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2 were selected under a microscope in a glove box and sealed into glass capillaries. The quality of the crystal was checked with some rotation pictures. The crystal structure solution and refinement were performed with the SHELXTL (G. M. Sheldrick, Göttingen 1997) program package. Further details of the crystal structure investigations may be obtained from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen, Germany (fax: (+49)7247-808-666, e-mail: crysdata@fiz-karlsruhe.de), on quoting the depository number CSD-412665.
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