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Volumn 43, Issue 34, 2002, Pages 5941-5944

Pure acetonitrile as solvent for the efficient electrochemical conversion of aryl bromides in organozinc species and their coupling reaction with acetyl chloride

(4) Fillon, Hyacinthe a Le Gall, Erwan a Gosmini, Corinne a Périchon, Jacques a

a CNRS (France)

Author keywords

[No Author keywords available]

Indexed keywords

ACETONITRILE; ACETYLCHOLINE; BROMINE DERIVATIVE; COBALT BROMIDE; LIGAND; PALLADIUM; SOLVENT; UNCLASSIFIED DRUG;

ARTICLE; CATALYST; CELL; ELECTROCHEMICAL ANALYSIS; SPECIES;

EID: 0037136099 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(02)01256-X Document Type: Article

Times cited : (31)

References (16)

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- -2 mmol) and a slight excess of acetyl chloride (1 mL, 12.5 mmol) at room temperature. The solution is stirred until total consumption of the organozinc compound (1-3 h) and quenched by addition of a 2 M HCl solution. The organic materials are then extracted with diethyl ether and the organic layer washed with brine, dried with magnesium sulfate and evaporated under reduced pressure. The resulting crude oil is purified over silica gel using a pentane/diethyl ether mixture (90/10) as an eluent.

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