(C2H10N2)[BPO4F2] - Structural relations between [BPO4F2]2- and [Si2O6]4-

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 629, Issue 1, 2003, Pages 3-5

  Huang, Ya Xi ^d   Schäfer, Gerd ^b   Borrmann, Horst ^d   Zhao, Jing Tai ^c   Kniep, Rüdiger ^a  

^a MAX PLANCK INSTITUTE FOR CHEMICAL PHYSICS OF SOLIDS   (Germany)

^b INM LEIBNIZ INSTITUTE FOR NEW MATERIALS   (Germany)

^c SHANGHAI INSTITUTE OF CERAMICS   (China)

^d NONE

Author keywords

Borophosphate; Fluorine substitution; Templates

Indexed keywords

BORON DERIVATIVE; CHEMICAL COMPOUND; ETHYLENEDIAMINE; FLUORINE DERIVATIVE; HYDROCARBON; HYDROCHLORIC ACID; PHOSPHATE; POLYANION; SILICATE;

ARTICLE; CRYSTAL STRUCTURE; ISOELECTRIC POINT; METHODOLOGY; SYNTHESIS;

EID: 0037259788     PISSN: 00442313     EISSN: None     Source Type: Journal    
DOI: 10.1002/zaac.200390015     Document Type: Article

References (13)

1. F. Liebau, Structural Chemistry of Silicates, Springer, Berlin, 1985.
2. B. Warren, W. L. Bragg, Z. Kristallogr. 1928, 69, 168.
3. M. Ozima, Acta Crystallogr. C 1983, 39, 1169.
4. D. W. J. Cruickshank, Acta Crystallogr. 1964, 17, 681.
5. F. C. Hawthorne, C. Calvo, J. Solid State Chem. 1977, 22, 157.
6. R. Kniep, H. Engelhardt, C. Hauf, Chem. Mater. 1998, 10, 2930.
7. I. Boy, C. Hauf, R. Kniep, Z. Naturforsch. 1998, 53 b, 631.
8. -3; b) G. M. Sheldrick, SHELXS 97-2, Program for the solution of crystal structures, Göttingen, 1997; c) G. M. Sheldrick, SHELXL 97-2, Program for the refinement of crystal structures, Göttingen, 1997; d) Further details on the crystal structure may be obtained from the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 172711. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax: int.code+(1223)336-033; e-mail: fileserv@ccdc.cam.ac.uk).
9. -3; b) G. M. Sheldrick, SHELXS 97-2, Program for the solution of crystal structures, Göttingen, 1997; c) G. M. Sheldrick, SHELXL 97-2, Program for the refinement of crystal structures, Göttingen, 1997; d) Further details on the crystal structure may be obtained from the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 172711. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax: int.code+(1223)336-033; e-mail: fileserv@ccdc.cam.ac.uk).
10. -3; b) G. M. Sheldrick, SHELXS 97-2, Program for the solution of crystal structures, Göttingen, 1997; c) G. M. Sheldrick, SHELXL 97-2, Program for the refinement of crystal structures, Göttingen, 1997; d) Further details on the crystal structure may be obtained from the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 172711. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax: int.code+(1223)336-033; e-mail: fileserv@ccdc.cam.ac.uk).
11. 19F π/2 pulse of 3 μs, an acquisition time of 16 ms, a dead time delay of 4.5 μs, and a recycle delay of 10 s; resonance frequency of 376.5 MHz. A total of 64 scans was accumulated. For results see text.
12. T. Steiner, Angew. Chem. 2002, 114, 50; Angew. Chem. Int. Ed. 2002, 41, 48.
13. T. Steiner, Angew. Chem. 2002, 114, 50; Angew. Chem. Int. Ed. 2002, 41, 48.