Multianvil high-pressure/high-temperature preparation, crystal structure, and properties of the new oxoborate β-ZnB4O7

Solid State Sciences

Volumn 5, Issue 2, 2003, Pages 281-289

  Huppertz, Hubert ^a   Heymann, Gunter ^a  

^a UNIVERSITY OF MUNICH   (Germany)

Author keywords

Borates; Crystal structure; High pressure; Multianvil; ZnB4O7

Indexed keywords

CRYSTAL STRUCTURE; HIGH PRESSURE EFFECTS; HIGH TEMPERATURE EFFECTS; SINGLE CRYSTALS; X RAY DIFFRACTION ANALYSIS;

OXOBORATE COMPOUNDS;

BORATE MINERALS;

BORIC ACID; BORON DERIVATIVE; OXYGEN; ZINC DERIVATIVE; ZINC OXIDE;

ARTICLE; CHEMICAL ANALYSIS; CLASSIFICATION; CRYSTAL STRUCTURE; HIGH TEMPERATURE; INFRARED SPECTROSCOPY; POWDER; PRESSURE; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0037319794     PISSN: 12932558     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1293-2558(02)00057-2     Document Type: Article

References (69)

1. P. Becker, Adv. Mater. 10 (1998) 979.
2. T. Sasaki, Y. Mori, M. Yoshimura, Y.K. Yap, T. Kamimura, Mater. Sci. Eng. 30 (2000) 1.
3. D.A. Keszler, Curr. Opin. Solid State Mater. Sci. 1 (1996) 204.
4. H. Huppertz, B. von der Eltz, J. Am. Chem. Soc. 124 (2002) 9376.
5. H. Huppertz, unpublished results.
6. H. Emme, H. Huppertz, Z. Anorg. Allg. Chem. 628 (2002) 2165.
7. 9 (Ln = Eu, Gd, Tb) [6].
8. H. Bauer, Z. Anorg. Allg. Chem. 320 (1963) 306.
9. C.E. Weir, R.A. Schroeder, J. Res. Nat. Bur. Stand. 86A (1964) 465.
10. M. Martinez-Ripoll, S. Martinez-Carrera, S. Garcia-Blanco, Acta Crystallogr., Sect. B 27 (1971) 672.
11. P. Smith, S. Garcia-Blanco, L. Rivoir, Z. Krist. 115 (1961) 460.
12. P. Smith, S. Garcia-Blanco, L. Rivoir, Z. Krist. 119 (1964) 375.
13. P. Smith-Verdier, S. Garcia-Blanco, Z. Krist. 151 (1980) 175.
14. E. Ingerson, G.W. Morey, O.F. Tuttle, Amer. J. Sci. 246 (1948) 31.
15. N.A. Toropov, P.F. Konovalov, Doklady Akad. Nauk SSSR 66 (1949) 1105.
16. H.E. Swanson, E. Tatge, J. Res. Nat. Bur. Stand. 46 (1951) 318.
17. D.E. Harrison, F.A. Hummel, J. Electrochem. Soc. 103 (1956) 491.
18. Yu.S. Leonov, Doklady Akad. Nauk SSSR 114 (1957) 976.
19. S. Garcia-Blanco, J. Fayos, Z. Krist. 127 (1968) 145.
20. A. Whitaker, J. Mater. Sci. 7 (1972) 189.
21. W.T.A. Harrison, T.E. Gier, G.D. Stucky, Angew. Chem. 105 (1993) 788, Angew. Chem. Int. Ed. 32 (1993) 724.
22. W.T.A. Harrison, T.E. Gier, G.D. Stucky, Angew. Chem. 105 (1993) 788, Angew. Chem. Int. Ed. 32 (1993) 724.
23. S. Luger, J. Felsche, P. Fischer, Acta Crystallogr., Sect. C 43 (1987) 1.
24. H. Huppertz, Z. Naturforsch. 56b (2001) 697.
25. D. Walker, M.A. Carpenter, C.M. Hitch, Am. Mineral. 75 (1990) 1020.
26. D. Walker, Am. Mineral. 76 (1991) 1092.
27. D.C. Rubie, Phase Trans. 68 (1999) 431.
28. P.-E. Wemer, L. Eriksson, M. Westdahl, J. Appl. Crystallogr. 18 (1985) 367.
29. POW Software, STOE & CIE GmbH, Darmstadt, 1998.
30. W. Herrendorf, H. Bärnighausen, HABITUS, Program for Numerical Absorption Correction, University of Karlsruhe/Gieβen, Germany, 1993/1997.
31. A.L. Spek, PLATON - A Multipurpose Crystallographic Tool, Utrecht University, Utrecht, Netherlands, 2002.
32. G.M. Sheldrick, SHELXS-97, Program for the Solution of Crystal Structures, University of Göttingen, Germany, 1997.
33. G.M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, University of Göttingen, Germany, 1997.
34. A. Neuhaus, Chimia 18 (1964) 93.
35. G.E. Gurr, P.W. Montgomery, C.D. Knutson, B.T. Gorres, Acta Crystallogr., Sect. B 26 (1970) 906.
36. C.T. Prewitt, R.D. Shannon, Acta Crystallogr., Sect. B 24 (1968) 869.
37. J.R. Clark, Am. Mineral. 49 (1964) 1549.
38. J.A. Konnert, J.R. Clark, C.L. Christ, Am. Mineral. 55 (1970) 1911.
39. S. Ghose, C. Wan, Am. Mineral. 62 (1977) 979.
40. A. Perloff, S. Block, Acta Cryst. 20 (1966) 274.
41. D.L. Corker, A.M. Glazer, Acta Crystallogr., Sect. B 52 (1996) 260.
42. W.E. Klee, Z. Kristallogr. 179 (1987) 67.
43. A. Beukemann, W.E. Klee, Z. Kristallogr. 209 (1994) 709.
44. A. Beukemann, W.E. Klee, Z. Kristallogr. 201 (1992) 37.
45. G. Thimm, S. Schumacher, W. Uhr, W.E. Klee, TOPOLAN - Topological Analysis of Crystal Structures, Universität Karlsruhe, 1993.
46. F.C. Hawthorne, P.C. Bums, J.D. Grice, in: E.S. Grew, L.M. Anovitz (Eds.), Boron: Mineralogy, Petrology, and Geochemistry, Mineralogical Society of America, Washington, 1996, Chap. 2, Reviews in Mineralogy 33.
47. A.D. Negro, L. Ungaretti, Am. Mineral. 56 (1971) 1553.
48. E. Ketatni, B. Memari, F. Abraham, O. Mentre, J. Solid State Chem. 153 (2000) 48.
49. G. Schäfer, H. Borrmann, R. Kniep, Z. Anorg. Allg. Chem. 627 (2001) 61.
50. K. Bluhm, C.H. Park, Z. Naturforsch. 52B (1997) 102.
51. P.C. Bums, J.D. Grice, F.C. Hawthorne, Can. Mineral. 33 (1995) 1131.
52. J.D. Grice, P.C. Bums, F.C. Hawthorne, Can. Mineral. 37 (1999) 731.
53. P. Becker, Z. Kristallogr. 216 (2001) 523.
54. R. Hoppe, Angew. Chem. 78 (1966) 52, Angew. Chem. Int. Ed. Engl. 5 (1966) 95.
55. R. Hoppe, Angew. Chem. 78 (1966) 52, Angew. Chem. Int. Ed. Engl. 5 (1966) 95.
56. R. Hoppe, Angew. Chem. 82 (1970) 7, Angew. Chem. Int. Ed. Engl. 9 (1970) 25.
57. R. Hoppe, Angew. Chem. 82 (1970) 7, Angew. Chem. Int. Ed. Engl. 9 (1970) 25.
58. R. Hoppe, R. Hübenthal, MAPLE, Program for the Calculation of MAPLE-Values, Vers. 4, University of Gieβen, 1993.
59. E.H. Kisi, M.M. Elcombe, Acta Crystallogr., Sect. C 45 (1989) 1867.
60. I.D. Brown, D. Altermatt, Acta Crystallogr., Sect. B 41 (1985) 244.
61. N.E. Brese, M. O'Keeffe, Acta Crystallogr., Sect. B 47 (1985) 192.
62. R. Hoppe, S. Voigt, H. Glaum, J. Kissel, H.P. Müller, K. Bemet, J. Less-Common Met. 156 (1989) 105.
63. M. Ren, J.H. Lin, Y. Dong, L.Q. Yang, M.Z. Su, L.P. You, Chem. Mater. 11 (1999) 1576.
64. J.P. Laperches, P. Tarte, Spectrochim. Acta 22 (1966) 1201.
65. G. Blasse, G.P.M. van den Heuvel, Phys. Stat. Sol. 19 (1973) 111.
66. W.C. Steele, J.C. Decius, J. Chem. Phys. 25 (1956) 1184.
67. R. Böhlhoff, H.U. Bambauer, W. Hoffmann, Z. Kristallogr. 133 (1971) 386.
68. K. Machida, H. Hata, K. Okuno, G. Adachi, J. Shiokawa, J. Inorg. Nucl. Chem. 41 (1979) 1425.
69. 3-II was obtained as a single-phase (JCPDS: 76-781), coarsely crystalline, colorless solid (yield: 30 mg per run).