Preparation of resolved fourfold symmetric amphiphilic helices using chiral metallacrown building blocks

Angewandte Chemie - International Edition

Volumn 41, Issue 24, 2002, Pages 4667-4670

  Cutland Van Noord, Annabel D ^a   Kampf, Jeff W ^a   Pecoraro, Vincent L ^a  

^a UNIVERSITY OF MICHIGAN   (United States)

Author keywords

Copper; Crown compounds; Helical structures; Lanthanides; Supramolecular chemistry

Indexed keywords

COMPLEXATION; COORDINATION REACTIONS; IMAGE ANALYSIS; MIRRORS;

CHILARITY;

ISOMERS;

AMPHOPHILE; HYDROXAMIC ACID DERIVATIVE; LIGAND; PHENYLALANINE;

CHEMICAL PARAMETERS; CHEMICAL STRUCTURE; CHIRALITY; COMPLEX FORMATION; ISOMER; SHORT SURVEY; SYNTHESIS;

EID: 0037122156     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200290010     Document Type: Short Survey

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30. +.
31. 2, R1 = 0.0560, and wR2 = 0.1543. A PLATON/SQUEEZE subroutine (Spek, A.L. Platon, Acta Crystallogr. Sect. A 1990, 46, C-34) was used to handle solvent and anion disorder. Further details are given in the Supporting Information.
32. +.
33. 2, R1 = 0.0387, wR2 = 0.1025. A PLATON/SQUEEZE subroutine (Spek) was used to handle solvent and anion disorder. Further details are given in the Supporting Information. CCDC-192390 (1) and CCDC-192391 (1a) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB21EZ, UK; fax: (+ 44) 1223-336-033; or deposit@ccdc.cam.ac.uk).