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22
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0010733047
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note
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Focused microwave irradiations used in this study were generated by a Coherent Synthesis-Smith Workstation package (Personal Chemistry AB, Sweden).
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23
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0035961529
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For a theoretical study concerning the energetics of the various reaction intermediates along the Magnus pathway see: Yamanaka M., Nakamura E. J. Am. Chem. Soc. 123:2001;1703.
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Yamanaka, M.1
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24
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0010733362
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note
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18OSi requires C, 71.60; H, 8.30%.
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25
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0010733048
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note
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1H NMR spectra after the crude reaction mixture was purified by flash column chromatography. No attempt was made to separate the diastereomers, however, the ratios given must be considered approximate.
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26
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0010648435
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note
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13C NMR spectroscopic techniques by microanalysis and/or high resolution mass spectroscopy.
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