Improved synthesis and X-ray crystal structure of pentafluorophenylcobalt tricarbonyl triphenylphosphine

Inorganica Chimica Acta

Volumn 340, Issue , 2002, Pages 221-224

  Gipson, Stephen L ^a   Bryson, Leslie A ^a   Klausmeyer, Kevin K ^a  

^a BAYLOR UNIVERSITY   (United States)

Author keywords

Carbonyl complexes; Cobalt(I) complexes; Pentafluorophenyl complexes

Indexed keywords

CHLORINE COMPOUNDS; CRYSTAL ATOMIC STRUCTURE; X RAY CRYSTALLOGRAPHY; X RAYS;

AXIAL POSITIONS; CARBONYL COMPLEXES; COBALT (I) COMPLEX; PENTAFLUOROPHENYL; TITLE COMPOUNDS; TRIGONAL BIPYRAMIDAL GEOMETRY; TRIPHENYL PHOSPHINES; X RAY CRYSTAL STRUCTURES;

COBALT COMPOUNDS;

CARBONYL DERIVATIVE; CHLORINE DERIVATIVE; COBALT COMPLEX; PENTAFLUOROBENZOYL CHLORIDE; PENTAFLUOROPHENYLCOBALT TRICARBONYLTRIPHENYLPHOSPHINE; TRIPHENYLPHOSPHINE; UNCLASSIFIED DRUG;

ARTICLE; CRYSTAL STRUCTURE; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 0037175588     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(02)01096-4     Document Type: Article

References (30)

1. Wojcicki A. Stone F.G.A., West R., Advances in Organometallic Chemistry. 11:1973;87 Academic Press, New York.
2. Galamb V., Pályi G. Coord. Chem. Rev. 59:1984;203.
3. Kovács I., Ungváry F. Coord. Chem. Rev. 161:1997;1.
4. Zucchi C., Cornia A., Boese R., Kleinpeter E., Alper H., Pályi G. J. Organomet. Chem. 586:1999;61.
5. Nagy-Gergely I., Szalontai G., Ungváry F., Markó L., Moret M., Sironi A., Zucchi C., Sisak A., Tschoerner C.M., Martinelli A., Sorkau A., Pályi G. Organometallics. 16:1997;2740.
6. Kovács I., Szalontai G., Ungváry F. J. Organomet. Chem. 524:1996;115.
7. Ungváry F., Markó L. Inorg. Chim. Acta. 227:1994;211.
8. Fernandez A.L., Prock A., Giering W.P. Organometallics. 13:1994;2767.
9. Amatore C., Bayachou M., Verpeaux J.-N., Pospísil L., Fiedler J. J. Electroanal. Chem. 387:1995;101.
10. McClellan W.R. J. Am. Chem. Soc. 83:1961;1598.
11. Hieber V.W., Beck W., Lindner E. Z. Naturforsch., T. B. 16:1961;229.
12. Mullica D.F., Sappenfield E.L., Gipson S.L., Wilkinson C.C. Acta Crystallogr., C. 53:1997;572.
13. J.B. Wilford, A. Forster, F.G.A. Stone, J. Chem. Soc. (1965) 6519.
14. J.B. Wilford, H.M. Powell, J. Chem. Soc. (A) (1967) 2092.
15. Galamb V., Pályi G., Cser F., Furmanova M.G., Struchkov Y.T. J. Organomet. Chem. 209:1981;183.
16. Galamb V., Pályi G., Boese R., Schmid G. Organometallics. 6:1987;861.
17. Ungváry F., Kovács I., Hammerschmitt B., Cordier G. Organometallics. 12:1993;2849.
18. C. Zucchi, R. Boese, K. Alberts, T. Herbrich, G. Tóth, L. Bencze, G. Pályi, Eur. J. Inorg. Chem. (2001) 2297.
19. Heck R.F., Breslow D.S. J. Am. Chem. Soc. 84:1962;2499.
20. Royo P., España N., Vazquez de Miguel A. Inorg. Synth. 23:1985;22.
21. CAD4 version 5.0 Structure Determination Package, Enraf-Nonius, Delft, The Netherlands, 1988
22. SHELXTL-PC, Siemens Analytical X-ray Instruments, Madison, WI, USA, 1989.
23. G.M. Sheldrick, SHELXL-97, University of Göttingen, Göttingen, Germany.
24. Ibers J.A., Hamilton W.C. International Tables for X-ray Crystallography. IV:1974;Kynoch, Birmingham, UK.
25. España N., Gomez P., Royo P., Vazquez de Miguel A. J. Organomet. Chem. 256:1983;141.
26. T. Blackmore, M.I. Bruce, F.G.A. Stone, J. Chem. Soc. (A) (1968) 2158.
27. R.L. Bennett, M.I. Bruce, R.C.F. Gardner, J. Chem. Soc., Dalton Trans. (1973) 2653.
28. Doucette W.J., Kim J., Kautz J.A., Gipson S.L. Inorg. Chim. Acta. 304:2000;237.
29. A.G. Orphen, L. Brammer, F.H. Allen, O. Kennard, D.G. Watson, R. Taylor, J. Chem. Soc., Dalton Trans. (1989) S1.
30. BIDICS, Bond Index of the Determination of Inorganic Crystal Structures, Institute for Materials Research, Hamilton, Canada, 1969-1981.