A new mild and rapid deprotecting method for aryl cyclohex-2-en-1-yl ethers to phenols

Tetrahedron Letters

Volumn 43, Issue 37, 2002, Pages 6533-6535

  Carato, Pascal ^a   Laconde, Guillaume ^a   Ladjel, Chehla ^a   Depreux, Patrick ^a   Hénichart, Jean Pierre ^a  

^a Faculté des Sciences Pharmaceutiques et Biologiques Université de Lille   (France)

Author keywords

Phenol deprotection

Indexed keywords

ETHER DERIVATIVE; PHENOL DERIVATIVE;

ARTICLE; DEGRADATION; DEPROTECTION REACTION; MOLECULAR STABILITY; SUBSTITUTION REACTION; TEMPERATURE;

EID: 0037048514     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)01466-1     Document Type: Article

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11. 3 (3 mmol) and the desired halogeno reagent (3 mmol). The solution was refluxed for 2 h, filtered and evaporated under reduced pressure. The oily residue was washed with petroleum ether (40-60) and recrystallized. Yield (89-98%).
12. Ar).
13. Ar).