12 8, 12 10, and 12 12. J. Polym. Sci., Polym. Phys. 38:2000;1209.
5. Jones N.A., Atkins E.D.T., Hill M.J. Comparison of structures and behavior on heating of solution-grown, chain-folded lamellar crystals of 31 even-even nylons. Macromolecules. 33:2000;2642.
6. Jones N.A., Atkins E.D.T., Hill M.J., Cooper S.J., Franco L. Chain-folded lamellar crystals of aliphatic polyamides. Investigation of nylons 4 8, 4 10, 4 12, 6 10, 6 12, 6 18 and 8 12. Polymer. 38:1997;2689.
7. Biangardi H.J. Brill transition of polyamide 6 12. J. Macromol. Sci. - Phys. B29(2&3):1990;139.
8. Jones N.A., Cooper S.J., Atkins E.D.T., Hill M.J., Franco L. Temperature-induced changes in chain-folded lamellar crystals of aliphatic polyamides. Investigation of nylons 2 6, 2 8, 2 10, and 2 12. J. Polym. Sci., Polym. Phys. 35:1997;675.
9. Ramesh C. New crystalline transition in nylon 4 6, 6 10 and 6 12 using high-temperature X-ray diffraction studies. Macromolecules. 32:1999;3721.
10. Radusch H.T., Stolp M., Androsch R. Structure and temperature-induced changes of various polyamides. Polymer. 35:1994;3568.
11. Brill R. Beziehungen zwischen wasserstoffbindung und einigen eigenschaften von polyamiden. Makromol. Chem. 18/19:1956;2940.
12. Colclough M.L. Polymorphism in nylon 6 6. J. Mater. Sci. 13:1978;2531.
13. Murthy N.S., Curran S.A., Aharoni S.M., Minor H. Premelting crystalline relaxations and phase transitions in nylon 6 and 6 6. Macromolecules. 24:1991;3215.
14. 1 H NMR Macromolecules. 23:1990;2153.
15. Yan D.Y., Li Y.J., Zhu X.Y. Brill transition in nylon 10 12 investigated by variable temperature XRD and real time FT-IR. Macromol. Rapid Commun. 21:2000;1040.
16. Li Y.J., Zhu X.Y., Tian G.H., Yan D.Y., Zhou E.L. Multiple melting endotherms in melt-crystallized nylon 10 12. Polym. Int. 50:2001;677.
17. Li Y.J., Yan D.Y., Zhu X.Y., Jiang X.L. The Brill transition of nylon 10 12. J. Chin. Univ. Chem. 20:2000;983.
18. Ehrenstein M., Sikorski P., Atkins E., Smith P. Structures of X 34-nylons in chain-folded lamellae and gel-spun fibers. J. Polym. Sci., Polym. Phys. 40:2002;2685.
19. Ehrenstein M., Dellsperger S., Kocher C., Stutzmann N., Weder C., Smith P. New polyamides with long alkane segments: nylon 6.24 and 6.34. Polymer. 41:2000;3531.
20. Brandrup J., Immergnt E.H. Polymer handbook. 2nd ed. 1975;Wiley, NewYork.
21. Huang Y, Li WH, Yan DY. Preparation and characterization of a series of polyamides with long alkylene segments: nylons 12 20, 10 20, 8 20, 6 20, 4 20 and 2 20. Polym Bull, in press.
22. Miyake A. Infrared spectra and crystal structure of polyamides. J. Polym. Sci. 10:1960;223.
23. Matsubara I., Magill J.H. An infrared study of the interaction of polyamides with iodine in iodine-potassium iodide solution. Polymer. 7:1966;199.
24. Skrovanek D.J., Painter P.C., Coleman M.M. Hydrogen bonding in polymers. 2. Infrared temperature studies of nylon 11. Macromolecules. 19:1986;699.
25. Coleman M.M., Lee K.H., Skrovanek D.J., Painter P.C. Hydrogen bonding in polymers. 4. Infrared temperature studies of a simple polyurethane. Macromolecules. 19:1986;2149.
26. Cooper S.J., Coogan M., Everall N., Priestnall I. A polarised μ-FTIR study on a model system for nylon 6 6: implications for the nylon Brill structure. Polymer. 42:2001;10119.
27. Vasanthan N., Murthy N.S., Bray R.G. Investigation of Brill transition in nylon 6 and nylon 6 6 by infrared spectroscopy. Macromolecules. 31:1998;8433.
28. Sandeman I., Keller A. Crystallinity studies of polyamides by infrared, specific volume and X-ray methods. J. Polym. Sci. 19:1956;401.
29. Jakeš J., Krimm S. A valence force field for the amide group. Spectrochim. Acta. 27A:1971;19.
30. Garcia D., Starkweather H.W. Hydrogen bonding in nylon 6 6 and model compounds. J. Polym. Sci. 23:1985;537.