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6
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0027764253
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For leading references to previous syntheses of enantiomerically pure morphine, see: (a) Hong, C. Y.; Kado, N.; Overman, L. E. J. Am. Chem. Soc. 1993, 115, 11028. (b) White, J. D.; Hrnciar, P.; Stappenbeck, F. J. Org. Chem. 1997, 62, 5250. (c) Trauner, D.; Bats, J. W.; Werner, A.; Mulzer, J. J. Org. Chem. 1998, 63, 5908. (d) Nagata, H.; Miyazawa, N.; Ogasawara, K. Chem. Commun. 2001, 1094.
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(1993)
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Hong, C.Y.1
Kado, N.2
Overman, L.E.3
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7
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0030837809
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For leading references to previous syntheses of enantiomerically pure morphine, see: (a) Hong, C. Y.; Kado, N.; Overman, L. E. J. Am. Chem. Soc. 1993, 115, 11028. (b) White, J. D.; Hrnciar, P.; Stappenbeck, F. J. Org. Chem. 1997, 62, 5250. (c) Trauner, D.; Bats, J. W.; Werner, A.; Mulzer, J. J. Org. Chem. 1998, 63, 5908. (d) Nagata, H.; Miyazawa, N.; Ogasawara, K. Chem. Commun. 2001, 1094.
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J. Org. Chem.
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White, J.D.1
Hrnciar, P.2
Stappenbeck, F.3
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8
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0032555441
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For leading references to previous syntheses of enantiomerically pure morphine, see: (a) Hong, C. Y.; Kado, N.; Overman, L. E. J. Am. Chem. Soc. 1993, 115, 11028. (b) White, J. D.; Hrnciar, P.; Stappenbeck, F. J. Org. Chem. 1997, 62, 5250. (c) Trauner, D.; Bats, J. W.; Werner, A.; Mulzer, J. J. Org. Chem. 1998, 63, 5908. (d) Nagata, H.; Miyazawa, N.; Ogasawara, K. Chem. Commun. 2001, 1094.
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(1998)
J. Org. Chem.
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Trauner, D.1
Bats, J.W.2
Werner, A.3
Mulzer, J.4
-
9
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0035927908
-
-
For leading references to previous syntheses of enantiomerically pure morphine, see: (a) Hong, C. Y.; Kado, N.; Overman, L. E. J. Am. Chem. Soc. 1993, 115, 11028. (b) White, J. D.; Hrnciar, P.; Stappenbeck, F. J. Org. Chem. 1997, 62, 5250. (c) Trauner, D.; Bats, J. W.; Werner, A.; Mulzer, J. J. Org. Chem. 1998, 63, 5908. (d) Nagata, H.; Miyazawa, N.; Ogasawara, K. Chem. Commun. 2001, 1094.
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(2001)
Chem. Commun.
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Nagata, H.1
Miyazawa, N.2
Ogasawara, K.3
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10
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33947457625
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1952)
J. Am. Chem. Soc.
, vol.74
, pp. 1109
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Gates, M.1
Tschudi, G.2
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11
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1954)
J. Am. Chem. Soc.
, vol.76
, pp. 312
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Elad, D.1
Ginsburg, D.2
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12
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0014178250
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1967)
Chem. Ber.
, vol.100
, pp. 1550
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Grewe, R.1
Friedrichsen, W.2
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13
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0003023946
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1967)
Tetrahedron Lett.
, vol.41
, pp. 4055
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Morrison, G.C.1
Waite, R.O.2
Shavel J., Jr.3
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14
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0014461918
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1969)
J. Chem. Soc. C
, pp. 2030
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Kametani, T.1
Ihara, M.2
Fukumoto, K.3
Yagi, H.4
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15
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0016843247
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1975)
J. Am. Chem. Soc.
, vol.97
, pp. 1239
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Schwartz, M.A.1
Mami, I.S.2
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16
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0018743195
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1979)
Recl. Trav. Chim. Pays-Bas.
, vol.98
, pp. 419
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Lie, T.S.1
Maat, L.2
Beyerman, H.C.3
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17
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0000221405
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1980)
J. Org. Chem.
, vol.45
, pp. 3135
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Rice, K.C.1
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1982)
Tetrahedron Lett.
, vol.23
, pp. 285
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Evans, D.A.1
Mitch, C.H.2
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19
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0020587259
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1983)
J. Org. Chem.
, vol.48
, pp. 227
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Moos, W.H.1
Gless, R.D.2
Rapoport, H.3
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20
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0023151035
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1987)
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Toth, J.E.1
Fuchs, P.L.2
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21
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0026687198
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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(1992)
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Kerr, M.A.2
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For leading references to previous syntheses of racemic morphine, see: (a) Gates, M.; Tschudi, G. J. Am. Chem. Soc. 1952, 74, 1109. (b) Elad, D.; Ginsburg, D. J. Am. Chem. Soc. 1954, 76, 312. (c) Grewe, R.; Friedrichsen, W. Chem. Ber. 1967, 100, 1550. (d) Morrison, G. C.; Waite, R. O.; Shavel, J., Jr. Tetrahedron Lett. 1967, 41, 4055. (e) Kametani, T.; Ihara, M.; Fukumoto, K.; Yagi, H. J. Chem. Soc. C 1969, 2030. (f) Schwartz, M. A.; Mami, I. S. J. Am. Chem. Soc. 1975, 97, 1239. (g) Lie, T. S.; Maat, L.; Beyerman, H. C. Recl. Trav. Chim. Pays-Bas 1979, 98, 419. (h) Rice, K. C. J. Org. Chem. 1980, 45, 3135. (i) Evans, D. A.; Mitch, C. H. Tetrahedron Lett. 1982, 23, 285. (j) Moos, W. H.; Gless, R. D.; Rapoport, H. J. Org. Chem. 1983, 48, 227. (k) Toth, J. E.; Fuchs, P. L. J. Org. Chem. 1987, 52, 473. (l) Tius, M. A.; Kerr, M. A. J. Am. Chem. Soc. 1992, 114, 5959. (m) Parker, K. A.; Fokas, D. J. Org. Chem. 1994, 59, 3933.
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Fokas, D.2
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For leading references to previous approaches to the ring system of morphine, see: (a) Monkivic, I.; Conway, T. T.; Wong, H.; Perron, Y. G.; Patchter, I. J.; Belleau, B. J. Am. Chem. Soc. 1973, 95, 7910. (b) Schultz, A. G.; Lucci, R. D. J. Chem. Soc., Chem. Commun. 1976, 925. (c) Ciganek, E. J. Am. Chem. Soc. 1981, 103, 6261. (d) Boger, D. L.; Patel, M.; Mullican, M. D. Tetrahedron Lett. 1982, 23, 4559. (e) Hudlicky, T.; Boros, C. H.; Boros, E. E. Synthesis 1992, 174.
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Conway, T.T.2
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Perron, Y.G.4
Patchter, I.J.5
Belleau, B.6
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For leading references to previous approaches to the ring system of morphine, see: (a) Monkivic, I.; Conway, T. T.; Wong, H.; Perron, Y. G.; Patchter, I. J.; Belleau, B. J. Am. Chem. Soc. 1973, 95, 7910. (b) Schultz, A. G.; Lucci, R. D. J. Chem. Soc., Chem. Commun. 1976, 925. (c) Ciganek, E. J. Am. Chem. Soc. 1981, 103, 6261. (d) Boger, D. L.; Patel, M.; Mullican, M. D. Tetrahedron Lett. 1982, 23, 4559. (e) Hudlicky, T.; Boros, C. H.; Boros, E. E. Synthesis 1992, 174.
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For leading references to previous approaches to the ring system of morphine, see: (a) Monkivic, I.; Conway, T. T.; Wong, H.; Perron, Y. G.; Patchter, I. J.; Belleau, B. J. Am. Chem. Soc. 1973, 95, 7910. (b) Schultz, A. G.; Lucci, R. D. J. Chem. Soc., Chem. Commun. 1976, 925. (c) Ciganek, E. J. Am. Chem. Soc. 1981, 103, 6261. (d) Boger, D. L.; Patel, M.; Mullican, M. D. Tetrahedron Lett. 1982, 23, 4559. (e) Hudlicky, T.; Boros, C. H.; Boros, E. E. Synthesis 1992, 174.
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Ciganek, E.1
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26
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For leading references to previous approaches to the ring system of morphine, see: (a) Monkivic, I.; Conway, T. T.; Wong, H.; Perron, Y. G.; Patchter, I. J.; Belleau, B. J. Am. Chem. Soc. 1973, 95, 7910. (b) Schultz, A. G.; Lucci, R. D. J. Chem. Soc., Chem. Commun. 1976, 925. (c) Ciganek, E. J. Am. Chem. Soc. 1981, 103, 6261. (d) Boger, D. L.; Patel, M.; Mullican, M. D. Tetrahedron Lett. 1982, 23, 4559. (e) Hudlicky, T.; Boros, C. H.; Boros, E. E. Synthesis 1992, 174.
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Boger, D.L.1
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Mullican, M.D.3
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For leading references to previous approaches to the ring system of morphine, see: (a) Monkivic, I.; Conway, T. T.; Wong, H.; Perron, Y. G.; Patchter, I. J.; Belleau, B. J. Am. Chem. Soc. 1973, 95, 7910. (b) Schultz, A. G.; Lucci, R. D. J. Chem. Soc., Chem. Commun. 1976, 925. (c) Ciganek, E. J. Am. Chem. Soc. 1981, 103, 6261. (d) Boger, D. L.; Patel, M.; Mullican, M. D. Tetrahedron Lett. 1982, 23, 4559. (e) Hudlicky, T.; Boros, C. H.; Boros, E. E. Synthesis 1992, 174.
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Hudlicky, T.1
Boros, C.H.2
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Harrison, A.W.3
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0010968685
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note
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13C NMR and also to simplify the chiral ketal product distribution and separation.
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35
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0010963407
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note
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(b) Sodium bis(2-methoxyethoxy)aluminum hydride is sold as both Red-Al and Vitride.
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37
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0011011089
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note
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Attempted epoxidation with peracids led to extensive decomposition.
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38
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0001304372
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Iijima, I.; Rice, K. C.; Silverton, J. V. Heterocycles 1977, 6, 1157.
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Heterocycles
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Iijima, I.1
Rice, K.C.2
Silverton, J.V.3
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40
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0011005339
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note
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β-Tetralone 13 was initially ketalized with (R,R)-(+)-hydrobenzoin. The first ketal diastereomer to elute via chromatography was converted to the p-bromobenzenesulfonamide i. This was determined by X-ray analysis to have the configuration at C-9, C-13, and C-14 shown.
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