메뉴 건너뛰기




Volumn 54, Issue 1-3, 2002, Pages 357-368

Enantiomeric determination of amlodipine in human plasma by liquid chromatography coupled to tandem mass spectrometry

Author keywords

1 acid glycoprotein; Amlodipine; Enantiomer separation; Solid phase extraction; Tandem mass spectrometry

Indexed keywords

ACETIC ACID; AMLODIPINE; AMMONIUM ACETATE; BUFFER; ION; METHANOL; OROSOMUCOID; PROPANOL; PROPRANOLOL; SILICON DIOXIDE; WATER;

EID: 0037207253     PISSN: 0165022X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0165-022X(02)00133-1     Document Type: Article
Times cited : (85)

References (44)
  • 2
    • 0026012842 scopus 로고
    • Amlodipine. A review of its pharmacodynamic and pharmacokinetic properties, and therapeutic use in cardiovascular disease
    • Murdoch D., Heel R.C. Amlodipine. A review of its pharmacodynamic and pharmacokinetic properties, and therapeutic use in cardiovascular disease. Drugs. 41:1991;478-505.
    • (1991) Drugs , vol.41 , pp. 478-505
    • Murdoch, D.1    Heel, R.C.2
  • 3
    • 0022552815 scopus 로고
    • Long-acting dihydropyridine calcium antagonists: 1. 2-Alkylmethyl derivatives incorporating basic substituents
    • Arrowsmith J.E., Campbell F., Cross E., Stubbs J.K., Burges R.A., Gardiner D.G.et al. Long-acting dihydropyridine calcium antagonists: 1. 2-Alkylmethyl derivatives incorporating basic substituents. J. Med. Chem. 29:1986;1696-1702.
    • (1986) J. Med. Chem. , vol.29 , pp. 1696-1702
    • Arrowsmith, J.E.1    Campbell, F.2    Cross, E.3    Stubbs, J.K.4    Burges, R.A.5    Gardiner, D.G.6
  • 4
    • 0026662745 scopus 로고
    • Determination of the absolute configuration of the active amlodipine enantiomer as (-)-S: A correction
    • Goldmann S., Stoltefuss J., Born L. Determination of the absolute configuration of the active amlodipine enantiomer as (-)-S: a correction. J. Med. Chem. 35:1992;3341-3344.
    • (1992) J. Med. Chem. , vol.35 , pp. 3341-3344
    • Goldmann, S.1    Stoltefuss, J.2    Born, L.3
  • 5
    • 0029057787 scopus 로고
    • Detection and determination of total amlodipine by high-performance thin-layer chromatography: A useful technique for pharmacokinetics studies
    • Pandya K.K., Satia M., Gandhi T.P., Modi I.A., Modi R.I., Chakravarthy B.K. Detection and determination of total amlodipine by high-performance thin-layer chromatography: a useful technique for pharmacokinetics studies. J. Chromatogr., B. 667:1995;315-320.
    • (1995) J. Chromatogr., B , vol.667 , pp. 315-320
    • Pandya, K.K.1    Satia, M.2    Gandhi, T.P.3    Modi, I.A.4    Modi, R.I.5    Chakravarthy, B.K.6
  • 8
    • 0024956735 scopus 로고
    • Analysis of amlodipine in serum by a sensitive high-performance liquid chromatographic method with amperometric detection
    • Shimooka K., Sawada Y., Tatematsu H. Analysis of amlodipine in serum by a sensitive high-performance liquid chromatographic method with amperometric detection. J. Pharm. Biomed. Anal. 7:1989;1267-1272.
    • (1989) J. Pharm. Biomed. Anal. , vol.7 , pp. 1267-1272
    • Shimooka, K.1    Sawada, Y.2    Tatematsu, H.3
  • 9
    • 0028846832 scopus 로고
    • Sensitive high-performance liquid chromatographic analysis of amlodipine in human plasma with amperometric detection and a single-step solid-phase sample preparation
    • Josefsson M., Zackrisson A.-L., Norlander B. Sensitive high-performance liquid chromatographic analysis of amlodipine in human plasma with amperometric detection and a single-step solid-phase sample preparation. J. Chromatogr., B. 672:1995;310-313.
    • (1995) J. Chromatogr., B , vol.672 , pp. 310-313
    • Josefsson, M.1    Zackrisson, A.-L.2    Norlander, B.3
  • 10
    • 0029737994 scopus 로고    scopus 로고
    • Quantitative determination of amlodipine in serum by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry
    • Yasuda T., Tanaka M., Iba K. Quantitative determination of amlodipine in serum by liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry. J. Mass Spectrom. 31:1996;879-884.
    • (1996) J. Mass Spectrom. , vol.31 , pp. 879-884
    • Yasuda, T.1    Tanaka, M.2    Iba, K.3
  • 11
    • 0028237563 scopus 로고
    • Enantioselective gas chromatographic assay with electron-capture detection for amlodipine in biological samples
    • Scharpf F., Riedel K.-D., Laufen H., Leitold M. Enantioselective gas chromatographic assay with electron-capture detection for amlodipine in biological samples. J. Chromatogr., B. 655:1994;225-233.
    • (1994) J. Chromatogr., B , vol.655 , pp. 225-233
    • Scharpf, F.1    Riedel, K.-D.2    Laufen, H.3    Leitold, M.4
  • 12
    • 0027076203 scopus 로고
    • Evaluation of six chiral stationary phases in LC for their selectivity towards drug enantiomers
    • Vandenbosch C., Massart D.L., Lindner W. Evaluation of six chiral stationary phases in LC for their selectivity towards drug enantiomers. J. Pharm. Biomed. Anal. 10:1992;895-908.
    • (1992) J. Pharm. Biomed. Anal. , vol.10 , pp. 895-908
    • Vandenbosch, C.1    Massart, D.L.2    Lindner, W.3
  • 13
    • 0025316762 scopus 로고
    • Enantioselective determination of felodipine and other chiral dihydropyridine calcium entry blockers in human plasma
    • Soons P.A., Roosemalen M.C.M., Breimer D.D. Enantioselective determination of felodipine and other chiral dihydropyridine calcium entry blockers in human plasma. J. Chromatogr. 528:1990;343-356.
    • (1990) J. Chromatogr. , vol.528 , pp. 343-356
    • Soons, P.A.1    Roosemalen, M.C.M.2    Breimer, D.D.3
  • 14
    • 0027212618 scopus 로고
    • Determination of felodipine enantiomers using chiral stationary phase liquid chromatography and gas chromatography/mass spectrometry, and the study of their pharmacokinetic profiles in human and dog
    • Sakamoto T., Ohtake Y., Itoh M., Tabata S., Kuriki T., Uno K. Determination of felodipine enantiomers using chiral stationary phase liquid chromatography and gas chromatography/mass spectrometry, and the study of their pharmacokinetic profiles in human and dog. Biomed. Chromatogr. 7:1993;99-103.
    • (1993) Biomed. Chromatogr. , vol.7 , pp. 99-103
    • Sakamoto, T.1    Ohtake, Y.2    Itoh, M.3    Tabata, S.4    Kuriki, T.5    Uno, K.6
  • 15
    • 0026566014 scopus 로고
    • Determination of manidipine enantiomers in human serum using chiral chromatography and column-switching liquid chromatography
    • Yamaguchi M., Yamashita K., Aoki I., Tabata T., Hirai S., Yashiki T. Determination of manidipine enantiomers in human serum using chiral chromatography and column-switching liquid chromatography. J. Chromatogr. 575:1992;123-129.
    • (1992) J. Chromatogr. , vol.575 , pp. 123-129
    • Yamaguchi, M.1    Yamashita, K.2    Aoki, I.3    Tabata, T.4    Hirai, S.5    Yashiki, T.6
  • 16
    • 0028917610 scopus 로고
    • Determination of felodipine, its enantiomers, and a pyridine metabolite in human plasma by capillary gas chromatography with mass spectrometric detection
    • Dru J.D.-Y., Hsieh J.Y.-K., Matuszewski B.K., Dobinska M.R. Determination of felodipine, its enantiomers, and a pyridine metabolite in human plasma by capillary gas chromatography with mass spectrometric detection. J. Chromatogr., B. 666:1995;259-267.
    • (1995) J. Chromatogr., B , vol.666 , pp. 259-267
    • Dru, J.D.-Y.1    Hsieh, J.Y.-K.2    Matuszewski, B.K.3    Dobinska, M.R.4
  • 17
    • 0027256704 scopus 로고
    • Simultaneous assessment of the intravenous and oral disposition of the enantiomers of racemic nimodipine by chiral stationary-phase high-performance liquid chromatography and gas chromatography/mass spectroscopy combined with stable isotope technique
    • Fischer C., Schonberger F., Mück W., Heuck K., Eichelbaum M. Simultaneous assessment of the intravenous and oral disposition of the enantiomers of racemic nimodipine by chiral stationary-phase high-performance liquid chromatography and gas chromatography/mass spectroscopy combined with stable isotope technique. J. Pharm. Sci. 82:1993;244-250.
    • (1993) J. Pharm. Sci. , vol.82 , pp. 244-250
    • Fischer, C.1    Schonberger, F.2    Mück, W.3    Heuck, K.4    Eichelbaum, M.5
  • 18
    • 0028340450 scopus 로고
    • Determination of the enantiomers of nisoldipine in human plasma using high-performance liquid chromatography on a chiral stationary phase and gas chromatography with mass-selective detection
    • Heinig R., Muschalek V., Ahr G. Determination of the enantiomers of nisoldipine in human plasma using high-performance liquid chromatography on a chiral stationary phase and gas chromatography with mass-selective detection. J. Chromatogr., B. 655:1994;286-292.
    • (1994) J. Chromatogr., B , vol.655 , pp. 286-292
    • Heinig, R.1    Muschalek, V.2    Ahr, G.3
  • 19
    • 0028226720 scopus 로고
    • Enantioselective assay for the determination of nisoldipine in dog, rat and mouse plasma by chiral microbore high-performance liquid chromatography combined with gas chromatography-mass spectrometry
    • Zimmer D., Muschalek V. Enantioselective assay for the determination of nisoldipine in dog, rat and mouse plasma by chiral microbore high-performance liquid chromatography combined with gas chromatography-mass spectrometry. J. Chromatogr., A. 666:1994;241-248.
    • (1994) J. Chromatogr., A , vol.666 , pp. 241-248
    • Zimmer, D.1    Muschalek, V.2
  • 20
    • 0035812962 scopus 로고    scopus 로고
    • Enantioselective assay of nisoldipine in human plasma by chiral high-performance liquid chromatography combined with gas chromatographic-mass spectrometry: Applications to pharmacokinetics
    • Marques M.P., Santos N.A.G., Coelho E.B., Bonato and P.S., Lanchote V.L. Enantioselective assay of nisoldipine in human plasma by chiral high-performance liquid chromatography combined with gas chromatographic-mass spectrometry: applications to pharmacokinetics. J. Chromatogr., B. 762:2001;87-95.
    • (2001) J. Chromatogr., B , vol.762 , pp. 87-95
    • Marques, M.P.1    Santos, N.A.G.2    Coelho, E.B.3    Bonato and, P.S.4    Lanchote, V.L.5
  • 21
    • 0028183348 scopus 로고
    • Bioanalytics of nimodipine - An overview of methods
    • Mück W., Bode H. Bioanalytics of nimodipine - an overview of methods. Pharmazie. 49:1992;130-139.
    • (1992) Pharmazie , vol.49 , pp. 130-139
    • Mück, W.1    Bode, H.2
  • 22
    • 0028840510 scopus 로고
    • Enantiospecific determination of nimodipine in human plasma by liquid chromatography-tandem mass spectrometry
    • Mück W.M. Enantiospecific determination of nimodipine in human plasma by liquid chromatography-tandem mass spectrometry. J. Chromatogr., A. 712:1995;45-53.
    • (1995) J. Chromatogr., A , vol.712 , pp. 45-53
    • Mück, W.M.1
  • 23
    • 0037080673 scopus 로고    scopus 로고
    • Enantioselective determination of felodipine in human plasma by chiral normal-phase liquid chromatography and electrospray ionisation mass spectrometry
    • Lindmark B., Ahnoff M., Persson B.A. Enantioselective determination of felodipine in human plasma by chiral normal-phase liquid chromatography and electrospray ionisation mass spectrometry. J. Pharm. Biomed. Anal. 27:2002;489-495.
    • (2002) J. Pharm. Biomed. Anal. , vol.27 , pp. 489-495
    • Lindmark, B.1    Ahnoff, M.2    Persson, B.A.3
  • 24
    • 0028918956 scopus 로고
    • Stereoselective pharmacokinetics of dihydropyridine calcium antagonists
    • Tokuma Y., Noguchi H. Stereoselective pharmacokinetics of dihydropyridine calcium antagonists. J. Chromatogr., A. 694:1995;181-193.
    • (1995) J. Chromatogr., A , vol.694 , pp. 181-193
    • Tokuma, Y.1    Noguchi, H.2
  • 25
    • 0031450345 scopus 로고    scopus 로고
    • Pharmacokinetic behaviour of R-(+)- and S-(-)-amlodipine after single enantiomer administration
    • Luksa J., Josic Dj., Kremser M., Kopitar Z., Milutinovic S. Pharmacokinetic behaviour of R-(+)- and S-(-)-amlodipine after single enantiomer administration. J. Chromatogr., B. 703:1997;185-193.
    • (1997) J. Chromatogr., B , vol.703 , pp. 185-193
    • Luksa, J.1    Josic, Dj.2    Kremser, M.3    Kopitar, Z.4    Milutinovic, S.5
  • 26
    • 0030296871 scopus 로고    scopus 로고
    • Coupled-column chromatography on a Chiral AGP phase for determination of amlodipine enantiomers in human plasma: An HPLC assay with electrochemical detection
    • Josefsson M., Norlander B. Coupled-column chromatography on a Chiral AGP phase for determination of amlodipine enantiomers in human plasma: an HPLC assay with electrochemical detection. J. Pharm. Biomed. Anal. 15:1996;267-277.
    • (1996) J. Pharm. Biomed. Anal. , vol.15 , pp. 267-277
    • Josefsson, M.1    Norlander, B.2
  • 27
    • 0030957177 scopus 로고    scopus 로고
    • Semi-preparative chromatographic purification of the enantiomers S-(-)-amlodipine and R-(+)-amlodipine
    • Luksa J., Josic Dj., Podobnik B., Furlan B., Kremser M. Semi-preparative chromatographic purification of the enantiomers S-(-)-amlodipine and R-(+)-amlodipine. J. Chromatogr., B. 693:1997;367-375.
    • (1997) J. Chromatogr., B , vol.693 , pp. 367-375
    • Luksa, J.1    Josic, Dj.2    Podobnik, B.3    Furlan, B.4    Kremser, M.5
  • 28
    • 0027076204 scopus 로고
    • Design of chiral LC separations for calcium antagonists on alpha 1-acid glycoprotein and ovomucoid columns
    • De Lorenzi E., Fell A.F., Caccialanza G., Massolini G., Kitsos M. Design of chiral LC separations for calcium antagonists on alpha 1-acid glycoprotein and ovomucoid columns. J. Pharm. Biomed. Anal. 10:1992;909-915.
    • (1992) J. Pharm. Biomed. Anal. , vol.10 , pp. 909-915
    • De Lorenzi, E.1    Fell, A.F.2    Caccialanza, G.3    Massolini, G.4    Kitsos, M.5
  • 29
    • 0034900515 scopus 로고    scopus 로고
    • Resolution of dihydropyridine calcium antagonist enantiomers using HPLC with ovoglycoprotein as chiral stationary phase
    • Fu Q., Matsunaga H., Haginaka J. Resolution of dihydropyridine calcium antagonist enantiomers using HPLC with ovoglycoprotein as chiral stationary phase. Anal. Sci. 17:2001;897-900.
    • (2001) Anal. Sci. , vol.17 , pp. 897-900
    • Fu, Q.1    Matsunaga, H.2    Haginaka, J.3
  • 30
    • 0028029917 scopus 로고
    • Enantioselective disposition of oral amlodipine in healthy volunteers
    • Laufen H., Leitold H. Enantioselective disposition of oral amlodipine in healthy volunteers. Chirality. 6:1994;531-536.
    • (1994) Chirality , vol.6 , pp. 531-536
    • Laufen, H.1    Leitold, H.2
  • 31
    • 0031790886 scopus 로고    scopus 로고
    • Enantioselective determination of isradipine in human serum using chiral stationary phase liquid chromatography and gas chromatography with nitrogen selective detection
    • Rask H.S., Angelo H.R., Christensen H.R. Enantioselective determination of isradipine in human serum using chiral stationary phase liquid chromatography and gas chromatography with nitrogen selective detection. Chirality. 10:1998;808-812.
    • (1998) Chirality , vol.10 , pp. 808-812
    • Rask, H.S.1    Angelo, H.R.2    Christensen, H.R.3
  • 32
    • 0029049286 scopus 로고
    • Determination of (+)- and (-)-nicardipine concentrations in human serum and their correlation with the antihypertensive effect oral administration of racemic nicardipine
    • Iwaoka T., Inotsume N., Inoue J., Naomi S., Okamoto Y., Higuchi S.et al. Determination of (+)- and (-)-nicardipine concentrations in human serum and their correlation with the antihypertensive effect oral administration of racemic nicardipine. Eur. J. Clin. Pharmacol. 48:1995;34-349.
    • (1995) Eur. J. Clin. Pharmacol. , vol.48 , pp. 34-349
    • Iwaoka, T.1    Inotsume, N.2    Inoue, J.3    Naomi, S.4    Okamoto, Y.5    Higuchi, S.6
  • 33
    • 0032736650 scopus 로고    scopus 로고
    • Automated sample preparation techniques for the determination of drug enantiomers in biological fluids using liquid chromatography with chiral stationary phases
    • Ceccato A., Toussaint B., Chiap P., Hubert Ph., Crommen J. Automated sample preparation techniques for the determination of drug enantiomers in biological fluids using liquid chromatography with chiral stationary phases. Enantiomer. 4:1999;305-315.
    • (1999) Enantiomer , vol.4 , pp. 305-315
    • Ceccato, A.1    Toussaint, B.2    Chiap, P.3    Hubert, Ph.4    Crommen, J.5
  • 34
    • 0032186343 scopus 로고    scopus 로고
    • Sample preparation for LC/MS/MS: Analyzing biological and environmental samples
    • Henion J., Brewer E., Rule G. Sample preparation for LC/MS/MS: analyzing biological and environmental samples. Anal. Chem. 70:1998;650A-656A.
    • (1998) Anal. Chem. , vol.70
    • Henion, J.1    Brewer, E.2    Rule, G.3
  • 35
    • 0030176327 scopus 로고    scopus 로고
    • High performance liquid chromatography enantioseparation of chiral pharmaceuticals using tris(chloro-methylphenylcarbamate)s of cellulose
    • Chankvetadze B., Chankvetadze L., Sidamonidze S., Yashima E., Okamoto Y. High performance liquid chromatography enantioseparation of chiral pharmaceuticals using tris(chloro-methylphenylcarbamate)s of cellulose. J. Pharm. Biomed. Anal. 14:1996;1295-1303.
    • (1996) J. Pharm. Biomed. Anal. , vol.14 , pp. 1295-1303
    • Chankvetadze, B.1    Chankvetadze, L.2    Sidamonidze, S.3    Yashima, E.4    Okamoto, Y.5
  • 36
    • 0026704392 scopus 로고
    • Immobilized proteins as chromatographic supports for chiral resolution
    • Narayanan S.R. Immobilized proteins as chromatographic supports for chiral resolution. J. Pharm. Biomed. Anal. 10:1992;251-262.
    • (1992) J. Pharm. Biomed. Anal. , vol.10 , pp. 251-262
    • Narayanan, S.R.1
  • 37
    • 0028931395 scopus 로고
    • Optimization of the separation of enantiomers of basic drugs. Retention mechanisms and dynamic modification of the chiral bonding properties on an alpha 1-acid glycoprotein column
    • Hermansson J., Grahn A. Optimization of the separation of enantiomers of basic drugs. Retention mechanisms and dynamic modification of the chiral bonding properties on an alpha 1-acid glycoprotein column. J. Chromatogr., A. 694:1995;57-69.
    • (1995) J. Chromatogr., A , vol.694 , pp. 57-69
    • Hermansson, J.1    Grahn, A.2
  • 38
    • 0032555720 scopus 로고    scopus 로고
    • Liquid chromatography-mass spectrometry in forensic and clinical toxicology
    • Maurer H.H. Liquid chromatography-mass spectrometry in forensic and clinical toxicology. J. Chromatogr., B. 713:1998;3-25.
    • (1998) J. Chromatogr., B , vol.713 , pp. 3-25
    • Maurer, H.H.1
  • 39
    • 0034306622 scopus 로고    scopus 로고
    • Enantiomeric determination of tramadol and its main metabolite O-desmethyltramadol in human plasma by liquid chromatography-tandem mass spectrometry
    • Ceccato A., Vanderbist F., Pabst J.-Y., Streel B. Enantiomeric determination of tramadol and its main metabolite O-desmethyltramadol in human plasma by liquid chromatography-tandem mass spectrometry. J. Chromatogr., B. 748:2000;65-76.
    • (2000) J. Chromatogr., B , vol.748 , pp. 65-76
    • Ceccato, A.1    Vanderbist, F.2    Pabst, J.-Y.3    Streel, B.4
  • 40
    • 0032559171 scopus 로고    scopus 로고
    • Advances in instrumentation in liquid chromatography-mass spectrometry and related liquid-introduction techniques
    • Niessen W.H.A. Advances in instrumentation in liquid chromatography-mass spectrometry and related liquid-introduction techniques. J. Chromatogr., A. 794:1998;407-435.
    • (1998) J. Chromatogr., A , vol.794 , pp. 407-435
    • Niessen, W.H.A.1
  • 42
    • 0031900683 scopus 로고    scopus 로고
    • Atmospheric pressure ionization LC/MS/MS techniques for drug disposition studies
    • Brewer E., Henion J. Atmospheric pressure ionization LC/MS/MS techniques for drug disposition studies. J. Pharm. Sci. 87:1998;395-402.
    • (1998) J. Pharm. Sci. , vol.87 , pp. 395-402
    • Brewer, E.1    Henion, J.2
  • 44
    • 0012667798 scopus 로고    scopus 로고
    • Guidance for industry, bionalytical method validation, US Department of Health and Human Services, Food and Drug Administration, Center for Drug Evaluation and Research (CDEC), Center for Veterinary Medicine (CVM), May 2001
    • Guidance for industry, bionalytical method validation, US Department of Health and Human Services, Food and Drug Administration, Center for Drug Evaluation and Research (CDEC), Center for Veterinary Medicine (CVM), May 2001.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.