메뉴 건너뛰기




Volumn 43, Issue 44, 2002, Pages 7953-7959

Preparation and properties of fluorenylidenephosphines bearing an electron-donating substituent, 2-alkoxy-4,6-di-t-butylphenyl or 2-(alkoxymethyl)-4,6-di-t-butylphenyl

Author keywords

Donors; Phosphaalkenes; Phosphorus compounds; Steric effects

Indexed keywords

[2,4 DI TERT BUTYL 6 (PHENOXYMETHYL)PHENYL](FLUORENYLIDENE)PHOSPHINE; CARBONYL DERIVATIVE; FUNCTIONAL GROUP; PHENYL GROUP; PHOSPHINE DERIVATIVE; PHOSPHORUS; TUNGSTEN DERIVATIVE; UNCLASSIFIED DRUG;

EID: 0037190876     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)01860-9     Document Type: Article
Times cited : (18)

References (40)
  • 5
    • 0001020381 scopus 로고    scopus 로고
    • For example, see; (a) Regitz, M.; Scherer, O. J. Multiple Bonds and Low Coordination in Phosphorus Chemistry; Georg Thieme Verlag: Stuttgart, 1990; (b) Yoshifuji, M. J. Organomet. Chem. 2000, 611, 210.
    • (2000) J. Organomet. Chem. , vol.611 , pp. 210
    • Yoshifuji, M.1
  • 26
    • 0010690098 scopus 로고    scopus 로고
    • 10b
    • 10b.
  • 28
    • 0034595255 scopus 로고    scopus 로고
    • A part of this work, including the preparation of 8d, was presented at the 78th National Meeting of the Chemical Society of Japan, Funabashi, March 2000, Abstr., No. 2G310. Recently, Oehme and co-workers reported the preparation of intramolecularly donor-stabilized silenes: (a) Mickoleit, M.; Schmohl, K.; Kempe, R.; Oehme, H. Angew. Chem., Int. Ed. 2000, 39, 1610; (b) Mickoleit, M.; Kempe, R.; Oehme, H. Chem. Eur. J. 2001, 7, 987.
    • (2000) Angew. Chem., Int. Ed. , vol.39 , pp. 1610
    • Mickoleit, M.1    Schmohl, K.2    Kempe, R.3    Oehme, H.4
  • 29
    • 0035793806 scopus 로고    scopus 로고
    • A part of this work, including the preparation of 8d, was presented at the 78th National Meeting of the Chemical Society of Japan, Funabashi, March 2000, Abstr., No. 2G310. Recently, Oehme and co-workers reported the preparation of intramolecularly donor-stabilized silenes: (a) Mickoleit, M.; Schmohl, K.; Kempe, R.; Oehme, H. Angew. Chem., Int. Ed. 2000, 39, 1610; (b) Mickoleit, M.; Kempe, R.; Oehme, H. Chem. Eur. J. 2001, 7, 987.
    • (2001) Chem. Eur. J. , vol.7 , pp. 987
    • Mickoleit, M.1    Kempe, R.2    Oehme, H.3
  • 30
    • 0010693226 scopus 로고    scopus 로고
    • note
    • 31P NMR spectroscopy. However, an attempted isolation of the corresponding compound failed. We tentatively assign the signal to [2,4-di-t-butyl-6-(dimethylamino)phenyl](9-fluorenylidene)phosphine.
  • 31
    • 0034838128 scopus 로고    scopus 로고
    • An analogous cyclization reaction has recently been reported: (a) Kobayashi, J.; Goto, K.; Kawashima, T. J. Am. Chem. Soc. 2001, 123, 3387; (b) Kobayashi, J.; Goto, K.; Kawashima, T.; Schmidt, M. W.; Nagase, S. J. Am. Chem. Soc. 2002, 124, 3703. See also, Ref. 12.
    • (2001) J. Am. Chem. Soc. , vol.123 , pp. 3387
    • Kobayashi, J.1    Goto, K.2    Kawashima, T.3
  • 32
    • 0037051626 scopus 로고    scopus 로고
    • See also, Ref. 12
    • An analogous cyclization reaction has recently been reported: (a) Kobayashi, J.; Goto, K.; Kawashima, T. J. Am. Chem. Soc. 2001, 123, 3387; (b) Kobayashi, J.; Goto, K.; Kawashima, T.; Schmidt, M. W.; Nagase, S. J. Am. Chem. Soc. 2002, 124, 3703. See also, Ref. 12.
    • (2002) J. Am. Chem. Soc. , vol.124 , pp. 3703
    • Kobayashi, J.1    Goto, K.2    Kawashima, T.3    Schmidt, M.W.4    Nagase, S.5
  • 36
    • 0010649356 scopus 로고    scopus 로고
    • note
    • w=0.151. Crystallographic data have been deposited at the Cambridge Crystallographic Data Centre (No. CCDC-190819).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.