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To the solution of 1 (0.01 mol) and 2 (0.01 mol) in ethanol (∼10 mL) added basic alumina (20 g)/montomorillonite (15 g) with constant stirring. The mixture was air dried at room temperature, placed in an alumina bath and subjected to MWI for 1.3 min/4 min respectively.
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25
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0012809692
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note
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To the solution of 1 (0.01 mol) and 2 (0.01 mol) in ethanol (∼10 mL) added montmorillonite K-10 clay (15 g) with constant stirring, air dried. Then placed in an alumina bath and subjected to MWI for 4 min. Upon formation of the intermediate (3) as observed by TLC, the solution of acyl chloride in ethanol was added to the same solid support with stirring, air dried and further subjected to MWI (approx. bulk temperature reached ∼100-120 °C).
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