First derivative ratio spectrophotometric, HPTLC-densitometric, and HPLC determination of nicergoline in presence of its hydrolysis - Induced degradation product

Journal of Pharmaceutical and Biomedical Analysis

Volumn 30, Issue 3, 2002, Pages 479-489

  Ahmad, Abdel Kader S ^a   Kawy, M Abdel ^a   Nebsen, M ^a  

^a CAIRO UNIVERSITY   (Egypt)

Author keywords

Basic or acidic degradation; Derivative ratio spectrophotometry; HPLC method; HPTLC; Nicergoline; Vasodilator

Indexed keywords

ACETIC ACID; ACETIC ACID ETHYL ESTER; CHLORPROMAZINE; METHANOL; NICERGOLINE; SILICA GEL;

ACCURACY; ARTICLE; DENSITOMETRY; DRUG DEGRADATION; DRUG DETERMINATION; DRUG HYDROLYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PERFORMANCE THIN LAYER CHROMATOGRAPHY; INSTRUMENT; INTERMETHOD COMPARISON; PRIORITY JOURNAL; STANDARD; TABLET FORMULATION; TECHNIQUE; ULTRAVIOLET SPECTROPHOTOMETRY; VALIDATION PROCESS;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DENSITOMETRY; HYDROLYSIS; NICERGOLINE; SPECTROPHOTOMETRY;

EID: 0037201653     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0731-7085(02)00132-2     Document Type: Article

References (44)

1. Martindale. The Complete Drug Reference. 32nd Edn:1999;Pharmaceutical Press, London.
2. Clarke E.G.C. Clarke's Isolation and Identification of Drugs in Pharmaceuticals, Body Fluids and Post-mortem Materials. second Edn:1986;The Pharmaceutical Press, London.
3. Banno K., Matsuoka M., Matsuo M., Kato J., Shimizu R., Kinumaki A. Iyakuhin Kenkyu. 20:(3):1989;621. Through Chem. Abst. (111), 180559f.
4. J. Vachek. Czech. CS; 236, 599, (1986). Through Chem. Abst. (106), 182777w.
5. J. Vachek. Czech. CS; 236, 599, (1986). Through Chem. Abst. (106), 182777w.
6. B. Trtik. Czech. CS; 239, 22, (1987). Through Chem. Abst. (110), 13664j.
7. B. Trtik. Czech. CS; 239, 22, (1987). Through Chem. Abst. (110), 13664j.
8. Kuhnert-Brandstaetter M., Geiler M., Wurian I. Sci. Pharm. 51:(1):1983;34-41. Through Chem. Abst. (99), 28089d.
9. Sturm J.C., Nunez-Vergara L.J., Squella J.A. Talanta. 39:(9):1992;1149-1154.
10. Radi A. Mikrochim. Acta. 132:(1):1999;49-53.
11. B. Trtik. Czech. CS; 232, 991, (1986). Through Chem. Abst. (107), 46426z.
12. B. Trtik. Czech. CS; 232, 991, (1986). Through Chem. Abst. (107), 46426z.
13. Fanali S., Fleiger M., Steinerova N., Nardi A. Electrophoresis. 13:(1-2):1992;39-43.
14. Halada P., Jegorov A., Ryska M., Havlicek V. Chem-Listy. 92:(7):1998;538. Through Anal. Abst.
15. Chen P., Tian Z., Digenis G.A., Tai H.H. Res. Commun. Mol. Pathol. Pharmacol. 92:(3):1996;315.
16. Pittner F., Gabor F., Hamilton G. Ger. Offen. DE. 4:1991;283.
17. Gabor F., Pittner F. Fresenius' J. Anal. Chem. 337:(1):1990;98.
18. Bizollon C.A., Rocher J.P., Chevalier P. Eur. J. Nucl. Med. 7:(7):1982;318.
19. Frank H., Heinish G., Neumayer E. Sci. Pharm. 54:(4):1986;305.
20. Evtushenko N.S., Popkov V.A., Fatova E.Y., Nechaeva Y.A., Rashetnyak V.Y., Azizov I.K. Farmatsiya. 39:(4):1990;36. Through Chem. Abst. (113), 158759r.
21. Schuetz H., Pielmeyer A., Weiler G. Aertzl. Lab. 36:(5):1990;113. Through Chem. Abst. (113), 110560s.
22. Cavazzutti G., Gagliardi L., Amato A., Profili M., Zagarese V., Tonelli D., Gattavecchia E. J. Chromatogr. 286:(3):1983;528.
23. Daldrup T., Rickert A. Fresenius Z. Anal. Chem. 334:(4):1989;349.
24. Banno K., Matsuoka M., Takahashi R. Chromatographia. 32:(3-4):1991;179.
25. Masumarra G., Scarlata G., Cirma G., Romano G., Palazzo S., Clementi S., Giulietti G. J. Chromatogr. 350:(1):1985;151.
26. Romano G., Caruso G., Masumarra G., Pavone D., Cruciani G. J. Planar Chromatog. Mod. TLC. 7:(3):1994;233.
27. Li J.Z., Zhao J. Yaowu-Fenxi-Zazhi. 20:(2):2000;124. Through Anal. Abst.
28. Flieger M., Sedmera P., Vokoun J., Rehacek Z., Stuchlik J., Cerny A. J. Chromatogr. 284:(1):1984;219.
29. Nieder M., Jaeger H. Z-Naturforsch. B: Anorg. Chem. Org. Chem. 42:(9):1987;1187.
30. Banno K., Horimoto S. Chromatographia. 31:(1-2):1991;50.
31. Banno K., Horimoto S., Mabuchi M. J. Chromatogr. Biomed. Appl. 106:(2):1991;375.
32. Yu J., Du C.B. Yaowu-Fenxi-Zazhi. 18:(2):1998;78. Through Anal. Abst.
33. Sioufi A., Sandrenan N., Godbillon J. Biomed. Chromatogr. 6:(1):1992;9.
34. Flieger M., Sinibaldi M., Cvak L., Castellani L. Chirality. 6:(7):1994;549.
35. Tesarova E., Zaruba K., Flieger M. J. Chromatogr.A. 844:(1-2):1999;137.
36. Farmitalia Carlo Erba Method; by personal communication.
37. ICH, Stability Testing of New Drug Substances and Products, International Conference on Harmonization, Geneva, October 1993.
38. Berzas Nevado J.J., Guiberteau Cabanillas C. Anal. Lett. 23:(11):1990;2077.
39. Morelli B. Talanta. 41:1994;673.
40. Morelli B. Anal. Lett. 27:(14):1994;2751.
41. Berzas Nevado J.J., Cuiberteau Cabanillas G., Salinas F. Talanta. 39:1992;547.
42. B. Renger. Proceeding of the Sixth International Symposium on Instrumental Planar Chromatography, Institute for Chromatography, Bad Duerkheim, 1991, p. 291.
43. Munson J.W. Pharmaceutical Analysis Modern Methods; PartB. 1984;Marcell Dekker, New York.
44. Brittain H.G. Valid. Anal. Methodol. 3:(3):1997;275.