Evaluation of cyclodextrins as chiral selectors in the separation of selected monoterpenes by capillary liquid chromatography and capillary electrophoresis

Journal of Liquid Chromatography and Related Technologies

Volumn 26, Issue 4, 2003, Pages 505-516

  Diagone, C A ^a   Ogawa, C A ^a   Lancas F M ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

Capillary electrophoresis; Capillary liquid chromatography; Citrus; Cyclodextrins; Monoterpenes

Indexed keywords

ELECTROPHORESIS; ISOMERS; ORGANIC COMPOUNDS; STEREOCHEMISTRY;

OPTICAL ISOMERS;

LIQUID CHROMATOGRAPHY;

BETA CYCLODEXTRIN; BETA PINENE; CARVONE; CITRAL; CYCLODEXTRIN; LINALOOL; PINENE; TERPENE;

ARTICLE; CAPILLARY ZONE ELECTROPHORESIS; CHEMICAL STRUCTURE; CHIRALITY; CHROMATOGRAPHY; CITRUS FRUIT; ISOMER; LIQUID CHROMATOGRAPHY; MICELLAR ELECTROKINETIC CHROMATOGRAPHY; NONHUMAN; STEREOCHEMISTRY;

CITRUS;

EID: 0037282920     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-120017895     Document Type: Article

References (13)

1. Cotroneo, A.; d'Alcontres, I.S.; Trozzi, A. On the genuineness of citrus essential oils. Part XXXIV. Detection of added reconstituted bergamot oil in genuine bergamot essential oil by high resolution gas chromatography with chiral capillary columns. Flavour Fragr. J. 1992, 7, 15-17.
2. Lanças, F.M.; Galhiane, M.S. High-temperature capillary gas-chromatography (HT-CGC) determination of limonin in citrus juice. J. High Resolut. Chromatogr. 1990, 13 (9), 654-655.
3. Kallio, H.; Kerrola, K.; Alhonmäki, P. Carvone and limonene in caraway fruits (carum-carvi 1) analyzed by supercritical carbon-dioxide extraction gas-chromatography. J. Agric. Food Chem. 1994, 42 (11), 2478-2485.
4. Pala-Paul, J.; Perez-Alonso, M.J.; Velasco-Negueruela, A.; Sanz, J. Analysis by gas chromatography-mass spectrometry of the volatile components of ageratina adenophora spreng., growing in the canary islands. J. Chromatogr. A. 2002, 947 (2), 327-331.
5. McCalley, D.V.; Torres-Grifol, J.F. Analysis of volatiles from oranges in good and bad condition by gas-chromatography and gas-chromatography mass-spectrometry. Analyst 1992, 117 (4), 721-725.
6. Moshonas, M.G.; Shaw, P.E. Quantitative-determination of 46 volatile constituents in fresh, unpasteurized orange juices using dynamic headspace gas-chromatography. J. Agric. Food. Chem. 1994, 42 (7), 1525-1528.
7. Tang, Y.P.; Lou, F.C. Separation and isolation of terpene lactones from ginkgo biloba 1. by direct high performance liquid chromatography. J. Liq. Chromatogr. & Relat. Technol. 2000, 23 (18), 2897-2900.
8. Armstrong, D.W.; Zukowski, J. Direct enantiomeric resolution of monoterpene hydrocarbons via reversed-phase high-performance liquidchromatography with an alpha-cyclodextrin bonded stationary-phase. J. Chromatogr. A 1994, 666 (1-2), 445-448.
9. Zukowski, J. Enantiomeric resolution of alpha-pinene by HPLC with a chiral mobile phase additive. J. High Resolut. Chromatogr. 1991, 14 (5), 361-362.
10. Bazyl'chik, V.V.; Polyakova, N.P.; Sedel'nikov, A.I.; Ionova, E.A. Separation of some monoterpenic constituents of essential oils by gas-liquidchromatography. J. Chromatogr. 1982, 248 (2), 321-324.
11. Mondello, L.; Bartle, K.D.; Dugo, G.; Dugo, P. Automated HPLC-HRGC-a powerful method for essential oil analysis. 3. Aliphatic and terpene aldehydes of orange oil. J. High Resolut. Chromatogr. 1994, 17 (5), 312-314.
12. Gahm, K.H.; Chang, L.W.; Armstrong, D.W. Chiral separation of monoterpenes using mixtures of sulfated beta-cyclodextrins and alphacyclodextrin as chiral additives in the reversed-polarity capillary electrophoresis mode. J. Chromatogr. A 1997, 759 (1-2), 149-155.
13. Revilla, A.L.; Havel, J.; Jandik, P. Peak splitting observed during capillary electrophoresis of alpha- and beta-naphthols in borate buffer. J. Chromatogr. A 1996, 745 (1-2), 225-232.