Changes in crystalline properties of nanosized hydroxyapatite powders prepared by low-temperature reactive crystallization

Journal of Chemical Engineering of Japan

Volumn 35, Issue 11, 2002, Pages 1203-1210

  Kim, Woon Soo ^a   Kim, Woo Sik ^b   Hirasawa, Izumi ^c  

^a Myong Ji University   (South Korea)

^b Kyung Hee University   (South Korea)

^c WASEDA UNIVERSITY   (Japan)

Author keywords

Crystallinity; Crystallite size; Hydroxyapatite; Reactive crystallization; Sintering; Supersaturation level

Indexed keywords

CHEMICAL REACTORS; CRYSTAL GROWTH; CRYSTALLIZATION; NANOSTRUCTURED MATERIALS; SINTERING; SUPERSATURATION;

SEMI-BATCH REACTORS;

HYDROXYAPATITE;

CHEMICAL REACTION; CRYSTALLIZATION; HYDROXYAPATITE; LOW TEMPERATURE; POWDER;

EID: 0036871904     PISSN: 00219592     EISSN: None     Source Type: Journal    
DOI: 10.1252/jcej.35.1203     Document Type: Article

References (24)

1. Bernard, L., M. Freche, J. L. Lacout and B. Biscans; "Preparation of Hydroxyapatite by Neutralization at Low Temperature-Influence of Purity of the Raw Martial," Powder Technology, 103, 19-25 (1999)
2. Bertoni, E., A. Bigi, G. Falini, S. Panzavolta and N. Roveri; "Hydroxyapatite/Polyacrylic Acid Nanocrystals," J. Mater. Chem., 9, 779-782 (1999)
3. Chang, C., J, Huang, J. Xia and C. Ding; "Study on Crystallization Kinetics of Plasma Sprayed Hydroxyapatite Coating," Ceramics International, 25, 479-483 (1999)
4. Fujishiro, Y., H. Yabuki, K. Kawamura, T. Sato and A. Okuwaki; "Preparation of Needle-Like Hydroxyapatite by Homogeneous Precipitation under Hydrothermal Conditions," J. Chem. Tech. Biotechnol., 57, 349-353 (1993)
5. Hosoi, K., T. Korenaga, H. Takahashi and N. Yamasaki; "New Synthesis Techniques for Making Hydroxyapatite Ceramics Using Hydrothermal Hot-Pressing," Rev. High Pressure Sci. Technol., 7, 1405-1407 (1998)
6. Kitamura, M.; "Controlling Factor of Polymorphs in Crystallization Process," J. of Crystal Growth, 237-239, 2205-2214 (2002)
7. Koutsopoulos, S., E. Pierri, E. Dalas, N. Tzavellas and N. Klouras; "Effect of Ferricenium Salts on the Crystal Growth of Hydroxyapatite in Aqueous Solution," J. of Crystal Growth, 218, 353-358 (2000)
8. Kweh, S. W. K., K. A. Khor and P. Cheang; "The Production and Characterization of Hydroxyapatite (HA) Powders," J. of Materials Processing Technology, 89-90, 373-377 (1999)
9. Landi, E., A. Tampieri, G. Celotti and S. Sprio; "Densification Behavior and Mechanisms of Synthetic Hydroxyapatites," J. of the European Ceramic Society, 20, 2377-2387 (2000)
10. Lazic, S., J. Katanic-Popovic, S. Zec and N. Miljevic; "Properties of Hydroxyapatite Crystallized from High Temperature Alkaline Solutions," J. of Crystal Growth, 165, 124-128 (1996)
11. Lazic, S.; "Microcrystalline Hydroxyapatite Formation from Alkaline Solutions," J. of Crystal Growth, 147, 147-154 (1995)
12. Li, H., K. A. Khor and P. Cheang; "Properties of Heat-Treated Calcium Phosphate Coatings Deposited by High-Velocity Oxy-Fuel (HVOF) Spray," Biomaterials, 23, 2105-2112 (2002)
13. Liu, C., Y. Huang, W. Shen and J. Cui; "Kinetics of Hydroxyapatite Precipitation at pH 10 to 11," Biomaterials, 22, 301-306 (2001a)
14. Liu, D. M., T. Troczynski and W. J. Tseng; "Water-Based Sol-Gel Synthesis of Hydroxyapatite: Process Development," Biomaterials, 22, 1721-1730 (2001b)
15. 2O at 5, 15, 25 and 37°C," J. of Research of the National Bureau of Standards-A. Physics and Chemistry, 81A, 273-281 (1977)
16. Matsumoto, T., M. Okazaki, M. Inoue, Y. Hamada, M. Taira and J. Takahashi; "Crystallinity and Solubility Characteristics of Hydroxyapatite Adsorbed Amino Acid," Biomaterials, 23, 2241-2247 (2002)
17. Raynaud, S., E. Champion, D. Bernache-Assollant and J.-P. Laval; "Determination of Calcium/Phosphorus Atomic Ratio of Calcium Phosphate Apatites Using X-ray Diffractometry," J. Am. Ceram. Soc., 84, 359-366 (2001)
18. Sada, E., H. Kumazawa and Y. Murakami; "Hydrothermal Synthesis of Crystalline Hydroxyapatites Ultrafine Particles," Chem. Eng. Comm., 103, 57-64 (1991)
19. Tampieri, A., G. Celotti, S. Sprio and C. Mingazzini; "Characteristics of Synthetic Hydroxyapatites and Attempts to Improve their Thermal Stability," Materials Chemistry and Physics, 64, 54-61 (2000)
20. Varma, H. K. and R. Sivakumar; "Dense Hydroxy Apatite Ceramics through Gel Casting Technique," Materials Letters, 29, 57-61 (1996)
21. Yamagishi, N.; "Control of Crystallinity of Hydroxyapatite through Reactive Crystallization," M.S. Thesis, Waseda University, Japan (1999)
22. Yen, F. S., H. L. Wen and Y. T. Hsu; "Crystallite Size Growth and the Derived Dilatometric Effect during q- to a-Phase Transformation of Nano-Sized Alumina Powders," J. of Crystal Growth, 233, 761-773 (2001)
23. 4," Biomaterials, 22, 2705-2712 (2001)
24. Yoshimura, M., H. Suda, K. Okamoto and K. Ioku; "Hydrothermal Synthesis of Biocompatible Whiskers," J. Material Science, 29,