SCOPUS 정보 검색 플랫폼

Volumn 43, Issue 19, 2002, Pages 3585-3587

Mild conversion of electron deficient aryl fluorides to phenols using 2-(methylsulfonyl)ethanol

Author keywords

[No Author keywords available]

Indexed keywords

2 (METHYLSULFONYL)ETHANOL; ALCOHOL; FLUORIDE; PHENOL DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; ELECTRON; GEL CHROMATOGRAPHY; ORGANIC CHEMISTRY; PURIFICATION; SYNTHESIS;

EID: 0037029779 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(02)00561-0 Document Type: Article

Times cited : (38)

References (6)

2
- 0004150487
- Collective 2nd ed.; John Wiley and Sons: New York
- (1941) Organic Synthesis , vol.1
- Gilman, H.¹

3
- 0004137017
- Interscience: New York
- (1971) The Chemistry of the Hydroxyl Group
- Patai, S.¹

5
- 0035815141
- (2001) J. Org. Chem. , vol.66 , pp. 2498-2500
- Parrish, C.¹ Buchwald, S.²

6
- 0008860364
- General procedure: To a stirring solution of aryl fluoride (1.0 equiv.) in DMF (0.66 M) was added 2-(methylsulfonyl-ethanol) (1.5 equiv.) and the solution cooled to 0°C. Sodium hydride (3.0 equiv.) was added and the reaction mixture allowed to warm to room temperature. The mixture was quenched with a 1N HCl solution and partitioned between ethyl acetate and brine. The organic layer was concentrated to dryness and the crude organics purified by flash column chromatography.

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