Determination of 17β-estradiol in bovine plasma: Development of a highly sensitive technique by ion trap gas chromatography-tandem mass spectometry using negative chemical ionization

Journal of Mass Spectrometry

Volumn 37, Issue 12, 2002, Pages 1266-1271

  Biancotto, Giancarlo ^a   Angeletti, Roberto ^a   Traldi, Pietro ^b   Silvestri, Massimiliano ^c   Saccon, Mauro ^c   Guidugli, Federico ^c  

^a ISTITUTO ZOOPROFILATTICO SPERIMENTALE DELLE VENEZIE   (Italy)

^b CNR   (Italy)

^c R and C Scientific ^*  (Italy)

Author keywords

17 estradiol; Ion trap; MSn; Negative chemical ionization; Plasma

Indexed keywords

CONCENTRATION (PROCESS); DIAGNOSIS; EXTRACTION; GAS CHROMATOGRAPHY; IONIZATION; IONS; METHANE;

BOVINE PLASMA;

MASS SPECTROMETRY;

ANION; BROMINE DERIVATIVE; ESTRADIOL; METHANE; TRIFLUOROACETAMIDE DERIVATIVE; ION;

ACCURACY; ANALYTIC METHOD; ARTICLE; BLOOD SAMPLING; CATTLE; CHEMICAL STRUCTURE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; ESTRADIOL BLOOD LEVEL; FRAGMENTATION REACTION; GAS CHROMATOGRAPHY; HORMONE DETERMINATION; INTERMETHOD COMPARISON; IONIZATION; NONHUMAN; PRIORITY JOURNAL; PURIFICATION; RADIOIMMUNOASSAY; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; STANDARDIZATION; STRUCTURE ANALYSIS; TANDEM MASS SPECTROMETRY; ANIMAL; BLOOD; CHEMISTRY; MASS FRAGMENTOGRAPHY; METHODOLOGY; REPRODUCIBILITY;

BOVINAE;

ANIMALS; CATTLE; ESTRADIOL; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; IONS; MOLECULAR STRUCTURE; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 0036932226     PISSN: 10765174     EISSN: None     Source Type: Journal    
DOI: 10.1002/jms.397     Document Type: Article

References (12)

1. Hoffmann B, Goes de Pinho T, Schuler G. Exp. Clin. Endocrinol. Diabetes 1997; 105: 296.
2. Hendricks L, Gielen B, Pottie G, Haesen V, Bagyary S, Raus J. Anal. Chim. Acta 1993; 275: 113.
3. Korenman SG, Stevens RS, Carpenter LA. J. Clin. Endocrinol. Metab. 1974; 38: 718.
4. Council of the European Communities, Council Directive 96/23/EC. Off. J. Eur. Communities: Legis. 1996; L125: 3.
5. Bagnati R, Castelli MG, Airoldi L, Oriundi MP, Ubaldi A, Fanelli R. J. Chromatogr. Biomed-Appl. 1990; 527(2): 267.
6. Bagnati R, Fanelli R. J. Chromatogr. 1991; 547(1-2): 325.
7. Yost RA. Spectra. Finnigan: 1990; 3.
8. Nakamura S, Tan Hwee S, Daishima S. J. Chromatogr. Sect. A 2001; 919: 275.
9. Daeseleire E, Vandeputte R, Van Peteghem C. Analyst 1998; 123: 2595.
10. Draisci R, Palleschi L, Ferretti E, Marchiafava C, Lucentini L, Cammarata P. Analyst 1998; 123: 2605.
11. Singh G, Gutierrez A, Keyang X, Blair IA. Anal. Chem. 2000; 72: 3007.
12. Council of the European Communities, Commission Decision 93/256/EEC. Off. J. Eur. Communities: Legis. 1993; L118: 64.