Synthesis and characterization of nickel(II) complexes of benzoic acid and methyl substituted benzoic acid hydrazides and x-ray structure of Ni[C6H5CONHNH2]3Cl 2·3CH3OH

Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry

Volumn 33, Issue 2, 2003, Pages 205-221

  Odunola, O A ^a   Adeoye, I O ^b   Woods, J A O ^b   Gelebe, A C ^a  

^a UNIVERSITY OF LIMPOPO   (South Africa)

^b UNIVERSITY OF IBADAN   (Nigeria)

Author keywords

Electronic; Hydrazides; Infrared; Magnetic; Microbiology; Nickel; X ray

Indexed keywords

ANTIFUNGAL AGENT; ANTIINFECTIVE AGENT; BENZOIC ACID; BENZOIC ACID DERIVATIVE; CARBONYL DERIVATIVE; CHELATING AGENT; CHLORIDE ION; HYDRAZIDE DERIVATIVE; LIGAND; METHANOL; METHYL GROUP; NICKEL COMPLEX; NITROGEN; OXYGEN;

ANTIBACTERIAL ACTIVITY; ANTIFUNGAL ACTIVITY; ARTICLE; CRYSTAL STRUCTURE; DRUG ACTIVITY; DRUG STRUCTURE; DRUG SYNTHESIS; INFRARED SPECTROSCOPY; MAGNETISM; NONHUMAN; REFLECTOMETRY; ROOM TEMPERATURE; SOLVATION; SUBSTITUTION REACTION; X RAY DIFFRACTION;

EID: 0037222908     PISSN: 00945714     EISSN: None     Source Type: Journal    
DOI: 10.1081/SIM-120017781     Document Type: Article

References (34)

1. Tabakova, S.; Dodoff, N. Effect of platinum(II) complexes of 4-methoxy- and 4-chlorobenzoic acid hydrazides on Saccharomyces cerevisae. Z. Naturforsch. 1997, 52C, 45-48.
2. Kushev, D.N.; Spassovska, N.C.; Taxirov, S.I.; Grancharov, K.C. Cytotoxicity of aromatic and cycloalkane carboxylic acid hydrazides. Z. Naturforsch. 1997, 52C, 49-54.
3. Dodoff, N.; Grancharov, K.; Spassovska, N. Platinum(II) complexes of benzoic and 3-methoxybenzoic acid hydrazides. Synthesis, characterisation and cytotoxic effect. J. Inorg. Biochem. 1994, 54, 221-223.
4. Dodoff, N.; Grancharov, K.; Spassovska, N. Platinum(II) complexes of 4-methoxy- and 4-chlorobenzoic acid hydrazides. Synthesis, characterisation and cytotoxic effect. J. Inorg. Biochem. 1995, 60, 257-266.
5. Tabakova, S.; Dodoff, N. Effect of platinum(II) complexes of benzoic and 3-methoxybenzoic acid hydrazides on Saccharomyces cerevisae. Z. Naturforsch. 1995, 50 C, 732-734.
6. Mamolo, M.G.; Falagiani, V.; Zampieri, D.; Vio, L.; Banfi, E. Synthesis and antimycobacterial activity of [5-(pyridin-2-yl)-1,3,4-thiadiazol-2-ylthio]acetic acid arylidenehydrazide derivatives. Farmaco 2001, 56 (8), 587-592.
7. Gürsoy, A.; Terzioglu, N.; Otuk, G. Synthesis of new hydrazides-hydrazones, thiosemicarbazides and thiazaolidinones as possible antimicrobials. Eur. J. Med. Chem. 1997, 32, 753-757.
8. Rando, D.G.; Sato, D.N.; Siqueira, L.; Malvezzi, A.; Leite, C.Q.F.; do Amaral, A.T.; Ferreira, E.I.; Tavares, L. Potential tuberculostatic agents. Topliss application on benzoic acid [(5-nitro-thiophen-2-yl)-methylene]hydrazide series. Bioorg. Med. Chem. 2002, 10, 557-560.
9. Rollas, S.; Gulerman, N.; Erdeniz, H. Synthesis and antimicrobial activity of some new hydrazones of 4-fluorobenzoic acid hydrazide and 3-acetyl-2,5-disubstituted-1,3,4-oxadiazolines. Farmaco 2002, 57, 171-174.
10. Zubareva, G.I.; Adeev, S.U.; Radushev, A.V., Gomzikov, A.I.; Zubarev, M.P. Treatment of wastewaters to remove metal ions by flotation with hydrazides of aliphatic carboxylic acid. Russ. J. Appl. Chem. 1998, 71 (2), 283-287.
11. Zubareva, G.I.; Adeev, S.U.; Radushev, A.V.; Gomzikov, A.I.; Zubarev, M.P. Treatment of wastewaters to remove metal ions by flotation with hydrazides of aliphatic carboxylic acid. Chem. Abstr. 1998, 129, 112811d.
12. Shen, X.; Giese, R.W. Hydrazide as a ligand moiety in immobilized metal ion affinity chromatography: separation of BO-IMI and BODIPY-hydrazide. J. Chromatogr., A 1997, 777, 261-265.
13. Lunn, G.; Phillips, L.R.; Pacula-Cox, C. Reversed-phase high-perfomance liquid chromatography of 4-(2-pyridyl)-1-piperazinethiocarboxylic acid 2-[1-(pyridyl)ethylidene]hydrazide dihydrochloride (NSC 348977), a synthetic thiosemicarbazone with antitumor activity. J. Chromatogr., B 1998, 708, 217-222.
14. Gad, A.M.; El-Dissouky, A.; Mansour, E.M.; El-Maghraby, A. Thermal stability of poly-acryloyl benzoic acid hydrazide and its complexes with some transition metals. Polym. Degrad. Stab. 2000, 68, 153-158.
15. Aleman, C.; Puiggali, J. Conformational preferences of the 1,2-hydrazine dicarboxylic acid dimethylester. A comparison with the hydrazide analogue. J. Mol. Struct., Theochem. 2001, 541, 179-183.
16. Ahmed, A.D.; Chaudhuri, N.R. Acid hydrazides as ligands. III. Metal complexes of acetylhydrazide and benzohydrazides. J. Inorg. Nucl. Chem. 1971, 33, 189-201.
17. 2. Synth. React. Inorg. Met.-Org. Chem. 2002, 22 (4), 801-817.
18. Sorenson, J.R.J. Metal Ions in Biological Systems; Sigel, H., Ed.; Marcel Dekker: New York, 1982; Vol. 14, 77.
19. David, L.; Rusu, M.; Cozar, O.; Rusu, D.; Todica, M.; Balan, C. Spectroscopic and magnetic investigations of some transition metal complexes with N-4-methoxyphenyl-N-4-chlorobenzoyl hydrazides as ligand. J. Mol. Struct. 1999, 482,483, 148-152.
20. Vogel's Textbook of Quantitative Inorganic Analysis; Bassett, J., Denney, R.C., Jeffery, G.H., Mendham, J., Eds.; Longman Scientific and Technical: London; 1986; 316-322.
21. Earnshaw, A. The Introduction to Magnetochemistry; Academic Press: London; 1968; 80-86.
22. Sheldrick, G.M. SHELXL 97, Program for Crystal Structure Refinement; University of Göttingen, Germany, 1997.
23. International Tables for X-Ray Crystallography; Kynoch Press: Birmingham, 1974; Vol. 3.
24. Silverstein, R.M.; Webster, F.X. Spectrometric Identification of Organic Compounds, 6th Ed.; John Wiley and Sons Inc., 1998; 73-109.
25. Pavia, D.L.; Lampman, G.M.; Kriz, G.S. Introduction to Spectroscopy, 2nd Ed.; Saunders College Publishing, 1996; 14-85.
26. Holland, J.M.; Kilner, C.A.; Thornton-Pett, M.; Halcrow, M.A. Steric effects on the electronic and molecular structures of nickel(II) and cobalt(II) 2,6-dipyrazol-1-ylpyridine complexes. Polyhedron 2001, 20, 2829-2840.
27. Sacconi, L. Electronic Structure and Stereochemistry of Nickel(II). In Transition Metal Chemistry, A Series of Advances; Carlin, R.L., Ed.; Edward Arnold Ltd.: London, 1968, Vol. 4, 199-298.
28. Lever, A.B.P. Inorganic Electronic Spectroscopy, 4th Ed.; Elsevier: London, 1986; 481-579.
29. Higgs, T.C.; Carrano, C.J. A new class of biomimetically relevant "scorpionate" ligands. 2. The (2-hydroxyphenyl)bis(pyrazoly)-methanes. Structural characterization of a series of mono-, di-, and trinuclear nickel(II) complexes. Inorg. Chem. 1997, 36, 298-306.
30. Manonmani, J.; Thirumuruhan, R.; Kandaswamy, M.; Narayanan, V.; Raj, S.S.; Ponnuswamy, M.N.; Shanmugam, G.; Fun, H.K. Synthesis of copper(II) and nickel(II) complexes using compartmental ligands: x-ray, electrochemical and magnetic studies. Polyhedron 2001, 20, 3039-3048.
31. Hart, S.M.; Boyens, J.C.A.; Hancock, R.D. Mixing of states and the determination of ligand-field parameters for high-spin octahedral complexes of nickel(II). Electronic spectrum and structure of bis(1,-7-diaza-4-thiaheptane)nickel(II) perchlorate. Inorg. Chem. 1983, 22, 982-986.
32. Greenwood, N.N.; Earnshaw, A. Chemistry of the Elements, 2nd Ed.; Butterworths and Heinemann, 1997; 1193.
33. Carcelli, M.; Ianelli, S.; Mavilla, L.; Pelizzi, C.; Pelizzi, G. Synthesis and spectroscopic characterization of bivalent metal complexes of 2,6-diacetylpyridinebis(octanoylhydrazone). X-ray crystal structure of a nickel(II) complex. Inorg. Chim. Acta 1996, 245, 43-49.
34. Kücükgüzel, S.G.; Oruc, E.E.; Rollas, S.; Şahin, F.; Özbek, A. Synthesis, characterization and biological activity of novel 4-thiazolidinones, 1,3,4-oxadiazoles and some related compounds. Eur. J. Med. Chem. 2002, 37, 197-206.