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Volumn 76, Issue 1, 2003, Pages 203-204

A novel approach to furopyrimidinones using dry media

Author keywords

[No Author keywords available]

Indexed keywords

CATALYST ACTIVITY; ENERGY TRANSFER; IRRADIATION; REACTION KINETICS; SYNTHESIS (CHEMICAL);

EID: 0037251083     PISSN: 00092673     EISSN: None     Source Type: Journal    
DOI: 10.1246/bcsj.76.203     Document Type: Article
Times cited : (33)

References (27)
  • 14
    • 0012865761 scopus 로고
    • Eu. Pat., 164268
    • M. P. Roer, Eu. Pat., 164268; Chem. Abstr., 105, 242726 (1986).
    • (1986) Chem. Abstr. , vol.105 , pp. 242726
    • Roer, M.P.1
  • 17
    • 0012868578 scopus 로고
    • R. G. Melik, Ogandzhanyan, A. S. Gapoyan, and V. E. Khachatryan, Sint. Geterosiki Soedin, 12, 24 (1981); Chem. Abstr., 95, 150553 (1981).
    • (1981) Chem. Abstr. , vol.95 , pp. 150553
  • 18
    • 0012881141 scopus 로고
    • Jpn Kokai Tokkyo Koho, 8168, 682
    • Sanyo Co. Ltd. Jpn Kokai Tokkyo Koho, 8168, 682; Chem. Abstr., 95, 132950 (1981).
    • (1981) Chem. Abstr. , vol.95 , pp. 132950
  • 20
    • 0012796827 scopus 로고    scopus 로고
    • note
    • Microwave irradiations were carried out in Kenstar microwave oven, Model No. OM9925E (2450 MHz, 800 Watts).
  • 24
    • 0012796828 scopus 로고    scopus 로고
    • note
    • To the solution of 1 (0.01 mol) and 2 (0.01 mol) in ethanol (∼10 mL) added basic alumina (20 g)/montomorillonite (15 g) with constant stirring. The mixture was air dried at room temperature, placed in an alumina bath and subjected to MWI for 1.3 min/4 min respectively.
  • 25
    • 0012809692 scopus 로고    scopus 로고
    • note
    • To the solution of 1 (0.01 mol) and 2 (0.01 mol) in ethanol (∼10 mL) added montmorillonite K-10 clay (15 g) with constant stirring, air dried. Then placed in an alumina bath and subjected to MWI for 4 min. Upon formation of the intermediate (3) as observed by TLC, the solution of acyl chloride in ethanol was added to the same solid support with stirring, air dried and further subjected to MWI (approx. bulk temperature reached ∼100-120 °C).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.