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max = 56.5°, R(int) = 0.0327), GOF = 1.060, R1 = 0.0209, wR2 = 0.0562. The final cycles of least-squares refinement included atomic coordinates and anisotropic thermal parameters for all atoms. Diffractometer: Siemens Smart CCD (Mo Kα radiation, graphite monochromator). Structure solution and refinement: SHELXTL(Sheldrick G.M. Version 5.1, Siemens Analytical X-ray Instruments, Madison, WI, 1998). Absorption correction: SADABS (Sheldrick, G. M., University of Göttingen, 1995)
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max = 56.5°, R(int) = 0.0327), GOF = 1.060, R1 = 0.0209, wR2 = 0.0562. The final cycles of least-squares refinement included atomic coordinates and anisotropic thermal parameters for all atoms. Diffractometer: Siemens Smart CCD (Mo Kα radiation, graphite monochromator). Structure solution and refinement: SHELXTL(Sheldrick G.M.Version 5.1, Siemens Analytical X-ray Instruments, Madison, WI, 1998). Absorption correction: SADABS (Sheldrick, G. M., University of Göttingen, 1995)
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