Scandium chloride, alkyl and phenyl complexes of diamido-donor ligands

Journal of the Chemical Society. Dalton Transactions

Volumn , Issue 24, 2002, Pages 4649-4657

  Ward, Benjamin D ^a   Dubberley, Stuart R ^a   Maisse François, Aline ^b   Gade, Lutz H ^b   Mountford, Philip ^a  

^a UNIVERSITY OF OXFORD   (United Kingdom)

^b UNIVERSITÉ DE STRASBOURG   (France)

Author keywords

[No Author keywords available]

Indexed keywords

CRYSTAL STRUCTURE; DIMERS; MONOMERS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANOMETALLICS;

PROTONOLYSIS REACTIONS;

SCANDIUM COMPOUNDS;

EID: 0037153851     PISSN: 14727773     EISSN: None     Source Type: Journal    
DOI: 10.1039/B209382K     Document Type: Article

References (45)

1. For recent reviews and leading references see: (a) P. R. Meehan, D. R. Aris and G. R. Willey, Coord. Chem. Rev., 1999, 181, 121;
2. (b) S. A. Cotton, Polyhedron, 1999, 18, 1691;
3. (c) F. T. Edelmann, in Comprehensive Organometallic Chemistry, E. W. Abel, F. G. A. Stone and G. Wilkinson, ed., Pergamon, Oxford, 1995, 2nd edn., vol. 4, p. 10;
4. (d) F. A. Hart, in Comprehensive Coordination Chemistry, R. D. Gillard, J. A. McCleverty and G. Wilkinson, ed., Pergamon, Oxford, 1987, vol. 3, p. 1059;
5. (e) F. G. N. Cloke, in Comprehensive Organometallic Chemistry, E. W Abel, F. G. A. Stone and G. Wilkinson, ed., 1995, 2nd edn., vol. 4, p. 1;
6. (f) P. J. Chirik and J. E. Bercaw, in Metallocenes: Synthesis, Reactivity, Applications, A. Togni and R. L. Halterman, ed., Wiley-VCH, New York, 1998, vol. 1, p. 111;
7. (g) J. Okuda and T. Eberle, in Metallocenes: Synthesis, Reactivity, Applications, A. Togni and R. L. Halterman, ed., Wiley-VCH, New York, 1998, vol. 1, p. 415.
8. J. Arnold, C. G. Hoffman, D. Y. Dawson and F. J. Hollander, Organometallics, 1993, 12, 3645.
9. F. T. Edelmann and J. Richter, Eur. J. Solid State Inorg. Chem., 1996, 33, 157; J. R. Hagedorn and J. Arnold, Organometallics, 1996, 15, 984.
10. F. T. Edelmann and J. Richter, Eur. J. Solid State Inorg. Chem., 1996, 33, 157; J. R. Hagedorn and J. Arnold, Organometallics, 1996, 15, 984.
11. M. D. Fryzuk, G. Giesbrecht and S. J. Rettig, Organometallics, 1996, 15, 3329.
12. P. L. Arnold, F. G. N. Cloke, P. B. Hitchcock and J. F. Nixon, J. Am. Chem. Soc., 1996, 118, 7630.; P. L. Arnold, F. G. N. Cloke and J. F. Nixon, Chem. Commun., 1998, 797.
13. P. L. Arnold, F. G. N. Cloke, P. B. Hitchcock and J. F. Nixon, J. Am. Chem. Soc., 1996, 118, 7630.; P. L. Arnold, F. G. N. Cloke and J. F. Nixon, Chem. Commun., 1998, 797.
14. S. Zhang and W. E. Piers, Organometallics, 2001, 20, 2088; P. G. Hayes, W. E. Piers and R. McDonald, J. Am. Chem. Soc., 2002, 124, 2132; P. G. Hayes, W. E. Piers, L. W. M. Lee, L. K. Knight, M. Parvez, M. R. J. Elsegood and W. Clegg, Organometallics, 2001, 20, 2533; D. J. H. Emslie, W. E. Piers and R. MacDonald, J. Chem. Soc., Dalton Trans., 2002, 293; J. Blackwell, C. Lehr, Y. Sun, W. E. Piers, S. D. Pearce-Batchilder, M. J. Zaworotko and V. G. Young Jr., Can. J. Chem., 1997, 75, 702.
15. S. Zhang and W. E. Piers, Organometallics, 2001, 20, 2088; P. G. Hayes, W. E. Piers and R. McDonald, J. Am. Chem. Soc., 2002, 124, 2132; P. G. Hayes, W. E. Piers, L. W. M. Lee, L. K. Knight, M. Parvez, M. R. J. Elsegood and W. Clegg, Organometallics, 2001, 20, 2533; D. J. H. Emslie, W. E. Piers and R. MacDonald, J. Chem. Soc., Dalton Trans., 2002, 293; J. Blackwell, C. Lehr, Y. Sun, W. E. Piers, S. D. Pearce-Batchilder, M. J. Zaworotko and V. G. Young Jr., Can. J. Chem., 1997, 75, 702.
16. S. Zhang and W. E. Piers, Organometallics, 2001, 20, 2088; P. G. Hayes, W. E. Piers and R. McDonald, J. Am. Chem. Soc., 2002, 124, 2132; P. G. Hayes, W. E. Piers, L. W. M. Lee, L. K. Knight, M. Parvez, M. R. J. Elsegood and W. Clegg, Organometallics, 2001, 20, 2533; D. J. H. Emslie, W. E. Piers and R. MacDonald, J. Chem. Soc., Dalton Trans., 2002, 293; J. Blackwell, C. Lehr, Y. Sun, W. E. Piers, S. D. Pearce-Batchilder, M. J. Zaworotko and V. G. Young Jr., Can. J. Chem., 1997, 75, 702.
17. S. Zhang and W. E. Piers, Organometallics, 2001, 20, 2088; P. G. Hayes, W. E. Piers and R. McDonald, J. Am. Chem. Soc., 2002, 124, 2132; P. G. Hayes, W. E. Piers, L. W. M. Lee, L. K. Knight, M. Parvez, M. R. J. Elsegood and W. Clegg, Organometallics, 2001, 20, 2533; D. J. H. Emslie, W. E. Piers and R. MacDonald, J. Chem. Soc., Dalton Trans., 2002, 293; J. Blackwell, C. Lehr, Y. Sun, W. E. Piers, S. D. Pearce-Batchilder, M. J. Zaworotko and V. G. Young Jr., Can. J. Chem., 1997, 75, 702.
18. S. Zhang and W. E. Piers, Organometallics, 2001, 20, 2088; P. G. Hayes, W. E. Piers and R. McDonald, J. Am. Chem. Soc., 2002, 124, 2132; P. G. Hayes, W. E. Piers, L. W. M. Lee, L. K. Knight, M. Parvez, M. R. J. Elsegood and W. Clegg, Organometallics, 2001, 20, 2533; D. J. H. Emslie, W. E. Piers and R. MacDonald, J. Chem. Soc., Dalton Trans., 2002, 293; J. Blackwell, C. Lehr, Y. Sun, W. E. Piers, S. D. Pearce-Batchilder, M. J. Zaworotko and V. G. Young Jr., Can. J. Chem., 1997, 75, 702.
19. P. Roussel, N. W. Alcock and P. Scott, Chem. Commun., 1998, 801.
20. M. A. Putzer, J. S. Rogers and G. C. Bazan, J. Am. Chem. Soc., 1999, 121, 8112.
21. S. Hajela, W. P. Schaefer and J. E. Bercaw, J. Organomet. Chem., 1997, 532, 45.
22. (a) S. C. Lawrence, S. R. Dubberley and P. Mountford, manuscript in preparation;
23. (b) S. Y. Bylikin, D. A. Robson, N. A. H. Male, L. H. Rees, P. Mountford and M. Schröder, J. Chem. Soc., Dalton Trans., 2001, 170;
24. (c) M. E. G. Skinner, B. R. Tyrrell, B. D. Ward and P. Mountford, J. Organomet. Chem., 2002, 647, 145;
25. (d) M. E. G. Skinner and P. Mountford, J. Chem. Soc., Dalton Trans., 2002, 1694.
26. M. E. G. Skinner, D. A. Cowhig and P. Mountford, Chem. Commun., 2000, 1167; M. E. G. Skinner, Y. Li and P. Mountford, Inorg. Chem., 2002, 41, 1110.
27. M. E. G. Skinner, D. A. Cowhig and P. Mountford, Chem. Commun., 2000, 1167; M. E. G. Skinner, Y. Li and P. Mountford, Inorg. Chem., 2002, 41, 1110.
28. For a review and leading references see L. H. Gade, Chem. Commun., 2000, 173 (feature article).
29. S. Friedrich, M. Schubart, L. H. Gade, I. J. Scowen, A. J. Edwards and M. McPartlin, Chem. Ber./Recueil, 1997, 130, 1751.
30. P. Mehrkhodavandi, P. J. Bonitatebus Jr. and R. R. Schrock, J.. Am. Chem. Soc., 2000, 122, 7841; J. P. Araujo, D. K. Wicht, R. R. Schrock and P. J. Bonitatebus, Organometallics, 2001, 20, 5682.
31. P. Mehrkhodavandi, P. J. Bonitatebus Jr. and R. R. Schrock, J.. Am. Chem. Soc., 2000, 122, 7841; J. P. Araujo, D. K. Wicht, R. R. Schrock and P. J. Bonitatebus, Organometallics, 2001, 20, 5682.
32. N. Emig, H. Nguyen, H. Krautscheid, R. Reau, J. Cazaux and G. Bertrand, Organometallics, 1998, 17, 3599.
33. F. G. N. Cloke, P. B. Hitchcock and J. B. Love, J. Chem. Soc., Dalton Trans., 1995, 25.
34. A. D. Horton, J. de With, A. J. van der Linden and H. van de Weg, Organometallics, 1996, 15, 2672.
35. For a review and leading references see L. H. Gade and P. Mountford, Coord. Chem. Rev., 2001, 216-217, 65.
36. B. D. Ward, R. A. Whannel, T. A. Lowes and P. Mountford, manuscript in preparation.
37. F. H. Allen and O. Kennard, Chem. Des. Automat. News, 1993, 8, 1-31; The United Kingdom Chemical Database Service, D. A. Fletcher, R. F. McMeeking and D. Parkin, J. Chem. Inf. Comput. Sci., 1996, 36, 746.
38. F. H. Allen and O. Kennard, Chem. Des. Automat. News, 1993, 8, 1-31; The United Kingdom Chemical Database Service, D. A. Fletcher, R. F. McMeeking and D. Parkin, J. Chem. Inf. Comput. Sci., 1996, 36, 746.
39. M. F. Lappert and R. Pearce, J. Chem. Soc., Chem. Commun., 1973, 126.
40. M. A. Putzer and G. P. Bartholomew, Z. Anorg. Allg. Chem., 1999, 625, 1777.
41. A. R. Rossi and R. Hoffmann, Inorg. Chem., 1975, 14, 365.
42. D. Gewirth, The HKL Manual, written with the co-operation of the program authors, Z. Otwinowski and W. Minor, Yale University, 1995.
43. A. Altomare, G. Cascarano, G. Giacovazzo, A. Guagliardi, M. C. Burla, G. Polidori and M. Camalli, J. Appl. Crystallogr., 1994, 27, 435.
44. OpenMoleN, Interactive Structure Solution, Nonius, Delft, 1997.
45. D. J. Watkin, C. K. Prout, J. R. Carruthers, P. W. Betteridge and R. I. Cooper, CRYSTALS Issue 11, Chemical Crystallography Laboratory, University of Oxford, 2001.