Expanding the frequency range of the solid-state T1ρ experiment for heteronuclear dipolar relaxation

Solid State Nuclear Magnetic Resonance

Volumn 22, Issue 4, 2002, Pages 423-438

  Krushelnitsky, Alexey ^a   Kurbanov, Rauf ^a   Reichert, Detlef ^b   Hempel, Guenter ^b   Schneider, Horst ^b   Fedotov, Vladimir ^a  

^a KAZAN INSTITUTE OF BIOCHEMISTRY AND BIOPHYSICS   (Russian Federation)

^b MARTIN LUTHER UNIVERSITY HALLE WITTENBERG   (Germany)

Author keywords

Molecular dynamics; NMR relaxation; Proton decoupling; Resonance offset; Rotating frame

Indexed keywords

LATTICE CONSTANTS; MAGNETIC FIELD EFFECTS; MOLECULAR DYNAMICS; NUCLEAR MAGNETIC RESONANCE;

HETERONUCLEAR DIPOLAR RELAXATION;

SOLID STATE PHYSICS;

CARBON; GLYCINE; NITROGEN; POLYLYSINE; PROTON;

ARTICLE; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE; SENSITIVITY AND SPECIFICITY; TEMPERATURE; THEORETICAL MODEL;

CARBON ISOTOPES; GLYCINE; MODELS, THEORETICAL; NITROGEN ISOTOPES; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; POLYLYSINE; PROTONS; SENSITIVITY AND SPECIFICITY; TEMPERATURE;

EID: 0036883036     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1006/snmr.2002.0071     Document Type: Article

References (18)

1. VanderHart D. L., Garroway A. N. J. Chem. Phys. 71:1979;2773-2787.
2. 13C in L-alanine. J. Chem. Phys. 78:1983;3567-3572.
3. 1 ρ NMR experiments by multipulse proton homonuclear decoupling. Magn. Res. Chem. 28:1990;S10-14.
4. Jones G. P. Spin-lattice relaxation in the rotating frame: Weak collision case. Phys. Rev. 148:1966;332-335.
5. Mulder F. A., van Tilborg P. J., Kaptein R., Boelens R. Microsecond time scale dynamics in the RXR DNA-binding domain from a combination of spin-echo and off-resonance rotating frame relaxation measurements. J. Biomol. NMR. 13:1999;275-288.
6. 13C NMR transverse relaxation. Biochemistry. 40:2001;2844-2853.
7. 1 values by a method which suppresses artifacts. J. Magn. Reson. 30:1978;613-616.
8. Abragam A. The Principles of Nuclear Magnetism. 1961;Clarendon Press, Oxford.
9. Kimmich R. NMR Tomography Diffusometry Relaxometry. 1997;Springer-Verlag, New York.
10. 13C-NMR spectroscopy. Biopolymers. 31:1991;967-973.
11. Prestrelski S. J., Tedeschi N., Arakawa T., Carpenter J. F. Dehydration-induced conformational transitions in proteins and their inhibition by stabilizers. Biophys. J. 65:1993;661-671.
12. 13 C nuclear magnetic relaxation in rotating frame. Poly. J. 25:1993;131-139.
13. Goldman M. Spin Temperature and Nuclear Magnetic Resonance in Solids. 1970;Clarendon Press, Oxford.
14. Ivanov Yu. N., Provotorov B. N., Feldman E. B. Thermodynamic theory of NMR spectral line narrowing in solids. Zh. Eksp. Teor. Fiz. (JETP, Moscow). 75:1978;1847-1861.
15. Atsarkin V. A., Khazanovich T. N. Effect of slow molecular movements on nuclear magnetic relaxation under "magic angle" conditions. Zh. Eksp. Teor. Fiz. (JETP, Moscow). 87:1984;279-288.
16. Reichert D., Hempel G., Zimmermann H., Schneider H., Luz Z. Dynamic carbon-13 MAS NMR: Application to benzene ring flips in polyaryl ethers. Solid State NMR. 18:2000;17-36.
17. Reichert D., Zimmermann H., Tekely T. P., Poupko R., Luz Z. Time-reverse ODESSA. A 1D exchange experiment for rotating solids with several groups of equivalent nuclei. J. Magn. Reson. 125:1997;245-258.
18. deAzevedo E., Bonagamba T., Hu W., Schmidt-Rohr K. Centerband-only detection of exchange: Efficient analysis of dynamics in solids by NMR. J. Am. Chem. Soc. 121:1999;8411-8420.